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This paper aims to study previously prepared and fully characterized chitosan nanoparticles (CNPs) as a starting substrate and microwave initiation technique for grafting acrylic acid (AA). This was done to see the influence of both CNPs with respect to well-dispersed nanosized particles, large surface areas, biodegradability, biocompatibility and reactivity and microwave initiation technique with respect to reduction in organic solvents, toxic chemical initiator and exposer time on exploiting the graft yield % and enhancing water solubility and antibacterial properties.

For evaluating the best accurate standard metrological method for calculating the graft yield %, the grafting parameters were stated in terms of graft yield percent and measured gravimetrically (based on dry weight method) and titrimetrically (based on carboxyl content). Microwave power, AA and CNPs concentrations and reaction duration were shown to be the most important parameters influencing the grafting process.

The optimum reaction conditions were obtained when CNPs 1.5 g, AA 150 bows, microwave irradiation power 500 W and reaction duration 120 s were used. Various analytical methods were used to characterize CNPs and poly(AA)–CNPs graft copolymers. According to the findings, Fourier transform infrared spectroscopy examination determines the attachment of carboxyl groups to CNPs chains. The thermogravimetric analysis revealed that the copolymers were more thermally stable than CNPs counterparts. Furthermore, the resulting copolymers were shown to have greater water solubility biodegradability resistance and antibacterial properties than CNPs counterpart. Finally, a preliminary mechanism demonstrating all occasions that occur during the polymerization reaction has been proposed.

The advancement addressed here is undertaken using previously prepared and fully characterized CNPs as a green bio-nanocompatible polymer and microwave initiation technique as green and efficient tool with respect to reduction in organic solvents toxic chemical initiator and exposer time for grafting AA.

The purpose of this article is to study the effect of ferrite content on electric, magnetic and microwave properties of screen-printed y(Ni0.4Co0.2Cd0.4Fe2O4) + (1 − y)Pb(Zr0.52Ti0.48)O3 (y = 0.0, 0.15, 0.30, 0.45, 1.0) thick films on alumina.

Thick films of ferrite–ferroelectric composite on alumina substrate have been delineated using screen printing technique. The structural analysis was carried out using X-ray diffraction method and scanning electron microscopy. The DC electrical resistivity was measured using the two-probe method. The magnetic measurement was carried out using a vibrating sample magnetometer. Microwave absorption was studied in the 8-18 GHz frequency range by using the vector network analyzer (N5230A). The permittivity in the 8-18 GHz frequency range was measured by using voltage standing wave ratio slotted section method.

The formation of two individual ferrite–ferroelectric phases in composite thick films was confirmed by the X-ray diffraction patterns. The scanning electron microscope morphologies show the growth of cobalt-substituted nickel cadmium ferrite grains which are well dispersed in lead zirconium titanate matrix. The DC electrical resistivity increases with increase in ferrite content and decreases with increase in temperature. The present ferrite shows ferromagnetic nature and it increases saturation magnetization and coercivity of the composite thick films. Tuning properties are observed in the Ku-band and broadband X-band microwave absorption is observed in the composite thick films. The imaginary part of permittivity increases with an increase in ferrite content, which increases microwave absorption. The real part of microwave permittivity varied from 17 to around 22 with an increase in ferrite content and it decreases with frequency. The microwave conductivity, which increases with an increase in ferrite content, reveals the loss of polaron conduction, which supports the dielectric loss in the microwave region.

Electric, magnetic and microwave properties of screen-printed y(Ni0.4Co0.2Cd0.4Fe2O4) + (1 − y)Pb(Zr0.52Ti0.48)O3 (y = 0.0, 0.15, 0.30, 0.45, 1.0) composite thick films on alumina substrate is reported for the first time.

This study aims to use multi-functional viscose fabric that was facilely developed with with respect to ease and care characteristics, reinforcement effect and antibacterial activity by using novel echo friendly antibacterial finish based on citric acid/sodium hypophosphite and the authors’ previously tailor-made poly meth acrylic acid (MAA)-chitosan graft copolymer via alternative microwave curing approach instead of traditional high-temperature cure one.

Viscose fabric was paddled twice in the cross-linking formulations containing different concentrations of citric acid, poly (MAA)-chitosan graft copolymer and sodium hypophosphite to 90 % wet pick up and dried at 100°C for 3 min in an electric oven. Then, the treated fabrics were placed on the disk spinner of the microwave oven and cured at different power (100–800 Watt) for various durations (60–180 s). The fabric was then water-rinsed and dried at ambient condition before use.

Results revealed that the above echo friendly method for finished viscose fabrics was found to achieve relatively high dry wrinkle recovery angle and maintain the loss in tensile strength within the acceptable range, as well as antibacterial activity against Escherichia coli and Staphylococcus aureus as a gram-negative and gram-positive bacteria, respectively; in addition to durability up to ten washing cycles. Furthermore, scanning electron microscope images, nitrogen content and add on % of the finished fabric confirmed the penetration of grafted chitosan inside the fabric structure. The tentative mechanism for these reactions is advocated.

The novelty addressed here is undertaken with the advantages of using citric acid as a nonformaldehyde, safe and cheap poly carboxylic acid as a crosslinking agent and sodium hypophosphite as a potential catalyst, in addition to the authors’ noncitable multifunctional echo friendly tailor-made poly (MAA)-chitosan graft copolymer for imparting reinforcement and antibacterial characteristics to viscose fabric that uses the pad-dry/cure microwave fixation for progressively persuaded heat within the fabric during curing.

This was done to see the impact of microwave as green and efficient tool with respect to reduction in organic solvents, chemicals and exposer time as well as fixation temperature on the finishing reaction in comparison with traditional pad-dry-cure method.

Poly (MAA)-chitosan graft copolymer as amphoteric biopolymer was expected to impart multifunctional properties to viscose fabrics especially with comparable dry wrinkle recovery angle and minimize the loss in tensile strength in addition to antibacterial properties in comparison with untreated one.

This paper aims to present an open‐ended microwave curing system for microelectronics components and a numerical analysis framework for virtual testing and prototyping of the system, enabling design of physical prototypes to be optimized, expediting the development process.

An open‐ended microwave oven system able to enhance the cure process for thermosetting polymer materials utilised in microelectronics applications is presented. The system is designed to be mounted on a precision placement machine enabling curing of individual components on a circuit board. The design of the system allows the heating pattern and heating rate to be carefully controlled optimising cure rate and cure quality. A multi‐physics analysis approach has been adopted to form a numerical model capable of capturing the complex coupling that exists between physical processes. Electromagnetic analysis has been performed using a Yee finite‐difference time‐domain scheme, while an unstructured finite volume method has been utilized to perform thermophysical analysis. The two solvers are coupled using a sampling‐based cross‐mapping algorithm.

The numerical results obtained demonstrate that the numerical model is able to obtain solutions for distribution of temperature, rate of cure, degree of cure and thermally induced stresses within an idealised polymer load heated by the proposed microwave system.

The work is limited by the absence of experimentally derived material property data and comparative experimental results. However, the model demonstrates that the proposed microwave system would seem to be a feasible method of expediting the cure rate of polymer materials.

The findings of this paper will help to provide an understanding of the behaviour of thermosetting polymer materials during microwave cure processing.

The aim of this paper is to investigate microwave Ku band absorbance, complex permittivity, and permeability of SrFe₁₂O₁₉ thick films by a simple and novel waveguide technique.

The glass frit free or fritless strontium hexaferrite thick films were formulated on alumina by screen printing technique from the powder synthesized by chemical co precipitation method for pH 11 adjusted during the reaction. The 13‐18 GHz frequency band microwave absorbance of the SrFe₁₂O₁₉ thick films by a simple waveguide method. The complex permittivity and permeability of strontium hexaferrite thick films was measured by voltage standing wave ratio technique.

SrFe₁₂O₁₉ thick films show high ∼80 percent absorbance in the whole 13‐18 GHz frequency band. The thickness dependant microwave properties of strontium hexaferrite thick films were observed. The real permittivity ε′ lies in between eight and 35 with the variation in thickness of the thick film SrFe₁₂O₁₉. The real microwave permeability μ′ of strontium hexaferrite thick films lies in the range 1.12‐6.41. The resonance type behavior was observed at frequency 14.3 GHz. The SrFe₁₂O₁₉ thick film of thickness 30 μm could be a wide band (∼5,000 MHz) absorber with absorbance ∼87 percent for the whole 13‐18 GHz frequency band.

The complex permeability of strontium hexaferrite thick films was measured by simple novel waveguide method. The high absorbance (∼87 percent) of thick film SrFe₁₂O₁₉ over a broad band ∼5,000 MHz will be useful in achieving RAM coatings required for 13‐18 GHz frequency band.

The purpose of this paper is to study the microwave interactions in polymer thick film resistors, namely, polyvinyl chloride (PVC)-graphite thick film resistors, and its applications in trimming of these resistors.

We applied microwave radiation in the form of pulses of various pulse durations and with different powers to polymer thick film resistors and observed the variation of resistance of these resistors with microwave radiation.

The paper finds that microwave radiation can be used for trimming of polymer thick film resistors.

The research implication of this paper is that polymer thick film resistors can be trimmed practically using this method.

The practical implication of this paper is that we can trim the polymer thick film resistors, namely, PVC-graphite thick film resistor, by using this method.

The value of the paper is in showing that microwave radiation can be used to trim downwards in the case of high-value resistors and trim upwards in the case of low-value resistors.

This paper aims to introduce and illustrate a computational technique capable of determining the geometry and complex permittivity of a supplementary dielectric insert making distributions of microwave-induced dissipated power within the processed material as uniform as possible.

The proposed technique is based on a 3D electromagnetic model of the cavity containing both the processed material and the insert. Optimization problem is formulated for design variables (geometrical and material parameters of the insert) identified from computational tests and an objective function (the relative standard deviation [RSD]) introduced as a metric of the field uniformity. Numerical inversion is performed with the method of sequential quadratic programming.

Functionality of the procedure is illustrated by synthesis of a dielectric insert in an applicator for microwave fixation. Optimization is completed for four design variables (two geometrical parameters, dielectric constant and the loss factor of the insert) with 1,000 points in the database. The best three optimal solutions provide RSD approximately 20 per cent, whereas for the patterns corresponding to all 1,000 non-optimized (randomly chosen) sets of design variables this metric is in the interval from 27 to 136 per cent with the average of 78 per cent.

As microwave thermal processing is intrinsically inhomogeneous and the heating time is not a part of the underlying model, the procedure is able to lead only to a certain degree of closeness to uniformity and is intended for applications with high heating rates. The initial phase of computational identification of design variables and their bounds is therefore very important and may pre-condition the “quality” of the optimal solution. The technique may work more efficiently in combination with advanced optimization techniques dealing with “smart” (rather than random) generation of the data; for the use with more general microwave heating processes characterized by lower heating rates, the technique has to use the metric of non-uniformity involving temperature and heating time.

While the procedure can be used for computer-aided design (CAD) of microwave applicators, a related practical limitation may emerge from the fact that the material with particular complex permittivity (determined in the course of optimization) may not exist. In such cases, the procedure can be rerun for the constant values of material parameters of the available medium mostly close to the optimal ones to tune geometrical parameters of the insert. Special manufacturing techniques capable of producing a material with required complex permittivity also may be a practical option here.

Non-uniformity of microwave heating remains a key challenge in the design of many practical applicators. This paper suggests a concept of a practical CAD and outlines corresponding computational procedure that could be used for designing a range of applied systems with high heating rates.

Among the various applications involving the use of microwave energy, its growing utility within the mining industry is particularly noteworthy. Conventional grinding processes are often overburdened by energy inefficiencies that are directly related to machine wear, pollution and rising project costs. In this work, we numerically investigate the effects of microwave pretreatment through a series of compression tests as a means to help mitigate these energy inefficiencies.

We investigate the effects of microwave pretreatment on various rock samples, as quantified by uniaxial compression tests. In particular, we assign sample heterogeneity based on a Gaussian statistical distribution and invoke a damage model for elemental tensile and compressive stresses based on the maximum tensile stress and the Mohr–Coulomb theories, respectively. We further couple the electromagnetic, thermal and solid displacement relations using finite element modeling.

(1) Increased power intensity during microwave pretreatment results in decreased axial compressive stress. (2) Leveraging statistics to induce variable compressive and tensile strength can greatly facilitate sample heterogeneity and prove necessary for damage modeling. (3) There exists a nonlinear trend to the reduction in smax with increasing power levels, implying an optimum energy output efficiency to create the maximum degradation-power cost relationship.

Previous research in this area has been largely limited to two-dimensional thermo-electric models. The onset of high-performance computing has allowed for the development of high-fidelity, three-dimensional models with coupled equations for electromagnetics, heat transfer and solid mechanics.

The purpose of this paper is to investigate the strategies and algorithms for expedited design optimization of microwave and antenna structures in multi-objective setup.

Formulation of the multi-objective design problem-oriented toward execution of the population-based metaheuristic algorithm within the segmented search space is investigated. Described algorithmic framework exploits variable fidelity modeling, physics- and approximation-based representation of the structure and model correction techniques. The considered approach is suitable for handling various problems pertinent to the design of microwave and antenna structures. Numerical case studies are provided demonstrating the feasibility of the segmentation-based framework for the design of real-world structures in setups with two and three objectives.

Formulation of appropriate design problem enables identification of the search space region containing Pareto front, which can be further divided into a set of compartments characterized by small combined volume. Approximation model of each segment can be constructed using a small number of training samples and then optimized, at a negligible computational cost, using population-based metaheuristics. Introduction of segmentation mechanism to multi-objective design framework is important to facilitate low-cost optimization of many-parameter structures represented by numerically expensive computational models. Further reduction of the design cost can be achieved by enforcing equal-volumes of the search space segments.

The study summarizes recent advances in low-cost multi-objective design of microwave and antenna structures. The investigated techniques exceed capabilities of conventional design approaches involving direct evaluation of physics-based models for determination of trade-offs between the design objectives, particularly in terms of reliability and reduction of the computational cost. Studies on the scalability of segmentation mechanism indicate that computational benefits of the approach decrease with the number of search space segments.

The proposed design framework proved useful for the rapid multi-objective design of microwave and antenna structures characterized by complex and multi-parameter topologies, which is extremely challenging when using conventional methods driven by population-based metaheuristics algorithms. To the authors knowledge, this is the first work that summarizes segmentation-based approaches to multi-objective optimization of microwave and antenna components.

Modern food processing methods and the widespread ownership of both domestic and catering microwave ovens have permitted rapid growth in the production of a wide range of frozen and cook‐chill foods for retail and catering use.