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The purpose of this study is to investigate the possibility of dyeing polyester (PET) fabric with natural dye extracted from annatto seeds using high temperature dyeing method.

PET fabric was dyed with annatto extract by varying dyeing parameters (temperature, time, pH and dye concentration) to determine the optimum dyeing conditions. The influences of KAl(SO₄)₂, FeSO₄, gallnut mordants or a commercial UV absorber on colour yield and fastness properties were further studied.

Optimum results were obtained when the fabric was dyed at 130°C for 30 min in a dyebath containing 15 per cent (owf) annatto dye at pH 6. The dyed fabric had an orange shade and exhibited good to excellent wash, crock, perspiration fastness and fair light fastness. Further dyeing with mordants or UV absorber mostly resulted in lower colour yield and similar fastness properties.

Although the light fastness was slightly improved to moderate level for the sample with UV absorber, a noticeable colour staining on cotton portion of multi-fibre fabric occurred when subjected to standard washing test. Compared to C.I. Disperse Orange 73, the annatto dye exhibited comparable colour fastness but had inferior light fastness when dyed at approximately the same colour strength.

Natural colourants from annatto seeds can be used to dye PET fabric at high temperature without mordants, yielding deep orange shade and satisfactory fastness properties. This study provides a promising application to reduce the environmental impact of synthetic dyes.

The purpose of this study is to optimize single-bath dyeing process of wool and silk blend, to achieve uniform colour strength for both the fibre after the dyeing process. Due to different absorption characteristics of wool and silk, two-stage dyeing is preferred in the industry. If the fibres are dyed together, the wool fibre becomes darker and the silk fibre becomes lighter after the dyeing process. Solid dyeing effect can be achieved using a single-bath dyeing process.

The dye-acceptor sites in the wool fibre are first blocked using one commercial syntan Mesitol HWS. Then, the syntan-treated wool and silk fibres (80:20 blend ratios) are dyed with Telon Navy AMF dyes in the presence of sodium sulphate. To explore the influence of Syntan, sodium sulphate and the experimental conditions on the dyeing process and to optimize the process, central composite design (CCD) of four factors and three levels was tested.

The design process is optimized using four independent variables: Mesitol HWS concentration, sodium sulphate concentration, pH of dyebath and temperature of dyeing. Three levels of Mesitol HWS concentration (5, 10 and 15 per cent), sodium sulphate concentration (10, 20 and 30 per cent), pH (2.5, 4 and 5.5) and temperature of dyeing (70, 80 and 900°C) were selected for this study. These variables are optimized using response surface regression equation of the ratio of K/S wool and K/S silk. The predicted equation matched well with the experimental data.

This paper proposes the use of one-bath dyeing process of wool and silk blend fabric to reduce the dyeing time, process step and to save water.

This study aims to show the dyeing behaviour of polyester fabrics using four novel heterocyclic disperse dyes.

The four dyes were synthesized based on 5, 5'-(1, 4-phenylene) bis (1, 3, 4-thiadiazol-2-amine) as a diazonium compound. The UV/Vis absorption spectroscopic data of these disperse dyes while dyeing polyester fabrics were investigated. Following this, the dyeing properties of these dyes on polyester fabrics were investigated under acid condition.

The results showed that increasing the dyeing temperature from 80°C to 100°C led to an increase in dye uptake for all dyes, but further increases of the temperature to 130°C led to higher dye uptake for dye 3 as the dye exhaustion increased by about 50% from 55.9% to 91.4%.

This study is important as it introduces new dyes for the dyeing of polyethylene terephthalate (PET) fibres with colours that range from yellowish orange to bluish yellow and scarlet red and all with excellent brightness, levelness and depth of shade.

Based on clarifying the structural difference between jade fibre and general polyester fibre, this paper aims to study the dyeing properties and dyeing adsorption mechanism of jade fibre with disperse dye and cationic dye.

The chemical structure and microstructure of jade fibre were briefly explained comparing with ordinary polyester fibre. The dyeing rate curve and dyeing adsorption isotherm of disperse dyes and cationic dyes on jade fibre were, respectively, studied. The dyeing uptake, dyeing absorption mechanism, and the main dyeing process parameters were proposed.

Jade fibre can be dyed with cationic dye and disperse dye. The suitable exhaust dyeing process is 110°C and 40 minutes for disperse dye, 100°C and 60 minutes for cationic dye. The dyeing uptake on jade fibre with both disperse dyes or cationic dyes is much higher than that on general polyester fibre and acrylic fibre, and the dyeing adsorption mechanism belongs to the combination of Langmuir and Nernst adsorption for disperse dyes and Langmuir adsorption for cationic dyes. Comparing with ordinary polyester fibre, jade fibre has the advantage of low temperature dyeing and reduced effluent, as is significant to energy-saving and emission reduction.

Jade fibre is a new type of modified polyester fibre with the function of health protection and energy conservation. There are little technical data in the literature at present about the dyeing property of jade fibre.

Natural dyes are mostly used for dyeing of natural fibre textiles to improve their eco-friendly features. For successful commercial use of natural dyes, the appropriate and standardized dyeing techniques need to be adopted. Appropriate scientific techniques or procedures need to be derived from scientific studies on dyeing methods, dyeing process variables, dyeing kinetics and compatibility of selective natural dyes with minimal use of hazardous chemicals.

In the present study, different enzymes (protease, amylase, xylanase, pectinase, phytase) were used efficiently with Rubia dye by using simultaneous and two-step processes; both the processes were developed with an aim for conservation of time and energy, for the ease of industrial use. The highlights of the study are twofold: eco-friendly natural dyeing by using enzyme replacing metal mordant and room temperature dyeing, which is a completely new concept.

Experiments showed that enzymatic treatment can give good colour strength to silk fabric using Rubia as a dye source and has good potential for commercial dyeing. It is a non-toxic dye. Use of enzymes were a deliberate attempt to avoid metal mordanting in silk dyeing, as it would make textile dyeing eco-friendlier. The order of reactivity of enzymes in one-step process was found to be protease > phytase > xylanase > amylase > pectinase. Similarly, for two-step dyeing process, the order of reactivity of enzymes observed was protease > amylase > xylanase = pectinase > phytase. Protease enzyme was the best option in both the cases. Overall, it can be concluded that in the case of enzymatic treatment, the two-step process was better in terms of larger K/S values, colour coordinate values and dye adherence.

A new domain of room temperature dyeing technique has been introduced.

In the present study, different enzymes (protease, amylase, xylanase, pectinase, phytase) were used efficiently with Rubia dye by using simultaneous and two-step processes; both the processes were developed with an aim for conservation of time and energy, for the ease of industrial use. The highlights of the research are twofold: eco-friendly natural dyeing by using enzyme replacing metal mordant and room temperature dyeing, which is a completely new concept. Overall, the ease of use for industrial application. Rubia dye from Sri Lanka has been used in conjunction with different enzymes to show that metal mordanting can be easily replaced by the use of eco-friendly and biodegradable enzymes. The most attractive feature of this study is the low-temperature dyeing at 30-40°C. For any dyeing house, this process can be easily adapted on jigger, winch or even in continuous padding machine. Good fastness properties and dye adherence have been the other highlights of this study.

The purpose of this paper is to improve the dyeing effect of fast-growing fir wood dyed with reactive dyes.

In this study, five factors including temperature, the dosage of dye accelerator, dyeing time, the dosage of fixing agent and fixing time were investigated. Then, the color difference and light resistance of the wood surface after dyeing were used as the evaluation indicators; the best dyeing process under the two indicators was obtained through the range analysis. Finally, the two indicators were considered comprehensively, and the fuzzy comprehensive evaluation method was used to obtain the best dyeing process under the comprehensive indicators.

The results show that when the comprehensive index was used as the evaluation index, the optimal dyeing process for reactive red X-3B dyeing fast-growing fir veneer was that the dyeing temperature was 65°C; the amount of dye accelerator was 25 g L⁻¹; the dyeing time was 2 h; the amount of fixing agent was 15 g L⁻¹; and the fixing time was 35 min.

The technique of wood dyeing is an important method to increase the value of wood products. When using different kinds of dyes or dyeing substrates for wood dyeing, the dyeing process is different. This study determined the best process for reactive dye dyeing of fast-growing fir veneer and provided a solution for improving the value of fast-growing fir wood.

Finding blue colorants from natural sources is extremely difficult and, usually, the anthocyanin compounds are used for producing the blue color. This study aims to apply the Red Cabbage as a natural colorant to obtain different colors on wool yarn, as well as specify the optimum dyeing condition by response surface methodology for obtaining a blue color.

The effect of dyeing process parameters such as mordant concentration, dyeing time, pH of dyeing bath and dyeing temperature examined in the color characteristics of the dyed wool samples.

The obtained results indicated that the diverse colors achieve by varying the dyeing process parameters, which is in the range of 26° up to 271°. The non-mordanted dyed wool samples showed a red and red brownish color (Hue angle = 26° up to 70°), and the mordanted dyed wool samples showed a blue and blue-greenish color (Hue angle = 230° up to 271°). The obtained blue color with the optimized dyeing condition presented a considerable good wash and lightfastness.

This study provides a promising application of Red Cabbage as a natural colorant for obtaining different colors by varying the dyeing process parameters such as pH and stannous ion concentrations. The stannous ions yielded a co-pigmentation and presented a blue color on wool fibers, which is extremely difficult to obtain with natural colorant.

This study aims to synthesize new disperse dyes based on novel pyrazolyl quinolinone derivatives EQ1 and EQ2 and evaluate their characteristics after dyeing them on a polyester fabric.

New dispersed dyes based on pyrazolyl quinolinone derivatives were prepared and confirmed by different analyses, such as infrared spectroscopy, elemental microanalysis and nuclear magnetic resonance spectroscopy. They were dyed on a polyester fabric. The characteristics of dyed polyester were determined by color measurements such as a*, b*, L*, C*, E, Ho, R% and color strength. The electronic structures of EQ1 and EQ2 in gaseous state were investigated using density functional theory/B3LYP/6-311++G (d, p) level of theory.

The suitability of the prepared dyestuffs for dyeing on polyester fabrics has been investigated. The study was concerned with comparing the contrasting depth of shade and levelness. The study was concerned mainly with dye uptake and color measurements at two different temperatures. The results showed that the exhaustion values of dyes inside the polyester at 130°C were higher than those obtained at conventional dyeing temperature (100°C). The exhaustion values of EQ2 were greater than those of EQ1 at 130°C with 2.2%, while the brightness of EQ2 was higher than that of EQ1 at the two investigated temperatures. The results of molecular orbital calculations show that the studied compounds are planar. In addition, the ionization potential of EQ1 was lower than that of EQ2. The results of the theoretical study helped in understanding the dyeing behavior of the investigated azo dyes.

The prepared disperse dyes based on pyrazolyl quinolinone derivatives could be used in textile dyeing of polyester on an industrial scale.

This paper aims to investigate the feasibility of developing an eco-friendly dyeing process for a regenerated polyester fiber (polytrimethylene terephthalate) using a natural dye (Lac) and bio-mordant.

The effects of temperature, time, initial pH of dye bath, material to liquor ratio and mordant concentration on color strength of polytrimethylene terephthalate fiber dyed with Lac were examined. The results were compared using three bio-mordant (catechu, myrobalan and pomegranate) and three inorganic mordant (alum, ferrous sulfate and stannous chloride). Single replicate of 25-design methodology was used to identify three significant factors affecting color strength, and optimization was done using response surface methodology based on 2³-central composite rotatable design.

Color strength achieved using catechu as a bio-mordant was close to that with ferrous sulfate and higher than with stannous chloride. Temperature, initial pH and mordant concentration were identified as significant factors affecting color strength of dyed fiber with catechu. Optimization revealed temperature of 133OC, initial pH of 6 and bio-mordant (Catechu) concentration of 10 per cent to be the optimal conditions for dyeing, with K/S value of 4.55.

The study revealed the possibility of satisfactory dyeing of regenerated polyester fibers with natural dyes, replacing disperse dyes. The comparison of color strength achieved indicated the possibility of replacing inorganic mordant with bio-mordant in such dyeing process. The dyeing process could thus be made more eco-friendly by removal of toxic chemicals from effluents.

The purpose of this paper is to develop an environmentally friendly dyeing process using brown pigment from chestnut shells (BPFCS). This material is obtained from foodstuff residues and can make a significant contribution to reusing a reproducible biomass resource, economizing petroleum, avoiding water pollution and protecting human health.

The brown pigment is extracted from the raw material and purified with solvents containing 30 and 100 per cent EtOH. It is then used to dye flax fabric in aqueous solution with added NaCl as a dye accelerator. The effects of dyeing conditions and fastness are investigated. The pigment, and the pristine and dyed fabrics are analysed by Fourier‐transform infrared spectroscopy (FT‐IR) and the fabric samples are observed using a scanning electron microscope (SEM). Fastness to washing, rubbing and light are also measured.

BPFCS show promising dyeability on cellulosic fibers. White flax fabric is successfully dyed with the pigment to a yellow‐brown colour. The base dyeing conditions are as follows: pigment concentration 16 g/l, NaCl concentration 10 g/l, liquor ratio 10:1, temperature 95°C, dyeing time 40 min. The dyed fabrics have lower fastness to washing and higher fastness to rubbing and light. A total of 4 per cent Al³⁺ or Fe²⁺ treatment of dyed fabric can improve fastness to washing, but decrease fastness to rubbing. The yellowish‐brown samples are transformed to brown or dark‐green after Al³⁺ or Fe²⁺ treatment, respectively. The pigment is a mixture with abundant hydroxyl groups.

The studies of dyeing conditions and fastness are carried out in detail as BPFCS used as a dye. However, a qualitative analysis of the pigment could not be performed due to the difficulty of separating the mixture. The BPFCS used in this paper can dye cellulosic fiber and can also be used to dye other fibers such as silk, wool and PET. Dyeing conditions for these other fibers need to be investigated.

BPFCS may play an important role in the dyeing industries because of its good dyeability, lack of toxicity and resistance to water, rubbing and light. The present work offers an environmentally friendly dye and a simple dyeing method.

At present, no report exists in the literature of work on dyeing flax fabric with BPFCS. This paper represents a preliminary study to determine the relationships of dyeing conditions to fastness and the role of mordant. BPFCS appears to be a new and practically useful natural dye.