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Article
Publication date: 7 February 2022

Beata Synkiewicz-Musialska, Dorota Szwagierczak, Jan Kulawik and Elżbieta Czerwińska

This paper aims to report on fabrication procedure and presents microstructure and dielectric behaviour of LiZn0.92Cu0.08PO4 ceramic material with Li2CO3 as a sintering aid.

Abstract

Purpose

This paper aims to report on fabrication procedure and presents microstructure and dielectric behaviour of LiZn0.92Cu0.08PO4 ceramic material with Li2CO3 as a sintering aid.

Design/methodology/approach

Substrates based on LiZn0.92Cu0.08PO4 with Li2CO3 addition were prepared via solid-state synthesis, doping, milling, pressing and sintering. Characterization of the composition, microstructure and dielectric properties was performed using X-ray diffractometry, energy dispersive spectroscopy, scanning electron microscopy, impedance spectroscopy in the 100 Hz to 2 MHz range and time-domain spectroscopy in the 0.1–3 THz range.

Findings

Doped LiZnPO4 ceramic, which exhibits a low dielectric constant of 5.9 at 1 THz and low sintering temperature of 800 °C, suitable for low temperature co-fired ceramics (LTCC) technology, was successfully prepared. However, further studies are needed to lower dielectric losses by optimising the doping level, synthesis and sintering conditions.

Originality/value

Search for new low dielectric constant materials applicable in LTCC technology and optimization of processing are essential tasks for developing modern microwave circuits. The dielectric characterization of doped LiZnPO4 ceramic in the terahertz range, which was performed for the first time, is crucial for potential millimetre-wave applications of this substrate material.

Details

Microelectronics International, vol. 39 no. 4
Type: Research Article
ISSN: 1356-5362

Keywords

Article
Publication date: 7 May 2020

Beata Synkiewicz-Musialska

The purpose of this paper is to report on fabrication procedure and present microstructure and dielectric behavior of willemite ceramic material with addition of 5% Li2CO3 as a…

Abstract

Purpose

The purpose of this paper is to report on fabrication procedure and present microstructure and dielectric behavior of willemite ceramic material with addition of 5% Li2CO3 as a sintering aid.

Design/methodology/approach

The samples were fabricated by ball milling of the ceramic powders, preparation of granulate and pressing and co-firing using temperature profile based on heating microscope observation. The dielectric properties of the material were measured by impedance spectroscopy (Hz-MHz), transmission method (GHz) and time domain spectroscopy (THz). The composition and microstructure of the material were investigated using X-ray diffraction, scanning electron microscopy and energy-dispersive spectroscopy analysis. Ceramic powder was used to fabricate a green tape and low temperature co-fired ceramics (LTCC) multilayer structures, which in the next steps of the research were examined at the angle of cooperation with conductive pastes, strength and geometric repeatability.

Findings

The fabricated material showed low sintering temperature (920°C–960°C), low dielectric constant 6.2–6.34 and low dissipation factor at the level of 0.004–0.007. As LTCC material, willemite with 5% Li2CO3 addition showed good compatibility with AgPd conductive paste.

Originality/value

Search for new materials with low dielectric constant, applicable in LTCC technology, and development of their fabrication procedure are important tasks for the progress in modern microwave circuits.

Details

Microelectronics International, vol. 37 no. 2
Type: Research Article
ISSN: 1356-5362

Keywords

Article
Publication date: 1 March 2003

Robert W. Bogue

Discusses recent progress in technology based on electromagnetic radiation at terahertz frequencies. Considers recent corporate activities and describes technological developments…

Abstract

Discusses recent progress in technology based on electromagnetic radiation at terahertz frequencies. Considers recent corporate activities and describes technological developments with applications in the physical and life sciences.

Details

Sensor Review, vol. 23 no. 1
Type: Research Article
ISSN: 0260-2288

Keywords

Article
Publication date: 3 December 2018

Magdalena Mieloszyk, Katarzyna Majewska and Wieslaw Ostachowicz

The purpose of this paper is to discuss the application of THz spectroscopy for the inspection and evaluation of the internal structure of complex samples with honeycomb fillers.

Abstract

Purpose

The purpose of this paper is to discuss the application of THz spectroscopy for the inspection and evaluation of the internal structure of complex samples with honeycomb fillers.

Design/methodology/approach

Three complex samples with honeycomb fillers are investigated using THz spectrometer in order to determine the applicability of chosen non-destructive method for the analysis of internal structure of structural components. The first analysed sample has aluminium honeycomb filler with some cells filled with water. The aim of the analysis is to distinguish empty and full cells. The other two sandwich samples are made of different non-metallic components and for them the possibility of THz spectroscopy application is analysed.

Findings

The empty and full cells in metal honeycomb filler were easily distinguished due to different absorption coefficients of electromagnetic waves in THz range for air and water. It was especially visible for frequency domain. The THz spectroscopy was able to inspect the non-metallic samples internal structures and distinguish skins (with layers), honeycomb fillers and adhesive layers between them. It was also possible to detect, localise and determine the size of a local damage of honeycomb walls due to impact influence.

Originality/value

The present study is an original research work. There are very limited literature papers which present analyses of internal structures of sandwich elements using THz spectroscopy and investigate utility of the method for mechanical damage and contamination (water) detection and localisation.

Details

International Journal of Structural Integrity, vol. 9 no. 6
Type: Research Article
ISSN: 1757-9864

Keywords

Article
Publication date: 8 January 2018

Robert Bogue

This paper aims to provide a technical insight into a selection of recent developments and applications involving terahertz sensing technology.

1178

Abstract

Purpose

This paper aims to provide a technical insight into a selection of recent developments and applications involving terahertz sensing technology.

Design/methodology/approach

Following an introduction, the first part of this paper considers a selection of research activities involving terahertz radiation sources and detectors. The second part seeks to illustrate how the technology is exerting a commercial impact and discusses a number of product developments and applications.

Findings

Terahertz sensing is a rapidly developing field and a strong body of research seeks to develop sources and detectors with enhanced features which often exploit novel materials, phenomena and technologies. Commercialisation is gathering pace, and a growing number of companies are producing terahertz sensing and imaging products which are finding a diversity of applications.

Originality/value

This provides details of recent research, product developments and applications involving terahertz sensing technology.

Details

Sensor Review, vol. 38 no. 2
Type: Research Article
ISSN: 0260-2288

Keywords

Article
Publication date: 12 June 2017

Fabienne Touchard, Michel Boustie, Laurence Chocinski-Arnault, Pedro Pascual González, Laurent Berthe, Davi de Vasconcellos, Luigi Sorrentino, Pawel Malinowski and Wieslaw Ostachowicz

The purpose of this paper is to study the damage induced in “green” and synthetic composites under impact loading.

Abstract

Purpose

The purpose of this paper is to study the damage induced in “green” and synthetic composites under impact loading.

Design/methodology/approach

The study was focussed on epoxy-based composites reinforced with woven hemp or glass fibres. Six assessment techniques were employed in order to analyse and compare impact damages: eye observation, back face relief, terahertz spectroscopy, laser vibrometry, x-ray micro-tomography and microscopic observations.

Findings

Different damage detection thresholds for each material and technique were obtained. Damage induced by mechanical and laser impacts showed relevant differences, but the damage mechanisms are similar in both types of impact: matrix cracks, fibre failure, debonding at the fibres/matrix interface and delamination. Damage shape on back surfaces is similar after mechanical or laser impacts, but differences were detected inside samples.

Originality/value

The combination of these six diagnoses provides complementary information on the damage induced by mechanical or laser impacts in the studied green and synthetic composites.

Details

International Journal of Structural Integrity, vol. 8 no. 3
Type: Research Article
ISSN: 1757-9864

Keywords

Article
Publication date: 4 July 2016

Przemyslaw Lopato

– The purpose of this paper is to present a system for automatic recognition of defects detected in non-conductive polymer composites using pulsed terahertz imaging.

Abstract

Purpose

The purpose of this paper is to present a system for automatic recognition of defects detected in non-conductive polymer composites using pulsed terahertz imaging.

Design/methodology/approach

On the beginning, non-destructive evaluation of composites using electromagnetic waves in terahertz frequency is shortly introduced. Next automatic defects recognition (ADR) algorithm is proposed, focussing on new features calculation. Dimensionality of features space is reduced by using principal component analysis. Finally, results of basalt fiber reinforced composite materials inspection and identification using artificial neural networks is presented and discussed.

Findings

It is possible to develop ADR system for non-destructive evaluation of dielectric materials using pulsed terahertz technique. New set of features in time and frequency domains is proposed and verified.

Originality/value

ADR in non-destructive testing is utilized in case of digital radiography and ultrasonic testing. Terahertz inspection with pulsed excitation is reported as a source of many useful information about the internal structure of the dielectric material. Up to now ADR based on terahertz non-destructive evaluation systems was not utilized.

Details

COMPEL: The International Journal for Computation and Mathematics in Electrical and Electronic Engineering, vol. 35 no. 4
Type: Research Article
ISSN: 0332-1649

Keywords

Article
Publication date: 3 May 2013

Przemyslaw Lopato, Tomasz Chady, Ryszard Sikora, Stanislaw Gratkowski and Marcin Ziolkowski

The purpose of this paper is to describe the full‐wave modelling of pulsed terahertz systems utilized in non‐destructive testing.

Abstract

Purpose

The purpose of this paper is to describe the full‐wave modelling of pulsed terahertz systems utilized in non‐destructive testing.

Design/methodology/approach

At the outset, some basic information on the terahertz NDT are outlined and then, general remarks on its numerical modelling are presented. Frequency domain FEM and time domain FDTD analysis is carried out. Finally comparison of computed and measured signals is shown in order to prove numerical analysis correctness.

Findings

It is possible to model in a relatively simple way a terahertz system for nondestructive evaluation of dielectric materials. In contrast to other published work, the entire measuring setup is modelled, including photoconductive antenna with hemispherical lens, focusing lens and evaluated material with exemplary defect.

Originality/value

This paper gives a description of the terahertz non‐destructive testing system with comparison of simulated and measured results.

Details

COMPEL - The international journal for computation and mathematics in electrical and electronic engineering, vol. 32 no. 3
Type: Research Article
ISSN: 0332-1649

Keywords

Article
Publication date: 3 December 2018

Katarzyna Majewska, Magdalena Mieloszyk and Wieslaw Ostachowicz

The purpose of this paper is to study if it is possible applying infrared thermography (both vibro and pulsed) to detect and localise material discontinuities as well as to find…

Abstract

Purpose

The purpose of this paper is to study if it is possible applying infrared thermography (both vibro and pulsed) to detect and localise material discontinuities as well as to find the place where the inclusion was introduced.

Design/methodology/approach

The experimental investigation is performed on samples manufactured during infusion process. The measurements were performed on three four-layered rectangular composite samples with discontinuities. The discontinuities introduced in the samples were as follow: all three samples between first and second layer counting form the bottom two optical fibres (OFs) were embedded and additionally: sample no. 1 – one of the OF was broken, sample no. 2 – the drop of water was introduced, and sample no. 3 – the little amount of dust was introduced.

Findings

For some discontinuities, the vibrothermography is excellent tool (placement of broken OF, drop of water), for same is not sufficient (healthy OFs or dust). For dust, the pulsed thermography seems to be the required tool. Different approaches (vibrothermography and pulsed thermography) for the same sample will confirm that for same defects vibrothermograpy is better and for some pulsed thermography – complex combination of different thermography approaches is needed to have complex response about sample structural condition.

Originality/value

The presented paper is an original research work. There are very limited literature papers applying both vibro and pulsed thermography for one problem. The assessment of different discontinuities (inclusions) and detailed analysis is presented.

Details

International Journal of Structural Integrity, vol. 9 no. 6
Type: Research Article
ISSN: 1757-9864

Keywords

Article
Publication date: 12 July 2011

Przemysław Łopato, Tomasz Chady and Ryszard Sikora

The purpose of this paper is to present capabilities of terahertz imaging technology in case of various composite materials and to propose a new defect detection algorithm.

Abstract

Purpose

The purpose of this paper is to present capabilities of terahertz imaging technology in case of various composite materials and to propose a new defect detection algorithm.

Design/methodology/approach

This paper first discusses an applicability of the terahertz technique in composite materials inspection. It then describes source of terahertz radiation (photoconductive antenna) and general structure of terahertz time domain imaging system. Next the terahertz imaging results of composite anticorrosion coating, glass‐ and carbon‐fiber‐reinforced laminates are presented. Then the signal processing and identification scheme based on time domain A‐scan signal equalization and C‐scan thresholding is presented. Data processed in this way are parameterized and defect identification database is prepared. The proposed procedure is verified using the exemplary inspection results of glass‐fiber laminate delamination. Finally, some comparison of terahertz time domain inspection with low energy digital radiography is presented.

Findings

This paper shows terahertz imaging as a well‐suited technique for composite structures inspection. The terahertz imaging results of composite anticorrosion coating, glass‐ and carbon‐fiber‐reinforced laminates are presented. An application of proposed signal processing algorithm enables accurate defects detection and effective data collection for identification database purpose.

Originality/value

The paper provides an insight into the potential of terahertz imaging of various composite structures. Proposed signal processing and defects detection scheme is applicable to wide range of composite structures.

Details

COMPEL - The international journal for computation and mathematics in electrical and electronic engineering, vol. 30 no. 4
Type: Research Article
ISSN: 0332-1649

Keywords

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