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The aim of this paper is to investigate microwave Ku band absorbance, complex permittivity, and permeability of SrFe12O19 thick films by a simple and novel waveguide technique.
Abstract
Purpose
The aim of this paper is to investigate microwave Ku band absorbance, complex permittivity, and permeability of SrFe12O19 thick films by a simple and novel waveguide technique.
Design/methodology/approach
The glass frit free or fritless strontium hexaferrite thick films were formulated on alumina by screen printing technique from the powder synthesized by chemical co precipitation method for pH 11 adjusted during the reaction. The 13‐18 GHz frequency band microwave absorbance of the SrFe12O19 thick films by a simple waveguide method. The complex permittivity and permeability of strontium hexaferrite thick films was measured by voltage standing wave ratio technique.
Findings
SrFe12O19 thick films show high ∼80 percent absorbance in the whole 13‐18 GHz frequency band. The thickness dependant microwave properties of strontium hexaferrite thick films were observed. The real permittivity ε′ lies in between eight and 35 with the variation in thickness of the thick film SrFe12O19. The real microwave permeability μ′ of strontium hexaferrite thick films lies in the range 1.12‐6.41. The resonance type behavior was observed at frequency 14.3 GHz. The SrFe12O19 thick film of thickness 30 μm could be a wide band (∼5,000 MHz) absorber with absorbance ∼87 percent for the whole 13‐18 GHz frequency band.
Originality/value
The complex permeability of strontium hexaferrite thick films was measured by simple novel waveguide method. The high absorbance (∼87 percent) of thick film SrFe12O19 over a broad band ∼5,000 MHz will be useful in achieving RAM coatings required for 13‐18 GHz frequency band.
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– This paper aims to study the structural, electrical and microwave properties of (Sr0.6Ca0.4) (CoyMn1−y) O3 (0.2 ≤ y ≤ 1.0) thick-film ceramics.
Abstract
Purpose
This paper aims to study the structural, electrical and microwave properties of (Sr0.6Ca0.4) (CoyMn1−y) O3 (0.2 ≤ y ≤ 1.0) thick-film ceramics.
Design/methodology/approach
The thick films of (Sr0.6Ca0.4) (CoyMn1−y) O3 (0.2 ≤ y ≤ 1.0) on the alumina substrate have been delineated using screen printing technique. The structural analysis was carried out using an X-ray diffraction method and scanning electron microscopy. The direct current (DC) electrical resistivity is measured using a two-probe method. Microwave absorption was studied in the 8-18 GHz frequency range by using the Waveguide Reflectometer Method. The permittivity and permeability in the 8-18 GHz frequency range were measured by using Voltage Standing Wave Ratio slotted section method.
Findings
The thick films have orthorhombic perovskite structure with dominant (020) plane. By using first-principle calculation method, theoretical and experimental lattice parameter and cell volume of (Sr0.6Ca0.4) (CoyMn1−y) O3 are matched with each other. The cobalt content changes the morphology from plates to needles. The DC electrical resistivity increases with increase in Co content and decreases with increase in temperature. (Sr0.6Ca0.4) (CoyMn1−y) O3 thick film shows 75 per cent microwave absorption both in the X band and Ku band. The microwave permittivity and permeability decreases with increase in frequency and Co content.
Originality/value
Structural, electrical and microwave properties of (Sr0.6Ca0.4) (CoyMn1−y) O3 (0.2 ≤ y ≤ 1.0). Thick film ceramics on alumina substrate is reported for the first time.
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S.N. Mathad, R.N. Jadhav and Vijaya Puri
The purpose of this paper was to determine the complex permittivity of bismuth strontium manganites (Bi1−xSrxMnO3) in the 8‐12 GHz range by using perturbation of Ag thick film…
Abstract
Purpose
The purpose of this paper was to determine the complex permittivity of bismuth strontium manganites (Bi1−xSrxMnO3) in the 8‐12 GHz range by using perturbation of Ag thick film microstrip ring resonator (MSRR) due to superstrate of both bulk and thick film.
Design/methodology/approach
The BSM ceramics were synthesized by simple low cost solid state reaction method and their fritless thick films were fabricated by screen printing technique on alumina substrate. A comparison has been made between the X band response of Ag thick film microstrip ring resonator due to perturbation of bulk and thick film Bi1−xSrxMnO3 ceramic.
Findings
The bulk and thick film superstrate decreases the resonance frequency of MSRR. In this technique even minor change in the properties of superstrate material changes the MSRR response. Variation of strontium content also influences microwave conductivity and penetration depth of bulk and thick films.
Originality/value
The microwave complex permittivity decreases with increase in Sr content in bismuth manganite and it is higher for bulk as compared to its thick films. The superstrate on Ag thick film microstrip ring resonator is an efficient tool capable of detecting the composition dependent changes in microwave properties of ceramic bulk and thick films.
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The purpose of this paper is to describe the use of copper‐substituted nickel manganite thick film and bulk ceramic superstrate on Ag thick film microstrip straight resonator…
Abstract
Purpose
The purpose of this paper is to describe the use of copper‐substituted nickel manganite thick film and bulk ceramic superstrate on Ag thick film microstrip straight resonator (MSR), to modify its response and measure complex permittivity as a function of copper.
Design/methodology/approach
The glass frit free (fritless) copper‐substituted nickel manganite thick films were formulated on alumina substrate by screen printing technique from the powder synthesized by oxalic precursor method. A comparison has been made between the X band response of Ag thick film MSR due to perturbation of bulk and thick film Ni(1−x)CuxMn2O4 (0≤x≤1) ceramic. The shift has been used to measure the permittivity of the ceramic. The dielectric constants obtained by superstrate technique on Ag thick film microstrip component are comparable to those obtained from theoretical calculations.
Findings
The resonance frequency of MSR shifts towards lower frequency due to the presence of Ni(1−x)CuxMn2O4 (0≤x≤1) ceramic as superstrate. The dielectric constant of bulk and thick film match well with the theoretical values. The dielectric constant increases with copper concentration and shows reduction of power gain of MSR. The peak output (power gain) of MSR due to thick film NiMn2O4 increases by 10.19 per cent with decrease in bandwidth and increase in the quality factor with copper concentration.
Originality/value
The superstrate on Ag thick film straight resonator is an efficient tool capable of detecting the composition‐dependent changes in microwave properties of ceramic thick films. These Ni(1−x)CuxMn2O4 ceramic being thermistor materials apart from modifying the response can also be used as power sensors providing cost‐effective miniaturization.
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A. Vivek, K. Shambavi and Zachariah C. Alex
This paper aims to focus on research work related to metamaterial-based sensors for material characterization that have been developed for past ten years. A decade of research on…
Abstract
Purpose
This paper aims to focus on research work related to metamaterial-based sensors for material characterization that have been developed for past ten years. A decade of research on metamaterial for sensing application has led to the advancement of compact and improved sensors.
Design/methodology/approach
In this study, relevant research papers on metamaterial sensors for material characterization published in reputed journals during the period 2007-2018 were reviewed, particularly focusing on shape, size and nature of materials characterized. Each sensor with its design and performance parameters have been summarized and discussed here.
Findings
As metamaterial structures are excited by electromagnetic wave interaction, sensing application throughout electromagnetic spectrum is possible. Recent advancement in fabrication techniques and improvement in metamaterial structures have led to the development of compact, label free and reversible sensors with high sensitivity.
Originality/value
The paper provides useful information on the development of metamaterial sensors for material characterization.
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N. Patil, N.B. Velhal, R. Pawar and Vijaya Puri
The purpose of this article is to study the effect of ferrite content on electric, magnetic and microwave properties of screen-printed y(Ni0.4Co0.2Cd0.4Fe2O4) + (1 …
Abstract
Purpose
The purpose of this article is to study the effect of ferrite content on electric, magnetic and microwave properties of screen-printed y(Ni0.4Co0.2Cd0.4Fe2O4) + (1 − y)Pb(Zr0.52Ti0.48)O3 (y = 0.0, 0.15, 0.30, 0.45, 1.0) thick films on alumina.
Design/methodology/approach
Thick films of ferrite–ferroelectric composite on alumina substrate have been delineated using screen printing technique. The structural analysis was carried out using X-ray diffraction method and scanning electron microscopy. The DC electrical resistivity was measured using the two-probe method. The magnetic measurement was carried out using a vibrating sample magnetometer. Microwave absorption was studied in the 8-18 GHz frequency range by using the vector network analyzer (N5230A). The permittivity in the 8-18 GHz frequency range was measured by using voltage standing wave ratio slotted section method.
Findings
The formation of two individual ferrite–ferroelectric phases in composite thick films was confirmed by the X-ray diffraction patterns. The scanning electron microscope morphologies show the growth of cobalt-substituted nickel cadmium ferrite grains which are well dispersed in lead zirconium titanate matrix. The DC electrical resistivity increases with increase in ferrite content and decreases with increase in temperature. The present ferrite shows ferromagnetic nature and it increases saturation magnetization and coercivity of the composite thick films. Tuning properties are observed in the Ku-band and broadband X-band microwave absorption is observed in the composite thick films. The imaginary part of permittivity increases with an increase in ferrite content, which increases microwave absorption. The real part of microwave permittivity varied from 17 to around 22 with an increase in ferrite content and it decreases with frequency. The microwave conductivity, which increases with an increase in ferrite content, reveals the loss of polaron conduction, which supports the dielectric loss in the microwave region.
Originality/value
Electric, magnetic and microwave properties of screen-printed y(Ni0.4Co0.2Cd0.4Fe2O4) + (1 − y)Pb(Zr0.52Ti0.48)O3 (y = 0.0, 0.15, 0.30, 0.45, 1.0) composite thick films on alumina substrate is reported for the first time.
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P.B. Kashid, D.C. Kulkarni, V.G. Surve and Vijaya Puri
The purpose of this paper is to study thickness dependent variation in microwave properties of the MgxMn(0.9−x)Al0.1Zn0.8Fe1.2O4 (x=0.8, 0.9) thick films and enhancement of power…
Abstract
Purpose
The purpose of this paper is to study thickness dependent variation in microwave properties of the MgxMn(0.9−x)Al0.1Zn0.8Fe1.2O4 (x=0.8, 0.9) thick films and enhancement of power efficiency of Ag thick film EMC patch antenna.
Design/methodology/approach
X‐band microwave properties of the MgxMn(0.9−x)Al0.1Zn0.8Fe1.2O4 (x=0.8, 0.9) thick films were measured by superstrate technique using Ag thick film EMC patch antenna as the resonant element. The complex permittivity and permeability of these thick films were also measured by this technique. The microwave response of the EMC patch, complex permeability and permittivity of Mg0.8Mn0.1Al0.1Zn0.8Fe1.2O4 and Mg0.9Al0.1Zn0.8Fe1.2O4 thick films and their thickness dependency were investigated.
Findings
The XRD patterns reveal the cubic spinel crystal system was obtained for both compositions. The crystallite size obtained was 134.68 nm for Mg0.8Mn0.1Al0.1Zn0.8Fe1.2O4 and 155.99 nm for Mg0.9Al0.1Zn0.8Fe1.2O4 The superstrate technique has been used successfully to evaluate the complex permittivity and permeability of the ferrite thick films in the X band. The EMC patch also show thickness and composition dependent frequency agility and enhancement of power efficiency.
Originality/value
The complex permeability of MgxMn(0.9−x)Al0.1Zn0.8Fe1.2O4 (x=0.8, 0.9) thick films measured by superstrate technique is reported in this paper. The superstrate of MgxMn(0.9−x)Al0.1Zn0.8Fe1.2O4 (x=0.8, 0.9) thick films makes the Ag thick film EMC patch antenna frequency agile and power amplification is obtained.
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The purpose of this paper is to investigate microwave reflection, transmission, and complex permittivity of p‐toluene‐2‐sulfonic acid doped conducting polypyrrole coated…
Abstract
Purpose
The purpose of this paper is to investigate microwave reflection, transmission, and complex permittivity of p‐toluene‐2‐sulfonic acid doped conducting polypyrrole coated nylon‐lycra textiles in the 1‐18 GHz frequency with a view to potential applications in the interaction of electromagnetic radiation with such coated fabrics.
Design/methodology/approach
The chemical polymerization of pyrrole is achieved by an oxidant, ferric chloride and doped with p‐toluene sulfonic acid (pTSA) to enhance the conductivity and improve stability. Permittivity of the conducting textile substrates is performed using a free space transmission method accompanied by a mathematical diffraction reduction method.
Findings
The real part of permittivity increases with polymerization time and dopant concentration, reaching a plateau at certain dopant concentration and polymerization time. The imaginary part of permittivity shows a frequency dependent change throughout the test range. All the samples have higher values of absorption than reflection. The total electromagnetic shielding effectiveness exceeds 80 percent for the highly pTSA doped samples coated for 3 h.
Originality/value
A non‐contact, non‐destructive free space method thin flexible specimens to be tested with high accuracy across large frequency range. The non‐destructive nature of the experiments enables investigation of the stability of the microwave transmission, reflection, absorption and complex permittivity values. Moreover, mathematical removal of the diffraction enables higher accuracy.
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The purpose of this paper is to predict permittivity of leafy vegetation using overlay technique.
Abstract
Purpose
The purpose of this paper is to predict permittivity of leafy vegetation using overlay technique.
Design/methodology/approach
The paper studies X band moisture dependent microwave permittivity of the stem and leaf of Ficus Bengalensis using overlay on Ag thick film microstripline. The perturbation obtained in the transmission and reflectance of the thick film microstripline due to the leafy vegetation overlay has been used to obtain the permittivity.
Findings
The paper finds that the permittivities obtained are in the range expected of leafy vegetation with moisture. Only the amplitude data have been used here. As the moisture content decreases, the dielectric constant and dielectric loss decrease. The return loss characteristics show interesting frequency dependent behaviour due to both stem and leaf overlay.
Originality/value
The paper is original in that a non‐resonant microstrip component has been used for the first time for such studies. The thick film component along with overlay can be a cost‐effective dielectric sensor especially for biomaterials, since any size and shape of the overlay can be used.
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Satish Geeri and Aditya Kolakoti
The purpose of the present work is to fabricate composite with strong absorbing nature and with more strength. The usage of wireless communication is increasing day by day…
Abstract
Purpose
The purpose of the present work is to fabricate composite with strong absorbing nature and with more strength. The usage of wireless communication is increasing day by day, electromagnetic absorbing material is required to reduce this pollution. In the present experimental investigation, composites were fabricated for zero and 45° fiber orientation and as a filler material of Multiwall Carbon Nanotubes (MWCNTs) for the proposed percentage in the composites. Microwave absorbing properties were investigated for both perfect electric conductor (PEC)-backed composites and without PEC-backed composites.
Design/methodology/approach
The electromagnetic absorbing performance was analyzed based on complex permeability, complex permittivity, dielectric tangent and magnetic tangent losses. The experimentation was done by Vector Network Analyzer in the frequency range of 8.2 to 12.4 GHz by X-band. The surface morphological study was done. The mechanical and thermal properties are also investigated for these composites.
Findings
By investigating the experimental values, the induced percentage of MWCNTs and PEC of composites affects the electromagnetic and microwave absorption properties of the composites. The microwave absorption properties improved when the composites were able to absorb wide bandwidth and low reflection loss. The best results are obtained for PEC-backed composites for 5%, which is about −43.56 dB at 11.1 GHz compared to without PEC-backed composites. The reflection loss is developed by the dielectric loss initiated from MWCNTs and by PEC.
Originality/value
To the best of the authors’ knowledge, no work was reported on hand lay-up method and PEC-backed composites in electromagnetic absorption properties with regression analysis.
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