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1 – 10 of 11Sagar H. Mane, Tushar S. Wagh, Gotan H. Jain and Madhavrao K. Deore
The study aims to develop an inexpensive metal oxide semiconductor gas sensor with high sensitivity, excellent selectivity for a specific gas and rapid response time.
Abstract
Purpose
The study aims to develop an inexpensive metal oxide semiconductor gas sensor with high sensitivity, excellent selectivity for a specific gas and rapid response time.
Design/methodology/approach
This study synthesized Zn2SnO4 nanostructures using a hydrothermal method with a 1 M concentration of zinc chloride (ZnCl2) as the zinc source and a 0.7 M concentration of tin chloride (SnCl4) as the tin source. Thick films of nanostructured Zn2SnO4 were then produced using screen printing. The structural properties of Zn2SnO4 were confirmed using X-ray diffraction, and the formation of Zn2SnO4 nanoparticles was verified by transmission electron microscopy. Scanning electron microscopy was used to analyse the surface morphology of the fabricated material, while energy dispersive spectroscopy provided insight into the chemical composition of the thick film. These fabricated thick films underwent testing for various hazardous gases, including nitrogen dioxide, ammonia, hydrogen sulphide (H2S), ethanol and methanol.
Findings
The nanostructured Zn2SnO4 thick film sensor demonstrates a notable sensitivity to H2S gas at a concentration of 500 ppm when operated at 160°C. Its selectivity, response time and recovery time were assessed and documented.
Research limitations/implications
The primary limitations of this research on metal oxide semiconductor gas sensors include poor selectivity to specific gases, limited durability and challenges in achieving detection at room temperature.
Practical implications
The nanostructured Zn2SnO4 thick film sensor demonstrates a strong response to H2S gas, making it a promising candidate for commercial production. The detection of H2S is crucial in various sectors, including industries and sewage plants, where monitoring this gas is essential.
Social implications
Currently, heightened global apprehension about atmospheric pollution stems from the existence of perilous toxic and flammable gases. This underscores the imperative need for monitoring such gases. Toxic and flammable gases are frequently encountered in both residential and industrial environments, posing substantial hazards to human health. Noteworthy accidents involving flammable gases have occurred in recent years. It is crucial to comprehend the presence and composition of these gases in the surroundings for precise detection, measurement and control. Thus, there has been a significant push for extensive research and development in diverse sensor technologies using various materials and methodologies to monitor and regulate these gases effectively.
Originality/value
In this research, Zn2SnO4 nanostructures were synthesized using a hydrothermal method with ZnCl2 at a concentration of 1 M for zinc and SnCl4 at a concentration of 0.7 M for tin. Thick films of nanostructured Zn2SnO4 were then fabricated via screen printing technique. Following fabrication, all thick films were subjected to testing with various toxic gases, and the results were compared to previously published data. The analysis indicated that the nanostructured Zn2SnO4 thick film sensor demonstrated outstanding performance concerning gas response, gas concentration, selectivity and response time, particularly towards H2S gas.
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Veysel Erturun and Eyyup Ozbay
The purpose of this study is AlZn-based produced by high speed mechanical alloying method to investigate the effect of Zn amount on the composite material, Al-Zn-Mg-Cu-SiC…
Abstract
Purpose
The purpose of this study is AlZn-based produced by high speed mechanical alloying method to investigate the effect of Zn amount on the composite material, Al-Zn-Mg-Cu-SiC composite material billets are obtained by sintering.
Design/methodology/approach
Mechanical alloying, X-ray diffraction analysis (XRD) graphics, sintering, polishing, scanning electron microscopy and energy dispersive X-ray analyzer (EDX) images and micro hardness tests were applied, respectively.
Findings
In the XRD analysis results, it was observed that the Al peak height decreased as the alloying time increased. When the samples sintered for 90 min are examined, it can be clearly seen that the hardness increases as the Zn ratio increases. EDX analysis results also support XRD results.
Originality/value
Increase in strength will require the use of thinner sheet metal and smaller rivets to achieve the same strength. This will reduce the weight of the aircraft. Weight reduction also means less fuel consumption and more economical flight. This increase in strength is a very important scientific achievement.
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Yu Fu, Junwen Zhao, Xujia Li and Yiwen Peng
This paper aims to prepare high corrosion-resistant chromium-free zinc-aluminum (Zn–Al) coatings reinforced with multi-walled carbon nanotubes (MWCNTs) and nano-ZnO particle…
Abstract
Purpose
This paper aims to prepare high corrosion-resistant chromium-free zinc-aluminum (Zn–Al) coatings reinforced with multi-walled carbon nanotubes (MWCNTs) and nano-ZnO particle composites.
Design/methodology/approach
The morphology, composition and corrosion resistance of the coatings were analyzed by electrochemical tests, water contact angle tests, immersion tests, scanning electron microscopy/energy dispersive spectrometer and X-ray diffraction.
Findings
The composite coating with 0.3% MWCNTs and 0.5% nano-ZnO particles demonstrated both high shielding performance and cathodic protection performance, which was attributed to the porosity filling of MWCNTs and nano-ZnO particles together with the electrical connection of MWCNTs between the zinc and aluminum powders.
Originality/value
This work laid an experimental foundation for the preparation and corrosion mechanism of high corrosion-resistant chromium-free Zn–Al coating reinforced with MWCNTs and nano-ZnO particles.
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Yitian Chi, Narayanan Murali and Xiaochun Li
High-performance wrought aluminum alloys, particularly AA6061, are pivotal in industries like automotive and aerospace due to their exceptional strength and good response to heat…
Abstract
Purpose
High-performance wrought aluminum alloys, particularly AA6061, are pivotal in industries like automotive and aerospace due to their exceptional strength and good response to heat treatments. Investment casting offers precision manufacturing for these alloys, because casting AA6061 poses challenges like hot cracking and severe shrinkage during solidification. This study aims to address these issues, enabling crack-free investment casting of AA6061, thereby unlocking the full potential of investment casting for high-performance aluminum alloy components.
Design/methodology/approach
Nanotechnology is used to enhance the investment casting process, incorporating a small volume fraction of nanoparticles into the alloy melt. The focus is on widely used aluminum alloy 6061, utilizing rapid investment casting (RIC) for both pure AA6061 and nanotechnology-enhanced AA6061. Microstructural characterization involved X-ray diffraction, optical microscopy, scanning electron microscopy, differential scanning calorimetry and energy dispersive X-ray spectroscopy. Mechanical properties were evaluated through microhardness and tensile testing.
Findings
The study reveals the success of nanotechnology-enabled investment casting in traditionally challenging wrought aluminum alloys like AA6061. Achieving crack-free casting, enhanced grain morphology and superior mechanical properties, because the nanoparticles control grain sizes and phase growth, overcoming traditional challenges associated with low cooling rates. This breakthrough underscores nanotechnology's transformative impact on the mechanical integrity and casting quality of high-performance aluminum alloys.
Originality/value
This research contributes originality and value by successfully addressing the struggles in investment casting AA6061. The novel nano-treating approach overcomes solidification defects, showcasing the potential of integrating nanotechnology into rapid investment casting. By mitigating challenges in casting high-performance aluminum alloys, this study paves the way for advancements in manufacturing crack-free, high-quality aluminum alloy components, emphasizing nanotechnology's transformative role in precision casting.
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Danusa Silva da Costa, Lucely Nogueira dos Santos, Nelson Rosa Ferreira, Katiuchia Pereira Takeuchi and Alessandra Santos Lopes
The aim was not to perform a systematic review but firstly to search in PubMed, Science Direct, Scopus and Web of Science databases on the papers published in the last five years…
Abstract
Purpose
The aim was not to perform a systematic review but firstly to search in PubMed, Science Direct, Scopus and Web of Science databases on the papers published in the last five years using tools for reviewing the statement of preferred information item for systematic reviews without focusing on a randomized analysis and secondly to perform a bibliometric analysis on the properties of films and coatings added of tocopherol for food packaging.
Design/methodology/approach
On January 24, 2022, information was sought on the properties of films and coatings added of tocopherol for use as food packaging published in PubMed, Science Direct, Scopus and Web of Science databases. Further analysis was performed using bibliometric indicators with the VOSviewer tool.
Findings
The searches returned 33 studies concerning the properties of films and coatings added of tocopherol for food packaging, which were analyzed together for a better understanding of the results. Data analysis using the VOSviewer tool allowed a better visualization and exploration of these words and the development of maps that showed the main links between the publications.
Originality/value
In the area of food science and technology, the development of polymers capable of promoting the extension of the shelf life of food products is sought, so the knowledge of the properties is vital for this research area since combining a biodegradable polymeric material with a natural antioxidant active is of great interest for modern society since they associate environmental preservation with food preservation.
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Mohamed El Boukhari, Ossama Merroun, Chadi Maalouf, Fabien Bogard and Benaissa Kissi
The purpose of this study is to experimentally determine whether mechanical properties of concrete can be improved by using olive pomace aggregates (OPA) as a substitute for…
Abstract
Purpose
The purpose of this study is to experimentally determine whether mechanical properties of concrete can be improved by using olive pomace aggregates (OPA) as a substitute for natural sand. Two types of OPA were tested by replacing an equivalent amount of natural sand. The first type was OPA mixed with olive mill wastewater (OMW), and the second type was OPA not mixed with OMW. For each type, two series of concrete were produced using OPA in both dry and saturated states. The percentage of partial substitution of natural sand by OPA varied from 0% to 15%.
Design/methodology/approach
The addition of OPA leads to a reduction in the dry density of hardened concrete, causing a 5.69% decrease in density when compared to the reference concrete. After 28 days, ultrasonic pulse velocity tests indicated that the resulting material is of good quality, with a velocity of 4.45 km/s. To understand the mechanism of resistance development, microstructural analysis was conducted to observe the arrangement of OPA and calcium silicate hydrates within the cementitious matrix. The analysis revealed that there is a low level of adhesion between the cement matrix and OPA at interfacial transition zone level, which was subsequently validated by further microstructural analysis.
Findings
The laboratory mechanical tests indicated that the OPCD_OPW (5) sample, containing 5% of OPA, in a dry state and mixed with OMW, demonstrated the best mechanical performance compared to the reference concrete. After 28 days of curing, this sample exhibited a compressive strength (Rc) of 25 MPa. Furthermore, it demonstrated a tensile strength of 4.61 MPa and a dynamic modulus of elasticity of 44.39 GPa, with rebound values of 27 MPa. The slump of the specimens ranged from 5 cm to 9 cm, falling within the acceptable range of consistency (Class S2). Based on these findings, the OPCD_OPW (5) formulation is considered optimal for use in concrete production.
Originality/value
This research paper provides a valuable contribution to the management of OPA and OMW (OPA_OMW) generated from the olive processing industry, which is known to have significant negative environmental impacts. The paper presents an intriguing approach to recycling these materials for use in civil engineering applications.
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Mandeep Singh, Khushdeep Goyal and Deepak Bhandari
The purpose of this paper is to evaluate the effect of titanium oxide (TiO2) and yttrium oxide (Y2O3) nanoparticles-reinforced pure aluminium (Al) on the mechanical properties of…
Abstract
Purpose
The purpose of this paper is to evaluate the effect of titanium oxide (TiO2) and yttrium oxide (Y2O3) nanoparticles-reinforced pure aluminium (Al) on the mechanical properties of hybrid aluminium matrix nanocomposites (HAMNCs).
Design/methodology/approach
The HAMNCs were fabricated via a vacuum die-assisted stir casting route by a two-step feeding method. The varying weight percentages of TiO2 and Y2O3 nanoparticles were added as 2.5, 5, 7.5 and 10 Wt.%.
Findings
Scanning electron microscope images showed the homogenous dispersion of nanoparticles in Al matrix. The tensile strength by 28.97%, yield strength by 50.60%, compression strength by 104.6% and micro-hardness by 50.90% were improved in HAMNC1 when compared to the base matrix. The highest values impact strength of 36.3 J was observed for HAMNC1. The elongation % was decreased by increasing the weight percentage of the nanoparticles. HAMNC1 improved the wear resistance by 23.68%, while increasing the coefficient of friction by 14.18%. Field emission scanning electron microscope analysis of the fractured surfaces of tensile samples revealed microcracks and the debonding of nanoparticles.
Originality/value
The combined effect of TiO2 and Y2O3 nanoparticles with pure Al on mechanical properties has been studied. The composites were fabricated with two-step feeding vacuum-assisted stir casting.
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Hossam El-Din Fawzy, Maher Badawy and Magda Farhan
This paper aims to discuss the scanning methodology depending on the close-range photogrammetry technique, which is appropriate for the precise three-dimensional (3D) modelling of…
Abstract
Purpose
This paper aims to discuss the scanning methodology depending on the close-range photogrammetry technique, which is appropriate for the precise three-dimensional (3D) modelling of objects in millimetres, such as the dimensions and structures in sub-millimetre scale.
Design/methodology/approach
The camera was adjusted to be tilted around the horizontal axis, while coded dot targets were used to calibrate the digital camera. The experiment was repeated with different rotation angles (5°, 10°, 15°, 20°, 25°, 30°, 50° and 60°). The images were processed with the PhotoModeler software to create the 3D model of the sample and estimate its dimensions. The features of the sample were measured using high-resolution transmission electron microscopy, which has been considered as a reference and the comparative dimensions.
Findings
The results from the current study concluded that changing the rotation angle does not significantly affect the results, unless the angle of imagery is large which prevent achieving about 20: 30% overlap between the images but, the more angle decreases, the more number of images increase as well as the processing duration in the programme.
Originality/value
Develop an automatic appropriate for the precise 3D modelling of objects in millimetres, such as the dimensions and structures in sub-millimetre scale using photogrammetry.
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Lindsey Bezek and Kwan-Soo Lee
Although ceramic additive manufacturing (AM) could be used to fabricate complex, high-resolution parts for diverse, functional applications, one ongoing challenge is optimizing…
Abstract
Purpose
Although ceramic additive manufacturing (AM) could be used to fabricate complex, high-resolution parts for diverse, functional applications, one ongoing challenge is optimizing the post-process, particularly sintering, conditions to consistently produce geometrically accurate and mechanically robust parts. This study aims to investigate how sintering temperature affects feature resolution and flexural properties of silica-based parts formed by vat photopolymerization (VPP) AM.
Design/methodology/approach
Test artifacts were designed to evaluate features of different sizes, shapes and orientations, and three-point bend specimens printed in multiple orientations were used to evaluate mechanical properties. Sintering temperatures were varied between 1000°C and 1300°C.
Findings
Deviations from designed dimensions often increased with higher sintering temperatures and/or larger features. Higher sintering temperatures yielded parts with higher strength and lower strain at break. Many features exhibited defects, often dependent on geometry and sintering temperature, highlighting the need for further analysis of debinding and sintering parameters.
Originality/value
To the best of the authors’ knowledge, this is the first time test artifacts have been designed for ceramic VPP. This work also offers insights into the effect of sintering temperature and print orientation on flexural properties. These results provide design guidelines for a particular material, while the methodology outlined for assessing feature resolution and flexural strength is broadly applicable to other ceramics, enabling more predictable part performance when considering the future design and manufacture of complex ceramic parts.
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Martin Novák, Berenika Hausnerova, Vladimir Pata and Daniel Sanetrnik
This study aims to enhance merging of additive manufacturing (AM) techniques with powder injection molding (PIM). In this way, the prototypes could be 3D-printed and mass…
Abstract
Purpose
This study aims to enhance merging of additive manufacturing (AM) techniques with powder injection molding (PIM). In this way, the prototypes could be 3D-printed and mass production implemented using PIM. Thus, the surface properties and mechanical performance of parts produced using powder/polymer binder feedstocks [material extrusion (MEX) and PIM] were investigated and compared with powder manufacturing based on direct metal laser sintering (DMLS).
Design/methodology/approach
PIM parts were manufactured from 17-4PH stainless steel PIM-quality powder and powder intended for powder bed fusion compounded with a recently developed environmentally benign binder. Rheological data obtained at the relevant temperatures were used to set up the process parameters of injection molding. The tensile and yield strengths as well as the strain at break were determined for PIM sintered parts and compared to those produced using MEX and DMLS. Surface properties were evaluated through a 3D scanner and analyzed with advanced statistical tools.
Findings
Advanced statistical analyses of the surface properties showed the proximity between the surfaces created via PIM and MEX. The tensile and yield strengths, as well as the strain at break, suggested that DMLS provides sintered samples with the highest strength and ductility; however, PIM parts made from environmentally benign feedstock may successfully compete with this manufacturing route.
Originality/value
This study addresses the issues connected to the merging of two environmentally efficient processing routes. The literature survey included has shown that there is so far no study comparing AM and PIM techniques systematically on the fixed part shape and dimensions using advanced statistical tools to derive the proximity of the investigated processing routes.
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