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Porosity is one of the most important properties of the textile substrate. It can influence the comfort of a garment by affecting its breathability and thermal conductivity. During the process of dyeing, the dye liquor comes in contact with the substrate; the absorption of the dye liquor into the substrate will be dependent on its porosity. The concept of porosity between the yarns of fabric is a common phenomenon; however, the porosity between the fibres in the yarn can also influence the dyeing behaviour of the fabric.

In this research, ring and rotor yarns of 25/s and 30/s counts are considered as textile substrates. The porosity of yarns was determined theoretically and experimentally using the image analysis method.

It was found that theoretical porosity is independent of the yarn manufacturing method. In addition, 30/s yarn was more porous as compared with 25/s yarn having a higher pore area. Rotor yarns had higher porosity, dye fixation and K/S as compared with ring yarns. Dyeing behaviour was also dependent on the count of yarn. Specifically, 30/s yarns have higher dye fixation as compared with 25/s yarns. However, 25/s yarns were dyed with deeper shades showing higher K/S values. Also, 25/s yarns are coarser than 30/s yarns having higher diameters and cross-sectional area, thus resulting in deeper shades and higher K/S values.

This novel technique is based on the comparative study of the porosity of various types of yarns using the image analysis technique. This investigation shows that the porosity between the fibres in the yarn can also influence the dyeing behaviour of the yarn.

Efficient numerical assessment of performance is particularly important in digital material design of porous materials. This study aims to present an up-scaled approach to virtually investigate permeation of fluids through a real porous filter membrane with a heterogeneous micro-structure.

The method of asymptotic homogenization is applied. The structural parameters of the micro-structure are directly obtained from structural equation modeling image analysis of a commercial filter membrane without fitting procedures. The simulation results are compared to permeation experiments of gaseous nitrogen and liquid water.

The authors found that variations in the pressure gradients across the membrane, resulting from the heterogeneity of pore structure, need to be considered. Remarkable agreement between simulations and experiments is observed.

Despite some research in the field of filtration, no studies on filter membranes have been published yet, although they represent a large segment of filtration technology.

This paper aims to study the anodization of aluminum in a mixture solution of 1,3-propanediol solutions and 0.4 mol l⁻¹ H₃PO₄ at a low temperature.

The morphology and composition of the resulting anodic aluminum oxide (AAO) template was characterized by means of a scanning electron microscope in combination with an energy dispersive spectrometer.

Pore density and pore diameter both were found to be dependent on the temperature of anodization.

The resulting AAO templates exhibited uniform and regular pores with diameters that were significantly smaller than those found in AAO templates anodized at room temperature.

In recent years, fire accidents in engineering structures have often been reported worldwide, leading to a severe risk to life and property safety. The present study is carried out to evaluate the performance of Ground Granulated Blast Furnace Slag (GGBS) and fly ash–blended laterized mortars at elevated temperatures.

This test program includes the replacement of natural river sand with lateritic fine aggregates (lateritic FA) in terms of 0, 50 and 100%. Also, the ordinary Portland cement (OPC) was replaced with fly ash and GGBS in terms of 10, 20, 30% and 20, 40 and 60%, respectively, for producing blended mortars.

This paper presents results related to the determination of residual compressive strengths of lateritic fine aggregates-based cement mortars with part replacement of cement by fly ash and GGBS exposed to elevated temperatures. The effect of elevated temperatures on the physical and mechanical properties was evaluated with the help of microstructure studies and the quantification of hydration products.

A sustainable cement mortar was produced by replacing natural river sand with lateritic fine aggregates. The thermal strength deterioration features were assessed by exposing the control specimens and lateritic fine aggregates-based cement mortars to elevated temperatures. Changes in the mechanical properties were evaluated through a quantitative microstructure study using scanning electron microscopy (SEM) images. The phase change of hydration products after exposure to elevated temperatures was qualitatively analyzed by greyscale thresholding of SEM images using Image J software.

The purpose of this paper is to evaluate the effect of post process combinations, e.g. hot isostatic pressing (HIP) only, HIP + T6 heat treatments, and T6 only, with different aging time, on surface properties, microstructure and mechanical properties of stress-relieved AlSi10Mg parts produced by direct laser metal sintering.

HIP process and HIP + T6 heat treatments were applied to as stress-relieved direct laser metal sintered (DMLS) AlSi10Mg parts. Aging times of 4 and 12 h are selected to examine the optimum duration. To analyze the advantages of HIP process, a T6 heat treatment with 4 h of aging was also applied. Densities, open porosities and roughness values of as stress-relieved, HIPed, HIP + T6, and T6-only samples were measured. The samples were characterized by OM and SEM together with EDX analysis. An image analysis study was made to evaluate the inner pore structure, thereby to understand the mechanical behavior.

HIP process does not cause a significant change in surface porosity; yet it has a positive influence on inner porosity. HIP process results in a microstructure of the aluminum matrix surrounded by a network of micron and nano size Si particles. Additional heat treatment results in larger particles and precipitation. After HIPing, ductility increases but strength decreases. Samples aged 4 h present improved yield and tensile strength but decreased elongation, yet samples aged for 12 h reach a combination of optimum strength and ductility. The lower level of tensile strength and ductility in T6-only condition indicates that HIP process plays a crucial role in elimination of the porosity thus improves the effectiveness of subsequent heat treatment.

The study investigates the effect of post-process conditions and optimizes the aging time of the T6 heat treatment after HIP process in order to obtain improved mechanical properties. The stress-relieved state was chosen as the reference to prevent distortion during HIPing or heat treatment.

Pores and shrink holes are unavoidable defects in the die-casting mass production process which may significantly influence the strength, fatigue and fracture behaviour as well as the life span of structures, especially if they are subjected to high static and dynamic loads. Such defects should be considered during the design process or after production, where the defects could be detected with the help of computed tomography (CT) measurements. However, this is usually not done in today's mass production environments. This paper deals with the stress analysis of die-cast structural parts with pores found from CT measurements or that are artificially placed within a structure.

In this paper the authors illustrate two general methodologies to take into account the porosity of die-cast components in the stress analysis. The detailed geometry of a die-cast part including all discontinuities such as pores and shrink holes can be included via STL data provided by CT measurements. The first approach is a combination of the finite element method (FEM) and the finite cell method (FCM), which extends the FEM if the real geometry cuts finite elements. The FCM is only applied in regions with pores. This procedure has the advantage that all simulations with different pore distributions, real or artificial, can be calculated without changing the base finite element mesh. The second approach includes the pore information as STL data into the original CAD model and creates a new adapted finite element mesh for the simulation. Both methods are compared and evaluated for an industrial problem.

The STL data of defects which the authors received from CT measurements could not be directly applied without repairing them. Therefore, for FEM applications an appropriate repair procedure is proposed. The first approach, which combines the FEM with the FCM, the authors have realized within the commercial software tool Abaqus. This combination performs well, which is demonstrated for test examples, and is also applied for a complex industrial project. The developed in-house code still has some limitations which restrict broader application in industry. The second pure FEM-based approach works well without limitations but requires increasing computational effort if many different pore distributions are to be investigated.

A new simulation approach which combines the FEM with the FCM has been developed and implemented into the commercial Abaqus FEM software. This approach the authors have applied to simulate a real engineering die-cast structure with pores. This approach could become a preferred way to consider pores in practical applications, where the porosity can be derived either from CT measurements or are artificially adopted for design purposes. The authors have also shown how pores can be considered in the standard FEM analysis as well.

Unrefined vegetable oils contain triglycerides and free fatty acids as the main ingredient, but besides, they contain waxes, phospholipids, tocopherols, β-carotene, chlorophyll and other trace amounts depending on the type of oil. Most undesirable substances such as residues, free fatty acids and phospholipids are separated in the neutralization process of the oil refining. As a pigment, β carotene is separated by the bleaching earth (BE) in the bleaching process. The BE is disposed of as waste after the bleaching process. In this study, waste BE, which is allocated for disposal, has become reusable.

For this purpose, the oil is separated from the BE by solvent extraction under room conditions. AOCS Ba 3-38, TS EN ISO 734, ISO 15305 and TS 324 standard methods were used.

As a result of the analysis, it was found that 1% of oil remained in the recovered BE. The recovered BE containing 1% oil was carbonized at 550^oC for 1 and 2 h. The BE obtained after this process was used in the bleaching process at a rate of 1%. Reuse attempts were repeated seven times, colour-opening capacities were measured and BET analyses were performed to establish a relationship between surface area-discolouration capacity and reusability.

This study demonstrates that recovery of waste BE can be performed and if this reusability considers in the industrial scale, it will save on oil refining costs and reduce waste.

This paper aims to investigate the electroporation phenomenon in a single cell exposed to ultra short (μs) and high voltage (kV) electric pulses.

The problem is addressed by two complementary approaches. First, numerical simulations based on an asymptotic approximation derived from the Smoluchowski theory are used to calculate the pore generation, growth and size evolution at the membrane of a spherical cell model, immersed in a suspension medium and consisting of cytoplasm and membrane. The numerical calculations are solved using the finite difference method. Second, an in vitro experiment with LLC-MK2 cells is carried out in which electroporation was monitored with molecules of propidium iodide. This part also comprehended the design and manufacturing of a portable electric pulse generator capable of providing rectangular pulses with amplitude of 1,000 V and duration in the range of 1-μs to 100-μs. The pulse generator is composed of three modules: a high voltage DC source, a control module, and an energy storage and high voltage switching.

The numerical simulations considered a 5-μm radius cell submitted to a 500 kV/m rectangular electric pulse for 1-μs. The results indicate the formation of around 3,500 pores at the cell membrane, most of them, around 950, located at the poles of the cell aligned to the applied electric pulse, with radii sizes varying from 0.5-nm to 13-nm. The in vitro experiment considered exposition of LLC-MK2 cells to pulses of 200 V, 500 V, and 700 V, and 1-μs. Images from fluorescence microscopy exhibit the LLC-MK2 cells with intense red, a strong evidence of the electroporation.

The work presents a thorough study of the electroporation phenomenon combining two complementary approaches, a rigorous numerical simulation and a detailed in vitro experiment.

This study aims to investigate the effect of three-dimensional (3D)- bioplotted polycaprolactone (PCL) scaffold geometry on the biological and mechanical characteristics of human adipose-derived stem cell (hASC) seeded constructs.

Four 3D-bioplotted scaffold disc designs (Ø14.5 × 2 mm) with two levels of strand–pore feature sizes and two strand laydown patterns (0°/90° or 0°/120°/240°) were evaluated for hASC viability, proliferation and construct compressive stiffness after 14 days of in vitro cell culture.

Scaffolds with the highest porosity (smaller strand–pore size in 0°/120°/240°) yielded the highest hASC proliferation and viability. Further testing of this design in a 6-mm thick configuration showed that cells were able to penetrate and proliferate throughout the scaffold thickness. The design with the lowest porosity (larger strand–pore size in 0°/90°) had the highest compression modulus after 14 days of culture, but resulted in the lowest hASC viability. The strand laydown pattern by itself did not influence the compression modulus of scaffolds. The 14-day cell culture also did not cause significant changes in compressive properties in any of the four designs.

hASC hold great potential for musculoskeletal tissue engineering applications because of their relative ease of harvest, abundance and differentiation abilities. This study reports on the effects of 3D-bioplotted scaffold geometry on mechanical and biological characteristics of hASC-seeded PCL constructs. The results provide the basis for future studies which will use this optimal scaffold design to develop constructs for hASC-based osteochondral tissue engineering applications.

The purpose of this study is to evaluate different 3D structures for humidity sensing that will enable the fabrication of complex geometries with high moisture sensitivity.

Humidity sensors based on alumina ceramics were fabricated using direct ink write (DIW) technique. Different engineered surface area, polymer binder ratio and post-processing treatment were considered to increase moisture sensitivity.

It was found that the binder ratio plays an important role in controlling the rheology of the paste during printing and determining the pore size after post-processing treatment. The sensibility of the fabricated humidity sensor was investigated by measuring its capacitance response toward relative humidity (RH) varying from 40% to 90% RH at 25°C. It is shown that using 3D lattice design, printed alumina humidity sensor could improve sensitivity up to 31.6 pF/RH%, over an order of magnitude higher than solid alumina.

Most of the alumina humidity sensors available are films in nature because of manufacturing difficulties, which limited its potential of higher sensitivity, and thus broader applications. In this paper, a novel 3D alumina humidity sensor was fabricated using DIW 3D printing technology.