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Because aero‐engine turbine blades operate at temperatures approaching 1,400°C they are designed with complex internal cooling passages. The only economic production process…
Abstract
Because aero‐engine turbine blades operate at temperatures approaching 1,400°C they are designed with complex internal cooling passages. The only economic production process capable of making the blades is to cast exotic alloys in a ceramic mould around a ceramic core. The core is usually an airfoil shaped ceramic part made to close limits of accuracy. Doulton Industrial Products has made ceramic cores used in the casting of turbine blades for most of the world's aero‐engine companies since 1961. The company's contribution in pioneering ceramic techniques is second to none.
Regina Knitter, Werner Bauer, Dieter Göhring and Peter Risthaus
Conventional shaping processes for ceramics are mostly based on a powder‐technological molding process using a negative mold and subsequent thermal compaction. Especially for…
Abstract
Conventional shaping processes for ceramics are mostly based on a powder‐technological molding process using a negative mold and subsequent thermal compaction. Especially for prototypes and small lot series of microcomponents the outlay for molds are the major costing factor. Consequently the use of rapid prototyping (RP) processes can decisively reduce the costs and time in product development of ceramic microcomponents. In spite of the fact, that a large number of freeform fabrication techniques for different materials were developed in recent years, most generative techniques of ceramics still have different drawbacks for the fabrication of prototypes and often exhibit limited resolution compared to those of polymers. The combination of RP techniques such as micro stereolithography and ceramic injection molding in a RP process chain can fill in the gap between the limited applicability of solid freeform fabrication of ceramics and the restricted material properties of polymers.
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Joel W. Barlow, Joseph J. Beaman and Badrinarayan Balasubramanian
Presents the mechanical properties of a new mould‐making material, proposed for producing rapidly prototyped injection mould inserts for plastics by selective laser sintering…
Abstract
Presents the mechanical properties of a new mould‐making material, proposed for producing rapidly prototyped injection mould inserts for plastics by selective laser sintering. Explains that although the strength of this material is far below that of the tool steel usually used to fabricate moulds, design calculations indicate that it can still be used for mould insert production. Points out that the thermal conductivity of this material is lower than that for steel but higher than that for plastic melts. Indicates from the calculations that proper choices of conduction length and cycle time can minimize differences, relative to steel moulds, in the operational behaviour of moulds made of the new material. Discusses the longevity of example moulds.
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Mimi Azlina Abu Bakar, Siti Norazlini Abd Aziz and Muhammad Hussain Ismail
This paper aims to investigate the vital characteristic of an innovative ceramic injection molding (CIM) process for orthopedic application with controlled porosity and improved…
Abstract
Purpose
This paper aims to investigate the vital characteristic of an innovative ceramic injection molding (CIM) process for orthopedic application with controlled porosity and improved tribological and mechanical properties which were affected by complex tribological interactions, whether lubricated like hip implants and other artificial prostheses. The main objective is to maximize the usage of palm stearin as a single based binder as the function of flow properties during injection molding process.
Design/methodology/approach
The binder used in this present study consists of 100 per cent palm stearin manufactured by Kempas Oil Sdn Bhd and supplied by Vistec Technology Sdn Bhd. The feedstock was prepared by using a Z-blade mixer (Thermo Haake Rheomix OS) and Brabender mixer model R2400. The feedstock prepared was injection molded using a manually operated vertical benchtop machine with an average pressure of about 5-7 bars. The firing step included the temporary holds at intermediate temperatures to burn out organic binders. At this stage, the green molded specimen was de-bound using a single-step wick-debinding method.
Findings
The maximum content of ceramic material is applied to investigate the efficiencies of net formulation that can be achieved by ceramic materials. The longer the viscosity will change with shear rate, the higher the value of n obtained instead. From the slope of the curves obtained in Figure 3, the value of n for the feedstock was determined to be less than 1, which indicates a pseudoplastic behavior and suitability for the molding process. Moreover, high shear sensitivity is important in producing complex and intrinsic specimens which are leading products in the CIM industry.
Originality/value
The feedstock containing HAp powder and palm stearin binder was successfully prepared at very low temperature of 70°C, which promoting a required pseudo-plastic behavior during rheological test. The single binder palm stearin should be optimized in other research works carried out, as palm stearin is most preferred compared to other polymeric materials that provided high energy consumption when subjected to the sintering process. Besides the binder is widely available in Malaysia, low cost and harmless effect during debinding process.
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The purpose of this study is to prepare a state-of-the-art review on advanced ceramic materials including their fabrication techniques, characteristics, applications and…
Abstract
Purpose
The purpose of this study is to prepare a state-of-the-art review on advanced ceramic materials including their fabrication techniques, characteristics, applications and wettability.
Design/methodology/approach
This review paper presents the various types of advanced ceramic materials according to their compounding elements, fabrication techniques of advanced ceramic powders as well as their consolidation, their characteristics, applications and wetting properties. Hydrophobic/hydrophilic properties of advanced ceramic materials are described in the paper with their state-of-the-art application areas. Optical properties of fine ceramics with their intrinsic characteristics are also presented within. Special focus is given to the brief description of application-based manipulation of wetting properties of advanced ceramics in the paper.
Findings
The study of wetting/hydrophobicity/hydrophilicity of ceramic materials is important by which it can be further modified to achieve the required applications. It also makes some sense that the material should be tested for its wetting properties when it is going to be used in some important applications like biomedical and dental. Also, these advanced ceramics are now often used in the fabrication of filters and membranes to purify liquid/water so the study of wetting characteristics of these materials becomes essential. The optical properties of advanced ceramics are equally making them suitable for many state-of-the-art applications. Dental, medical, imaging and electronics are the few sectors that use advanced ceramics for their optical properties.
Originality/value
This review paper includes various advanced ceramic materials according to their compounding elements, different fabrication techniques of powders and their consolidation, their characteristics, various application area and hydrophobic/hydrophilic properties.
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James G. Hemrick, Thomas L. Starr and David W. Rosen
Adhesion has been measured between a powder injection molded (PIM) part and the stereolithography epoxy mold surrounding it after cooling. Analysis of release behavior suggests a…
Abstract
Adhesion has been measured between a powder injection molded (PIM) part and the stereolithography epoxy mold surrounding it after cooling. Analysis of release behavior suggests a link to the thermal properties of the mold material. Subsequent measurements of cooling in the part and at the part/mold interface are consistent with a one‐dimensional heat transfer model. Adhesion development at the part/mold interface shows a complex dependence on the thermal characteristics of both the mold and the PIM feedstock.
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Aldi Mehmeti, Pavel Penchev, Donal Lynch, Denis Vincent, Nathalie Maillol, Johannes Maurath, Julien Bajolet, David Ian Wimpenny, Khamis Essa and Stefan Dimov
The paper reports an investigation into the mechanical behaviour of hybrid components produced by combining the capabilities of metal injection moulding (MIM) with the laser-based…
Abstract
Purpose
The paper reports an investigation into the mechanical behaviour of hybrid components produced by combining the capabilities of metal injection moulding (MIM) with the laser-based powder bed fusion (PBF) process to produce small series of hybrid components. The research investigates systematically the mechanical properties and the performance of the MIM/PBF interfaces in such hybrid components.
Design/methodology/approach
The MIM process is employed to fabricate relatively lower cost preforms in higher quantities, whereas the PBF technology is deployed to build on them sections that can be personalised, customised or functionalised to meet specific technical requirements.
Findings
The results are discussed, and conclusions are made about the mechanical performance of such hybrid components produced in batches and also about the production efficiency of the investigated hybrid manufacturing (HM) route. The obtained results show that the proposed HM route can produce hybrid MIM/PBF components with consistent mechanical properties and interface performance which comply with the American Society for Testing and Materials (ASTM) standards.
Originality/value
The manufacturing of hybrid components, especially by combining the capabilities of additive manufacturing processes with cost-effective complementary technologies, is designed to be exploited by industry because they can offer flexibility and cost advantages in producing small series of customisable products. The findings of this research will contribute to further develop the state of the art in regards to the manufacturing and optimisation of hybrid components.
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Luigi Morfini, Fankai Meng, Margherita Beretta, Jozef Vleugels, Roberto Spina and Eleonora Ferraris
This study aims to investigate the performance of filament-based material extrusion additive manufacturing (MEX), combined with debinding and sintering, as a novel approach to…
Abstract
Purpose
This study aims to investigate the performance of filament-based material extrusion additive manufacturing (MEX), combined with debinding and sintering, as a novel approach to manufacturing ceramic components.
Design/methodology/approach
A commercial ZrO2 filament was selected and analysed by infra-red (IR) spectroscopy, rheology and thermo-gravimetry. The influence of the print parameters (layer thickness, flow rate multiplier, printing speed) and sintering cycle were investigated to define a suitable printing and sintering strategy. Biaxial flexure tests were applied on sintered discs realised with optimised printing strategies, and the results were analysed via Weibull statistics to evaluate the mechanical properties of printed components. The hardness and thermal conductivity of sintered components were also tested.
Findings
Layer thickness and flow rate multiplier of the printing process were proved to have significant effect on the density of as-printed parts. Optimised samples display a sintered density >99% of the theoretical density, 20% linear sintering shrinkage, a characteristic flexural strength of 871 MPa with a Weibull modulus of 4.9, a Vickers hardness of 12.90 ± 0.3 GPa and a thermal conductivity of 3.62 W/mK. Gyroids were printed for demonstration purposes.
Originality/value
To the best of the authors’ knowledge, this work is the first to apply biaxial flexure tests and Weibull statistics to additively manufactured MEX zirconia components, hence providing comparable results to other additive technologies. Moreover, fractography analysis builds the connection between printing defects and the fracture mechanism of bending. This study also provides guidelines for fabricating high-density zirconia components with MEX.
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Martin Novák, Berenika Hausnerova, Vladimir Pata and Daniel Sanetrnik
This study aims to enhance merging of additive manufacturing (AM) techniques with powder injection molding (PIM). In this way, the prototypes could be 3D-printed and mass…
Abstract
Purpose
This study aims to enhance merging of additive manufacturing (AM) techniques with powder injection molding (PIM). In this way, the prototypes could be 3D-printed and mass production implemented using PIM. Thus, the surface properties and mechanical performance of parts produced using powder/polymer binder feedstocks [material extrusion (MEX) and PIM] were investigated and compared with powder manufacturing based on direct metal laser sintering (DMLS).
Design/methodology/approach
PIM parts were manufactured from 17-4PH stainless steel PIM-quality powder and powder intended for powder bed fusion compounded with a recently developed environmentally benign binder. Rheological data obtained at the relevant temperatures were used to set up the process parameters of injection molding. The tensile and yield strengths as well as the strain at break were determined for PIM sintered parts and compared to those produced using MEX and DMLS. Surface properties were evaluated through a 3D scanner and analyzed with advanced statistical tools.
Findings
Advanced statistical analyses of the surface properties showed the proximity between the surfaces created via PIM and MEX. The tensile and yield strengths, as well as the strain at break, suggested that DMLS provides sintered samples with the highest strength and ductility; however, PIM parts made from environmentally benign feedstock may successfully compete with this manufacturing route.
Originality/value
This study addresses the issues connected to the merging of two environmentally efficient processing routes. The literature survey included has shown that there is so far no study comparing AM and PIM techniques systematically on the fixed part shape and dimensions using advanced statistical tools to derive the proximity of the investigated processing routes.
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Kamatchi Subramanian, Neal Vail, Joel Barlow and Harris Marcus
The selective laser sintering (SLS) process is used to prepare test bars from Al2O3/polymer binder powders. Finds that binder‐coated A12O3 particles formed bars that were…
Abstract
The selective laser sintering (SLS) process is used to prepare test bars from Al2O3/polymer binder powders. Finds that binder‐coated A12O3 particles formed bars that were approximately twice as strong as could be formed from mixtures of alumina and polymer binder at the same binder level and processing conditions. In mixed systems, bar strengths increased nearly in proportion to increases in polymer binder content over the 20‐40 per cent volume binder range. Parts made in any particular laser scanning mode showed optimum values for strength and density as the laser energy density was systematically increased from 2‐8cal/cm2. Suggests that optima result from the counteracting influences of energy density on binder fusion and thermal degradation. The optimum energy density is mode or geometry sensitive and shifts to lower values as the laser scanning vector is reduced. Concludes that this behaviour is probably the result of the lower heat losses. Equivalently better utilization of laser energy is associated with the shorter scan vectors. Some of the SLS fabricated bars were infiltrated with colloidal alumina, fired to remove the binder, and sintered at 1,600°C to achieve alumina bars with 50 per cent relative densities, interconnected porosity, and strengths between 2 and 8MPa.
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