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1 – 10 of 303Natthawut Daoset, Samroeng Inglam, Sujin Wanchat and Nattapon Chantarapanich
This paper aims to investigate the influence of post-curing temperature, post-curing time and gamma ray irradiation dose upon the tensile and compressive mechanical properties of…
Abstract
Purpose
This paper aims to investigate the influence of post-curing temperature, post-curing time and gamma ray irradiation dose upon the tensile and compressive mechanical properties of the medical graded vat photopolymerization parts.
Design/methodology/approach
Medical graded vat photopolymerization specimens, made from photopolymer resin, were fabricated using bottom-up vat photopolymerization machine. Tensile and compressive tests were conducted to assess the mechanical properties. The specimens were categorized into uncured and post-curing groups. Temperature post-processing and/or gamma irradiation exposure were for post-curing specimens. The post-curing parameters considered included temperature levels of 50°C, 60°C and 70°C, with 1, 2, 3 and 4 h periods. For the gamma irradiation, the exposure doses were 25, 50, 75 and 100 kGy.
Findings
Post-curing improved the mechanical properties of medical graded vat photopolymerization parts for both tensile and compressive specimens. Post-curing temperature greater than 50°C or a prolonged post-curing period of more than 1 h made insignificant changes or deterioration in mechanical properties. The optimal post-curing condition was therefore a 50°C post-curing temperature with 1 h post-curing time. Exposure to gamma ray improved the compressive mechanical properties, but deteriorated tensile mechanical properties. Higher gamma irradiation doses could decrease the mechanical properties and also make the part more brittle, especially for doses more than 25 kGy.
Originality/value
The obtained results would be beneficial to the medical device manufacturer who fabricated the invasive temporary contact personalized surgical instruments by vat photopolymerization technique. In addition, it also raised awareness in excessive gamma sterilization in the medical graded vat photopolymerization parts.
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Tristan Schlotthauer, Jan Nitsche and Peter Middendorf
During post-processing of stereolithography photopolymers, the limited penetration depth of ultraviolet (UV) light can lead to inhomogeneous cross-linking. This is a major problem…
Abstract
Purpose
During post-processing of stereolithography photopolymers, the limited penetration depth of ultraviolet (UV) light can lead to inhomogeneous cross-linking. This is a major problem in part design for industrial applications as this creates uncertainty regarding the mechanical load capacity. Therefore, this paper aims to present an experimental method to measure the post-curing depth in stereolithography photopolymers.
Design/methodology/approach
Printed specimens made from urethane acrylate photopolymers are placed in a protective housing and are exposed on one side to UV light during post-processing. A depth profile of the hardness according to ASTM D2240 Shore D is determined alongside the specimens. UVA,-B and -C spectra are investigated and the dependence on exposure dose and pigmentation is studied. The results are directly linked to the mechanical properties via tensile tests and validated on an automotive trim part.
Findings
Exposure with a 405 nm light-emitting diode provides the deepest homogenous post-curing depth of 10.5 mm, which depends on the overall exposure dose and pigmentation. If the initially transparent photopolymer is colored with black pigments, post-curing depth is significantly reduced and no homogenous post-curing can be achieved. To obtain comparable mechanical properties by tensile tests, complete cross-linking of the specimen cross-section has to be ensured.
Research limitations/implications
The spatial resolution of the presented measurement method depends on the indenter size and sample hardness. As a result, the resolution of the used setup is limited in the area close to the edges of the specimen.
Originality/value
This paper shows that the spatially resolved hardness measurement provides more information on the post-curing influence than the evaluation of global mechanical properties. The presented method can be used to ensure homogenous cross-linking of stereolithography parts.
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Anna Danielak, Siddharth Singh Chauhan, Aminul Islam, Jacek Andrzejewski and David Bue Pedersen
The purpose of this paper is to evaluate the influence of layer thickness and post-curing temperature on shape memory properties in components manufactured by stereolithography.
Abstract
Purpose
The purpose of this paper is to evaluate the influence of layer thickness and post-curing temperature on shape memory properties in components manufactured by stereolithography.
Design/methodology/approach
Layer thicknesses of 20 and 100 µm and 22 and 45°C for post-curing temperature were selected following the design of experiments approach. Tensile and bending tests were applied for quantitative evaluation of the shape memory effect (SME). Qualitative analysis was performed using complex geometries and computed tomography as a measurement tool. Additionally, the degree of photopolymerization and glass transition temperature (Tg) were evaluated.
Findings
The tensile test resulted in fixity and recovery ratio values close to 100%. In bending, they varied between 97%–111% for fixity and 88%–95% for recovery. The layer thickness was found to have a higher influence on the SME. In complex structures, SME was dependent on geometry and less sensitive to variation in process parameters. The post-curing temperature had a higher influence on the photopolymerization and Tg. Average Tg of 77.5°C was achieved at 45°C, compared to 73.1°C at 22°C.
Originality/value
In the current state of the art in the processing of shape memory polymers with vat photopolymerization typically, the chemical composition or the thermal and deformation patterns are studied. The effect of the processing parameters is, however, not explored. This paper aims to close the research gap and facilitate the process optimization towards high fixing and recovery characteristics.
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Prashant Jindal, Mamta Juneja, Divya Bajaj, Francesco Luke Siena and Philip Breedon
3D printing techniques have been widely used for manufacturing complex parts for various dental applications. For achieving suitable mechanical strength, post-cure processing is…
Abstract
Purpose
3D printing techniques have been widely used for manufacturing complex parts for various dental applications. For achieving suitable mechanical strength, post-cure processing is necessary, where the relative time duration and temperature specification also needs to be defined. The purpose of this study/paper is to assess the effects of post curing conditions and mechanical properties of 3D printed clear dental aligners
Design/methodology/approach
Dental long-term clear resin material has been used for 3D printing of dental aligners using a Formlabs 3D printer for direct usage on patients. Post-curing conditions have been varied, all of which have been subjected to mechanical compression loading of 1,000 N to evaluate the curing effects on the mechanical strength of the aligners.
Findings
The experimental studies provide significant insight into both temperatures and time durations that could provide sufficient compressive mechanical strength to the 3D printed clear dental aligners. It was observed that uncured aligners deformed plastically with large deformations under the loading conditions, whereas aligners cured between 400°C–800°C for 15–20 min deformed elastically before fragmenting into pieces after safely sustaining higher compressive loads between 495 N and 666 N. The compressive modulus ratio for cured aligners ranged between 4.46 and 5.90 as compared to uncured aligners. For shorter cure time durations and lower temperature conditions, an appropriate elevated compressive strength was also achieved.
Originality/value
Based on initial assessments by dental surgeons, suitable customised clear aligners can be designed, printed and cured to the desired levels based on patient’s requirements. This could result in time, energy and unit production cost savings, which ultimately would help to alleviate the financial burden placed on both the health service and their patients.
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Mehdi Kazemi and Abdolreza Rahimi
Stereolithography (SLA) is a broadly used technology in the field of rapid prototyping. One of the disadvantages of SLA is poor mechanical properties of its products. To approach…
Abstract
Purpose
Stereolithography (SLA) is a broadly used technology in the field of rapid prototyping. One of the disadvantages of SLA is poor mechanical properties of its products. To approach the mechanical properties of original part, the mechanical properties of SLA part, such as tensile strength, should be optimized. In this process, there are many parameters that affect the tensile strength of parts. However, the “layer thickness”, “fabrication orientation” and “post curing time” are the most significant ones. Hence, the purpose of this study is to investigate the influence of these parameters on tensile strength of SLA parts.
Design/methodology/approach
According to the obtained results from experiments based on the “full factorial” method, an empirical equation was developed for the tensile strength in terms of the effective parameters by using regression analysis. Considering this empirical equation, the process parameters were optimized to maximize the tensile strength by using genetic algorithm. Finally, the tensile tests of the specimens were simulated via the general-purpose finite element package of ABAQUS.
Findings
The outputs of the numerical simulations were in good agreement with experimental results. Both experimental and numerical results show that the increase of layer thickness and the decrease in post curing time increase the tensile strength. Furthermore, the tensile strength of parts produced in vertical orientation is higher than that of parts produced in horizontal orientation.
Originality/value
This is a complete study about the tensile strength of the SLA parts from experimental and analytical viewpoints.
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J.Y.H. Fuh, L. Lu, C.C. Tan, Z.X. Shen and S. Chew
Rapid prototypes formed using stereolithography (SL) method have to undergo post‐curing to increase their strength and rigidity. This study attempts to reduce, if not eliminate…
Abstract
Rapid prototypes formed using stereolithography (SL) method have to undergo post‐curing to increase their strength and rigidity. This study attempts to reduce, if not eliminate, post‐cure distortion by characterising curing behaviours. Curing (both heat and UV initiated) characteristics of an acrylic‐based photopolymer under actual fabrication conditions were studied using Raman spectroscopy as well as differential scanning calorimetry (DSC) and differential scanning photo‐calorimetry (DSP). Specimens of single photopolymer lines were created using a SL machine. Raman spectroscopy was used to quantify the curing percentage at different areas on the cross‐section of these lines. Curing percentages before and after post‐curing were also obtained from the experiments. Difference in percentage of post‐curing gave an indication of the distortions faced. It was found that uncured and partially cured resins trapped within the photopolymer resulted in inhomogeneity of curing in the specimens causing shrinkage and distortion.
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D. Karalekas and D. Rapti
This paper presents an experimental study undertaken to determine the polymerisation‐induced residual stresses generated in stereolithography (SL) built test specimens, by using…
Abstract
This paper presents an experimental study undertaken to determine the polymerisation‐induced residual stresses generated in stereolithography (SL) built test specimens, by using the hole‐drilling strain gage method of stress relaxation. Experimentally measured strains, using special three‐element strain gage rosettes, were input into the blind‐hole analysis to calculate the induced residual stresses. The mechanical properties of resin specimens fabricated by the solidification process using an epoxy based photopolymer and post‐cured under ultraviolet (UV) and thermal exposure were determined and incorporated into the subsequent drill‐hole analysis. The effect of the pre‐selected fabrication parameters (hatching space and curing depth) and subsequent by the post‐curing procedure (UV, thermal curing) on the magnitude of the recorded strains is also presented.
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Huachao Mao, Wenxuan Jia, Yuen-Shan Leung, Jie Jin and Yong Chen
This paper aims to present a multi-material additive manufacturing (AM) process with a newly developed curing-on-demand method to fabricate a three-dimensional (3D) object with…
Abstract
Purpose
This paper aims to present a multi-material additive manufacturing (AM) process with a newly developed curing-on-demand method to fabricate a three-dimensional (3D) object with multiple material compositions.
Design/methodology/approach
Unlike the deposition-on-demand printing method, the proposed curing-on-demand printheads use a digital light processing (DLP) projector to selectively cure a thin layer of liquid photocurable resin and then clean the residual uncured material effectively using a vacuuming and post-curing device. Each printhead can individually fabricate one type of material using digitally controlled mask image patterns. The proposed AM process can accurately deposit multiple materials in each layer by combining multiple curing-on-demand printheads together. Consequently, a three-dimensional object can be fabricated layer-by-layer using the developed curing-on-demand printing method.
Findings
Effective cleaning of uncured resin is realized with reduced coated resin whose height is in the sub-millimeter level and improved vacuum cleaning performance with the uncleaned resin less than 10 µm thick. Also, fast material swapping is achieved using the compact design of multiple printheads.
Originality/value
The proposed multi-material stereolithography (SL) process enables 3D printing components using more viscous materials and can achieve desired manufacturing characteristics, including high feature resolution, fast fabrication speed and low machine cost.
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C.M. Cheah, J.Y.H. Fuh, A.Y.C. Nee and L. Lu
The effects of the addition of short glass fibers into an acrylic‐based photo‐polymer (De Solite SCR310) used in the laser solidification process have been studied. Comparisons of…
Abstract
The effects of the addition of short glass fibers into an acrylic‐based photo‐polymer (De Solite SCR310) used in the laser solidification process have been studied. Comparisons of the mechanical properties between pure‐polymer specimens and their fiber‐filled counterparts were made by subjecting the parts to tensile tests. It was observed that the fiber‐reinforced specimens yielded higher measured values of elastic modulus and ultimate tensile strength. The amount of shrinkage encountered by the reinforced prototypes during post‐curing was also found to be less than their non‐reinforced counterparts. It was also found that the mechanical properties of the post‐cured fiber‐reinforced specimens were functions of the layer pitch and laser exposure density used during fabrication. By increasing the laser exposure density and decreasing the layer pitch, the mechanical properties of the post‐cured fiber‐reinforced prototype can be improved, leading to the realization of end products with higher mechanical strengths and better dimensional accuracy.
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M. Kazemi and A.R. Rahimi
– The purpose of this study is to investigate the influences of the supports on tensile strength (TS) of stereolithography (SL) parts.
Abstract
Purpose
The purpose of this study is to investigate the influences of the supports on tensile strength (TS) of stereolithography (SL) parts.
Design/methodology/approach
The shape of specimens (tensile specimens) is according to the American Society Testing and Materials (ASTM) D638 standard. Some parts have support trace on one side and some have support trace on both sides. To achieve this target, some parts are fabricated on other parts; therefore, support of the upper part is fabricated on upper face of lower part.
Findings
Influences of supports traces on mechanical properties aren’t “zero”. Supports affect TS of SL parts by affecting surface roughness of parts. After experimentation and analyzing experimental results, it is concluded that the TS of the parts which have support on both sides is slightly lower than the parts which have support just on one side.
Originality/value
This is the first attempt toward investigation of supports effects on the mechanical properties in SL parts.
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