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Article
Publication date: 1 September 1995

B. Van der Schueren and J.P. Kruth

Selective metal powder sintering is a layer‐by‐layer manufacturing system producing metallic parts with good mechanical properties. Describes why an Fe‐Cu powder mixture has been…

2629

Abstract

Selective metal powder sintering is a layer‐by‐layer manufacturing system producing metallic parts with good mechanical properties. Describes why an Fe‐Cu powder mixture has been selected as the basic material for the process. Deals with the powder deposition issue and proposes a mechanism which can deposit thin powder layers on top of a recipient. Shows that the powder deposition mainly depends on the powder properties. States that the required powder properties are partially compatible with the specifications set by the technology of selective sintering but that some properties are in conflict with one another. Discusses the resulting compromises needed in the powder mixtures and the required modifications to the deposition mechanism.

Details

Rapid Prototyping Journal, vol. 1 no. 3
Type: Research Article
ISSN: 1355-2546

Keywords

Article
Publication date: 15 June 2010

Cheekur Krishnamurthy Srinivasa, Chinnakurli Suryanarayana Ramesh and S.K. Prabhakar

The purpose of this paper is to study the effect of blending time, SiC content and fill ratio on the homogeneity of iron‐silicon carbide powder mixture, blended in double‐cone…

1143

Abstract

Purpose

The purpose of this paper is to study the effect of blending time, SiC content and fill ratio on the homogeneity of iron‐silicon carbide powder mixture, blended in double‐cone blender; to evaluate density, microstructure and micro hardness of laser sintered iron and iron‐SiC specimens; and study the feasibility of building a complex iron‐SiC metal matrix composite (MMC) part by direct metal laser sintering (DMLS) process.

Design/methodology/approach

The morphology and particle size of iron and silicon carbide powders were evaluated. Nickel coating was carried out on silicon carbide particles. Blending of iron‐SiC powders were carried out in two phases in a double‐cone blending equipment. In the first phase, three tests were conducted with fill ratios (ratio of volume of conical blender to volume of powder mixture) of 1.68, 3.39, and 6.8 percent while iron‐SiC weight ratio was kept constant at 97:3. In the second phase, four tests were conducted with iron‐SiC weight ratios of 99:1, 98:2, 97:3, and 95:5 while keeping a constant fill ratio of 1.68 percent. In both the phases, blending was carried out for duration of 43 minutes. Homogeneity of the powder mixture was evaluated at different intervals of time by adopting sampling process. Sintering was carried out on iron and iron‐SiC powder mixture using DMLS machine at laser speed of 50, 75, 100, and 125 mm/s. Microstructure, density and micro hardness studies were carried out on the sintered specimens. A 3D model of a part with complex geometry was modeled using Unigraphics CAD/CAM software and prototype part was built by DMLS technology using the blended iron‐2 weight percent SiC powder.

Findings

A reduction in blending time was observed with increase in SiC content and decrease in fill ratio. Microstructure and micro hardness tests conducted on laser sintered iron‐silicon carbide specimens, reveal the homogeneity of blended powder. The density of the iron‐SiC composites sintered at a laser speed of 50 and 75 mm/s, decreased with increase in SiC content. Further, an increase in the micro hardness of iron‐SiC composites was observed with increase in SiC content and decrease in laser speed. Complex functional part was built by DMLS technology with out any supports.

Research limitations/implications

The experiments were conducted with standard blending equipment in which the speed is limited to 48 revolutions per minute only.

Originality/value

Meager information is available on blending of powders for producing MMCs by laser sintering process. The work presented in this paper will be a guideline for researchers to carry out further work in blending of powders for producing MMCs by rapid prototyping process.

Details

Rapid Prototyping Journal, vol. 16 no. 4
Type: Research Article
ISSN: 1355-2546

Keywords

Article
Publication date: 20 September 2021

Jared Allison, John Pearce, Joseph Beaman and Carolyn Seepersad

Additive manufacturing (AM) of thermoplastic polymers for powder bed fusion processes typically requires each layer to be fused before the next can be deposited. The purpose of…

Abstract

Purpose

Additive manufacturing (AM) of thermoplastic polymers for powder bed fusion processes typically requires each layer to be fused before the next can be deposited. The purpose of this paper is to present a volumetric AM method in the form of deeply penetrating radio frequency (RF) radiation to improve the speed of the process and the mechanical properties of the polymer parts.

Design/methodology/approach

The focus of this study was to demonstrate the volumetric fusion of composite mixtures containing polyamide (nylon) 12 and graphite powders using RF radiation as the sole energy source to establish the feasibility of a volumetric AM process for thermoplastic polymers. Impedance spectroscopy was used to measure the dielectric properties of the mixtures as a function of increasing graphite content and identify the percolation limit. The mixtures were then tested in a parallel plate electrode chamber connected to an RF generator to measure the heating effectiveness of different graphite concentrations. During the experiments, the surface temperature of the doped mixtures was monitored.

Findings

Nylon 12 mixtures containing between 10% and 60% graphite by weight were created, and the loss tangent reached a maximum of 35%. Selective RF heating was shown through the formation of fused composite parts within the powder beds.

Originality/value

The feasibility of a novel volumetric AM process for thermoplastic polymers was demonstrated in this study, in which RF radiation was used to achieve fusion in graphite-doped nylon powders.

Article
Publication date: 1 May 2003

Nikolay Tolochko, Sregei Mozzharov, Tahar Laoui and Ludo Froyen

A comparative characterisation of selective laser sintering (SLS) mechanisms of single‐ and two‐component powders is presented. The effects of the volume fraction of liquid phase…

1810

Abstract

A comparative characterisation of selective laser sintering (SLS) mechanisms of single‐ and two‐component powders is presented. The effects of the volume fraction of liquid phase and the powder absorptance were discussed. Single‐component Ni‐alloy, Fe and Cu powders as well as two‐component powder systems based on Ni‐alloy, Fe and Cu were investigated. In particular, the following types of two‐component powder systems were studied: Ni‐alloy‐Cu and Fe‐Cu powder mixtures as well as Cu‐coated Ni‐alloy powder and Cu‐coated Fe powders. SLS experiments were performed with a CW‐ Nd:YAG laser (λ=1.06 μm). The acting mechanism in all cases was liquid phase sintering.

Details

Rapid Prototyping Journal, vol. 9 no. 2
Type: Research Article
ISSN: 1355-2546

Keywords

Article
Publication date: 13 January 2012

Jialin Yang, Hongwu Ouyang, Chao Xu and Yang Wang

The purpose of this paper is to describe the stability and properties of the direct metal laser fabrication (DMLF) process, by putting forward top surface quality (TSQ), which…

1131

Abstract

Purpose

The purpose of this paper is to describe the stability and properties of the direct metal laser fabrication (DMLF) process, by putting forward top surface quality (TSQ), which could be a unique and crucially important feature compared with traditional manufacturing methods.

Design/methodology/approach

Through the systematic and detailed analysis of DMLF process using related theories of additive manufacturing technologies, it was revealed that TSQ was the key factor for controlling the stability of DMLF process and thus tailoring final properties of metallic parts. Only good TSQ can ensure the stability of DMLF process and excellent performance of metal parts in theory.

Findings

TSQ was defined as the surface morphology in macro and micro scopes in laser scanning area of unit layers during DMLF, and could be characterized by three key elements: flatness, compactness and cleanliness. The flatness was the significant factor to assure the shaping during DMLF, while the compactness and cleanliness were the decisive factors to assure the final properties of metal part for DMLF. As an example, the typical top surface defects and their contributing factors in DMLF for Cu‐based metal powder mixtures were investigated thoroughly according to the proposed definition and requirements. Moreover, the specific controlling methods of TSQ were provided and discussed. Eventually, DMLF of three‐dimensional Cu‐based metal sample with complicate structure was successfully performed by taking some effective measures for adjusting TSQ parameters.

Originality/value

Few comprehensive investigations have been carried out on this topic. The definition and evaluation methods of TSQ for DMLF have been introduced for the first time in the present paper.

Article
Publication date: 18 January 2016

Ming Fang and Baijin Chen

The purpose of this paper is to report the investigation on obtaining a high-porosity Cu-based structure which was sintered successfully using direct laser sintering and to reveal…

Abstract

Purpose

The purpose of this paper is to report the investigation on obtaining a high-porosity Cu-based structure which was sintered successfully using direct laser sintering and to reveal the mechanisms of obtaining high porosity and acceptable strength simultaneously as well as the effect of NaCl content on characteristics of the sintered samples.

Design/methodology/approach

Experimental study has been performed. The powder mixture utilized in this experiment includes metal powder (Cu and Cu3P mixture) and porogen [sodium chloride (NaCl)]. Scanning electron microscope, energy-dispersive X-ray analysis and the Archimedes density measurement were used to detect the characteristics of the sintered sample and to reveal the mechanism of forming high porosity and strength structure.

Findings

More than 57 per cent porosity can be achieved while the structural strength is acceptable, and the infiltrated experiment verifies the pores in the structure are inter-connected. During laser sintering, NaCl powder melts and brings a larger amount of liquid phase, inducing large rearrange force and fast rearrangement of Cu particles. Therefore, after NaCl is removed, the dense and strong longer-bar shape tracks with larger amount of pores in the microstructure can be obtained. The size of pores as well as the porosity of the sintered sample increase with the NaCl content in the powder mixture.

Originality/value

The mechanism of obtaining high porosity and acceptable strength simultaneously was revealed. The effect of NaCl content on characteristics of the sintered samples was also disclosed.

Details

Rapid Prototyping Journal, vol. 22 no. 1
Type: Research Article
ISSN: 1355-2546

Keywords

Article
Publication date: 12 January 2021

Ifeanyichukwu Donald Olumor, Lee Geuntak and Eugene Olevsky

The purpose of this study is to investigate the effect of two unique processing routes (solvent jetting (SJ) and binder jetting (BJ)), on the green density of printed stainless…

Abstract

Purpose

The purpose of this study is to investigate the effect of two unique processing routes (solvent jetting (SJ) and binder jetting (BJ)), on the green density of printed stainless steel 316L (SS316L) and Nickel (Ni) powders.

Design/methodology/approach

In the SJ processing route, a solvent is jetted unto the powder/binder mixture to selectively activate the binder, layer by layer. In the BJ processing route, a solution of the binder mixture is jetted onto the powder bed to selectively bind powder particles. The effects of printing parameters such as layer height, roller speed, shaker speed and nozzle temperature on the green density of printed components are investigated and compared for both processing routes.

Findings

Results show that layer height and nozzle temperature affect the relative density of the printed compact for both processing routes. Slightly higher relative densities were achieved via the SJ route, with the overall highest relative density being 42.7% at 100 µm layer height and 70% nozzle temperature for the SS316L components and 43.7% at 150 µm layer height and 90% nozzle temperature for the Ni components, respectively. Results also show an increase in the final sintered relative density with an increase in green (printed) relative density of the solvent jetted SS316L components, with the highest relative density being 87.2%.

Originality/value

The paper studies the influence of printing parameters on the green density of printed SS316L and Ni samples in an unprecedented effort to provide a comparative understanding of the process-property relationships in BJ and SJ of SS316L and Ni components to the additive manufacturing research community.

Details

Rapid Prototyping Journal, vol. 27 no. 2
Type: Research Article
ISSN: 1355-2546

Keywords

Article
Publication date: 1 December 2003

J.P. Kruth, X. Wang, T. Laoui and L. Froyen

Selective laser sintering (SLS) is one of the most rapidly growing rapid prototyping techniques (RPT). This is mainly due to its suitability to process almost any material…

18511

Abstract

Selective laser sintering (SLS) is one of the most rapidly growing rapid prototyping techniques (RPT). This is mainly due to its suitability to process almost any material: polymers, metals, ceramics (including foundry sand) and many types of composites. The material should be supplied as powder that may occasionally contain a sacrificial polymer binder that has to be removed (debinded) afterwards. The interaction between the laser beam and the powder material used in SLS is one of the dominant phenomena that defines the feasibility and quality of any SLS process. This paper surveys the current state of SLS in terms of materials and lasers. It describes investigations carried out experimentally and by numerical simulation in order to get insight into laser‐material interaction and to control this interaction properly.

Details

Assembly Automation, vol. 23 no. 4
Type: Research Article
ISSN: 0144-5154

Keywords

Article
Publication date: 12 August 2014

Cijun Shuai, Jingyu Zhuang, Shuping Peng and Xuejun Wen

The paper aims to fabricate an α-tricalcium phosphate (TCP) scaffold with an interconnected porous structure via selective laser sintering (SLS). To inhibit the phase…

Abstract

Purpose

The paper aims to fabricate an α-tricalcium phosphate (TCP) scaffold with an interconnected porous structure via selective laser sintering (SLS). To inhibit the phase transformation from β- to α-TCP in fabrication process of porous scaffolds, a small amount (1 weight per cent) of poly (L-lactic acid) (PLLA) is added into β-TCP powder to introduce the transient liquid phase.

Design/methodology/approach

The paper opted for the transient liquid phase of melting PLLA to decrease the sintering temperature in SLS. Meanwhile, the densification of β-TCP is enhanced with a combined effect of the capillary force caused by melting PLLA and the surface energy of β-TCP particles. Moreover, the PLLA will gradually decompose and completely disappear with laser irradiation.

Findings

The testing results show the addition of PLLA enables the scaffolds to achieve a higher β-TCP content of 77 ± 1.49 weight per cent compared with the scaffold sintered from β-TCP powder (60 ± 1.65 weight per cent), when the laser energy density is 0.4 J/mm2. The paper provides the mechanism of PLLA inhibition on the phase transformation from β- to α-TCP. And the optimum sintering parameters are obtained based on experimental results, which are used to prepare a TCP scaffold with an interconnected porous structure via SLS.

Research limitations/implications

This paper shows that the laser energy density is an important sintering parameter that can provide the means to control the micro-porous structure of the scaffold. If the laser energy density is too low, the densification is not enough. On the other hand, if the laser energy density is too high, the microcracks are observed which are attributed to the volume expansion during the phase transformation from β- to α-TCP. Therefore, the laser energy density must be optimized.

Originality/value

The paper provides a feasible method for fabricating TCP artificial bone scaffold with good biological and mechanical properties.

Details

Rapid Prototyping Journal, vol. 20 no. 5
Type: Research Article
ISSN: 1355-2546

Keywords

Article
Publication date: 1 February 2005

J‐P. Kruth, P. Mercelis, J. Van Vaerenbergh, L. Froyen and M. Rombouts

This paper provides an overview of the different binding mechanisms in selective laser sintering (SLS) and selective laser melting (SLM), thus improving the understanding of these…

31107

Abstract

Purpose

This paper provides an overview of the different binding mechanisms in selective laser sintering (SLS) and selective laser melting (SLM), thus improving the understanding of these processes.

Design/methodology/approach

A classification of SLS/SLM processes was developed, based on the binding mechanism occurring in the process, in contrast with traditional classifications based on the processed material or the application. A broad range of commercial and experimental SLS/SLM processes – found from recent articles as well as from own experiments – was used to explain the different binding mechanism categories.

Findings

SLS/SLM processes can be classified into four main binding mechanism categories, namely “solid state sintering”, “chemically induced binding”, “liquid phase sintering – partial melting” and “full melting”. Most commercial processes can be classified into the latter two categories, which are therefore subdivided. The binding mechanism largely influences the process speed and the resulting part properties.

Research limitations/implications

The classification presented is not claimed to be definitive. Moreover some SLM/SLM processes could be classified into more than one category, based on personal interpretation.

Originality/value

This paper can be a useful aid in understanding existing SLS/SLM processes. It can also serve as an aid in developing new SLS/SLM processes.

Details

Rapid Prototyping Journal, vol. 11 no. 1
Type: Research Article
ISSN: 1355-2546

Keywords

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