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The reliable performance of critical components working under extreme conditions is paramount to the safe operation of aircraft, and material selection is critical. Copper alloys are an obvious choice for such applications whenever a combination of transport, mechanical and tribological properties is required. However, low strength and hardness issues require development of new copper alloys and composites to improve service life and reliability. This study aims to investigate the effect of carbon nanotubes as reinforcement phase in copper-matrix composites.

The development of novel copper-based composites refined to the nanoscale was envisaged through mechanical milling of mixtures containing copper and carbon nanotubes (2 Wt.%). Milling took place in a planetary ball mill for times varying between 1 h and 16 h at 400 rpm. A ball-to-powder ratio of 20:1 and alumina vial and copper spheres were used under dry conditions or with addition of isopropyl alcohol. Scanning electron microscopy/energy dispersive spectroscopy, size distribution, Raman spectroscopy and X-ray diffraction were used to study the produced powders.

Attained results show that mechanical milling of the studied system produces nanostructured powders containing second-phase carbon nanotubes homogeneously distributed in the metallic matrix, together with severe copper grain refinement. This should correspond to increased residual microstresses, envisaging significant improvement of mechanical properties of the produced copper composites.

The novelty of the work resides in the use of carbon nanotubes for the reinforcement of copper, and on the systematic microstructural characterisation of the produced composites.

This paper aims to present the way of modifying surfaces of 316L stainless steel elements that were manufactured in the selected laser melting (SLM) technology and then subjected to mechanical and electrolytic processing (electropolishing [EP]). The surface of the as-generated and commercial produced parts was modified by grinding and EP, and the results were compared. The authors also present an example of the application of EP for the final processing of a sample technological model – an initial prototype of a 316L steel implant manufactured in the SLM technology.

The analyzed properties included surface topography, roughness, resistance to corrosion, microhardness and the chemical composition of the surface before and after EP. The roughness described with the Ra, Rt and Rz was determined before and after EP of samples manufactured from 316L steel with use of traditional methods and additive technologies.

EP provides us with the opportunity to process elements with a complex structure, which would not be possible with use of other methods (such as milling or grinding). Depending on the expected final surface of elements after the SLM process, it is possible to reduce the surface roughness with the use of EP (for t = 20 min, Ra = 3.53 ± 0.37 µm and for t = 40 min, Ra = 3.23 ± 0.22 µm) or mechanical processing and EP (for t = 4 min, Ra = 0.13 ± 0.02 µm). The application of the EP method to elements made from 316L steel, in a bath consisting of sulfuric acid (VI), H2SO4 (35 Vol.%), phosphoric acid (V), H3PO4 (60.5 Vol.%) and triethanolamine 99 per cent (4.5 Vol.%), allows us to improve the surface smoothness and to obtain a value of the Ra parameter ranging from 0.11 to 0.15 µm. The application of a current density of 20 A/dm2 and a bath temperature of 55ºC results in an adequate smoothing of the surface (Ra < 0.16 µm) for both cold rolled and SLM elements after grinding. The application of EP, to both cold rolled elements and those after SLM, considerably improves the resistance to corrosion. The results of potentiodynamic corrosion resistance tests (jkor, EKA and Vp) of the 316L stainless steel samples demonstrate that the values of Vp for elements subjected to EP (commercial material: 1.3·10-4 mm/year, SLM material: 3.5·10-4 mm/year) are lower than for samples that were only ground (commercial material: 4.0·10-4 mm/year, SLM material: 9.6·10-4 mm/year). The microhardness was found to be significantly higher in elements manufactured using SLM technology than in those cold rolled and ground. The ground 316L steel samples were characterized by a microhardness of 318 HV (cold rolled) and 411 HV (SLM material), whereas the microhardness of samples subjected to EP was 230 HV (commercial material) and 375 HV (SLM material).

The 316L samples were built by SLM method. The surface of the SLM samples was modified by EP. Surface morphological changes after EP were studied using optical methods. Potentiodynamic tests enabled to notice changes in the corrosion resistance of 316L. Microhardness results after electropolished 316L stainless steel were shown. The chemical composition of 316L surface samples was presented. The smoothening of the surface amounted to Ra = 0.16 µm.

This work aims to analyze the effect of mechanical activation on structural disordering (amorphization) in an alumina-silica ceramics system and formation of mullite most notably at a lower temperature using X-ray diffraction (XRD). Also, an objective of this work is to focus on a low-temperature fabrication route for the production of mullite powders.

A batch composition of kaolin, alumina and silica was manually pre-milled and then mechanically activated in a ball mill for 30 and 60 min. The activated samples were sintered at 1,150°C for a soaking period of 2 h. Mullite formation was characterized by XRD and scanning electron microscopy (SEM).

It was determined that the mechanical activation increased the quantity of the mullite phase. SEM results revealed that short milling times only helped in mixing of the precursor powders and caused partial agglomeration, while longer milling times, however, resulted in greater agglomeration.

It is noted that, a manual pre-milling of approximately 20 min and a ball milling approach of 60 min milling time can be suggested as the optimum milling time for the temperature decrease succeeded for the production of mullite from the specific stoichiometric batch formed.

During the operation of nickel-based alloys as blades and discs in turbines, the sliding activity between metallic surfaces is subjected to structural and compositional changes. In as much as friction and wear are influenced by interacting surfaces, it is necessary to investigate these effects. This study aims to understand better the mechanical and tribological characteristics of Ni-17Cr-10X (X = Mo, W, Ta) ternary alloy systems developed via spark plasma sintering (SPS) technique.

Nickel-based ternary alloys were fabricated via SPS technique at 50 MPa, 1100 °C, 100 °C/min and a dwell time of 10 mins. Scanning electron microscopy, X-Ray diffraction, energy dispersive X-ray spectroscopy, nanoindentation techniques and tribometer were used to assess the microstructure, phase composition, elemental dispersion, mechanical and tribological characteristics of the sintered nickel-based alloys.

The outcome of the investigation showed that the Ni-17Cr10Mo alloy exhibited the highest indentation hardness value of 8045 MPa, elastic modulus value of 386 GPa and wear resistance. At the same time, Ni-17Cr10W possessed the least mechanical and wear properties.

It can be shown that the SPS technique is efficient in the development of nickel-based alloys with good elemental distribution and without defects such as segregation of alloying elements, non-metallic inclusions. This is evident from the scanning electron microscopy micrographs.

The paper aims to examine the mechanical and wear performance of A356/Al₂O₃ (alumina) nanocomposites. The correlation between wear performance and the microstructural properties that result from various mechanical milling periods was investigated.

The production of nano alumina reinforced (1 Wt.%) A356 aluminum nanocomposite specimens was carried out using the traditional powder metallurgy method, incorporating three different mechanical milling times (1, 2 and 4 h). Subsequently, mechanical and wear performance assessments were conducted using hardness, compression and pin-on-disc wear tests.

Although the specimens subjected to the most prolonged mechanical milling (4 h) demonstrated superior hardness and compressive strength properties, they exhibited a remarkable weight loss during the wear tests. The traditional evaluation, which supports that the wear performance is generally correlated with hardness, does not consider the microstructural properties. Since the sample milled for 1 h has a moderate microstructure, it showed better wear performance than the sample with higher hardness.

The originality of the paper is demonstrated through its evaluation of wear performance, incorporating not only hardness but also the consideration of microstructural properties resulted from mechanical milling.

The peer review history for this article is available at: https://publons.com/publon/10.1108/ILT-02-2023-0031/

This paper aims to produce hybrid reinforcement for the development of aluminium matrix composites using ball-billing technique to avoid or reduce the problem of agglomeration of the reinforcement during casting.

In the present investigation, a mixture of silicon carbide (SiC) and rice husk ash (RHA) powder in equal weight percentage ratio 4:4 (1:1) was alloyed mechanically in a ball-mill at distinct milling times of 15, 30, 45, 60 and 75 h. Morphological Characterization and density measurements of the ball-milled powder were carried out after different intervals of milling times.

The results revealed that the process of ball milling is a novel technique for the conversion of two or more powders in to an integer powder and reduces the problem of agglomeration also. The density measurement results revealed that an increasing trend of density initially and reduction of the density with the increase of milling time. The density value of the combined particles became comparable to the density of aluminium at the milling time of 75 h for the equal weight percentage ratio 4:4 (1:1) of SiC and RHA.

The manuscript highlights the research work related to the development of the reinforcement for the aluminium hybrid composites by ball milling process. The use of this process for the development of the reinforcement not only reduces the problem of the agglomeration but reduces the density mismatch of the reinforcement and matrix material also.

This study aims to investigate the effects of ball–material ratio on the properties of mixed powders and Cu-Bi self-lubricating alloy materials.

Cu-Bi mixed powder was ball milled at different ball–material ratios, and the preparation of Cu-Bi alloy materials was achieved through powder metallurgy technology. Scanning electron microscopy, X-ray diffraction and Raman spectroscopy were conducted to study the microstructure and phase composition of the mixed powder. The apparent density and flow characteristics of mixed powders were investigated using a Hall flowmeter. Tests on the crushing strength, impact toughness and tribological properties of self-lubricating alloy materials were conducted using a universal electronic testing machine, 300 J pendulum impact testing machine and M200 ring-block tribometer, respectively.

With the increase in ball–material ratio, the spherical copper matrix particles in the mixed powder became lamellar, the mechanical properties of the material gradually reduced, the friction coefficient of the material first decreased and then stabilized and the wear rate decreased initially and then increased. The increase in the ball–material ratio resulted in the fine network distribution of the Bi phase in the copper alloy matrix, which benefitted its enrichment on the worn surface for the formation a lubricating film and improvement of the material’s tribological performance. However, a large ball–material ratio can excessively weaken the mechanical properties of the material and reduce its wear resistance.

The effects of ball–material ratio on Cu-Bi mixed powder and material properties were clarified. This work provides a reference for the mechanical alloying process and its engineering applications.

The purpose of this study is to reveal the friction reduction performance and mechanism of granular flow lubrication during the milling of difficult-to-machining materials and provide a high-performance lubrication method for the precision cutting of nickel-based alloys.

The milling tests for Inconel 718 superalloy under dry cutting, flood lubrication and granular flow lubrication were carried out, and the milling force and machined surface quality were used to evaluate their friction reduction effect. Furthermore, based on the energy dispersive spectrometer (EDS) spectrums and the topographical features of machined surface, the lubrication mechanism of different granular mediums was explored during granular flow lubrication.

Compared with flood lubrication, the granular flow lubrication had a significant force reduction effect, and the maximum milling force was reduced by about 30%. At the same time, the granular flow lubrication was more conducive to reducing the tool trace size, repressing surface damage and thus achieving better surface quality. The soft particles had better friction reduction performance than the hard particles with the same particle size, and the friction reduction performance of nanoscale hard particles was superior to that of microscale hard particles. The friction reduction mechanism of MoS₂ and WS₂ soft particles is the mending effect and adsorption film effect, whereas that of SiO₂ and Al₂O₃ hard particles is mainly manifested as the rolling and polishing effect.

Granular flow lubrication was applied in the precision milling of Inconel 718 superalloy, and a comparative study was conducted on the friction reduction performance of soft particles (MoS₂, WS₂) and hard particles (SiO₂, Al₂O₃). Based on the EDS spectrums and topographical features of machined surface, the friction reduction mechanism of soft and hard particles was explored.

The purpose of this paper is to focus on the fabrication of SAC nanocomposites solder and discuss the effects of nanoCu addition on the structure and properties of resulted nanocomposite solder.

Ball milling is a nonequilibrium processing technique for producing composite metal particles with submicron homogeneity by the repeated cold welding and fracture of powder particles. This method is believed to offer good processablity, precise control over the solder composition, and produce more homogeneous mixture.

It is found that the melting temperature, the wetting behaviour, and hardness are improved when the Cu nanoparticles are added.

So far, no work has been done on the preparation of Cu nanoparticle added composite by ball milling. This paper presents the fabrication of Sn‐Ag‐Cu nanocomposite solders in a planetary ball mill process, and the data are compared with related researches done.

This study aims to use nanofluid-based minimum quantity lubrication (NMQL) technique to minimize the use of cutting fluids in machining of Inconel-625 and Stainless Steel 304 (SS-304) (Ni-Cr alloys).

Machining of Ni-Cr-based alloys is very challenging as these exhibit lower thermal conductivity and rapid work hardening. So, these cannot be machined dry, and a suitable cutting fluid has to be used. To improve the thermal conductivity of cutting fluid, multi-walled carbon nanotubes (MWCNTs) were added to the soybean oil and used with MQL. This study attempts to compare tool wear of coated carbide inserts during face milling of Inconel-625 and SS-304 under dry, flooded and NMQL conditions. The machining performance of both materials, i.e. Inconel-625 and SS-304, has been compared on the basis of tool wear behavior evaluated using scanning electron microscopy-energy dispersive spectroscopy.

The results indicate higher tool wear and lower tool life during machining of Inconel-625 as compared to SS-304. Machining of Inconel-625 exhibited non-consistent tool wear behavior. The tool failure modes experienced during dry machining are discrete fracture, cracks, etc., which are completely eliminated with the use of NMQL machining. In addition, less adhesion wear and abrasion marks are noticed as compared to dry and flooded machining, thereby enhancing the tool life.

Inconel-625 and SS-304 have specific applications in aircraft and aerospace industry, where sculptured surfaces of the turbine blades are machined. The results of current investigation will provide a rich data base for effective machining of both materials under variety of machining conditions.

The literature review indicated that majority of research work on MQL machining has been carried out to explore machining of Ni-Cr alloys such as Inconel 718, Inconel 800, AISI4340, AISI316, AISI1040, AISI430, titanium alloys, hardened steel alloys and Al alloys. Few researchers have explored the suitability of nanofluids and vegetable oil-based cutting fluids in metal cutting operation. However, no literature is available on face milling using nanoparticle-based MQL during machining Inconel-625 and SS-304. Therefore, experimental investigation was conducted to examine the machining performance of NMQL during face milling of Inconel-625 and SS-304 by using soybean oil (vegetable oil) with MWCNTs to achieve ecofriendly machining.