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The purpose of this paper is to obtain high-temperature-resistant material with high density and to conduct microstructural investigations of 3D-printed Ni-based alloy 713C specimens.

High-density specimens of Ni-based alloy 713C were obtained by the optimizing selective laser melting (SLM) process parameters and an X-ray diffraction (XRD) analysis confirmed the occurrence of γ and γ′ phases and the presence of carbides in the SLM-manufactured Ni-based alloy 713C. The analysis of electron backscatter diffraction (EBSD) studies suggested a preferred 〈100〉 direction orientation and low angle misorientation for the SLM specimens.

The high-density specimens of Ni-based alloy 713C were obtained by the optimized SLM process parameters. XRD analysis confirmed the presence of γ and γ′ phases and carbides in the SLM-manufactured Ni-based alloy 713C. Analysis of EBSD studies suggested a preferred 〈100〉 direction orientation and low angle misorientation for the SLM specimen.

In this study, 3D-printed Ni-based alloy 713C with a high density of 99% was obtained for the first time, to the best of the authors’ knowledge.

Wire-arc-based additive manufacturing (WAAM) is a promising technology for the efficient and economical fabrication of medium-large components. However, the anisotropic behavior of the multilayered WAAM-fabricated components remains a challenging problem.

The purpose of this paper is to conduct a comprehensive study of the grain morphology, crystallographic orientation and texture in three regions of the WAAM printed component. Furthermore, the interdependence of the grain morphology in different regions of the fabricated component with their mechanical and tribological properties was established.

The electron back-scattered diffraction analysis of the top and bottom regions revealed fine recrystallized grains, whereas the middle regions acquired columnar grains with an average size of approximately 8.980 µm. The analysis revealed a higher misorientation angle and an intense crystallographic texture in the upper and lower regions. The investigations found a higher microhardness value of 168.93 ± 1.71 HV with superior wear resistance in the bottom region. The quantitative evaluation of the residual stress detected higher compressive stress in the upper regions. Evidence for comparable ultimate tensile strength and greater elongation (%) compared to its wrought counterpart has been observed.

The study found a good correlation between the grain morphology in different regions of the WAAM-fabricated component and their mechanical and wear properties. The Hall–Petch relationship also established good agreement between the grain morphology and tensile test results. Improved ductility compared to its wrought counterpart was observed. The anisotropy exists with improved mechanical properties along the longitudinal direction. Moreover, cylindrical components have superior tribological properties compared with cuboidal components.

Super 304HCu super austenitic stainless steel tubes containing 2.3 to 3 (Wt.%) of copper (Cu) is used in superheaters and reheater tubings of nuclear power plants. In general, austenitic stainless steels welded by conventional constant current gas tungsten arc welding (CC-GTAW) produce coarse columnar grains, alloy segregation and may result in inferior mechanical properties. Pulsed current gas tungsten arc welding (PC-GTAW) can control the solidification structure by altering the prevailing thermal gradients in the weld pool.

Super 304HCu tubes of Ø 57.1 mm and the wall thickness of 3.5 mm were autogenously welded using CC and PC-GTAW processes. Joints are characterized using optical microscopy, electron microscopy, energy dispersive spectroscopy and electron backscatter diffraction (EBSD) techniques. Hot tensile properties of the weld joints were evaluated and correlated with their microstructural features.

Current pulsing in GTAW has resulted in minimal eutectic film segregation, lower volume % of delta ferrite and appreciable improvement in tensile properties than CC-GTAW joints.

The EBSD boundary map and inverse pole orientation map of Super 304HCu weld joints evidence the grain refinement and much frequent high angle grain boundaries achieved using weld current pulsing.

Using wire as feedstock has several advantages for additive manufacturing (AM) of metal components, which include high deposition rates, efficient material use and low material costs. While the feasibility of wire-feed AM has been demonstrated, the accuracy and surface finish of the produced parts is generally lower than those obtained using powder-bed/-feed AM. The purpose of this study was to develop and investigate the feasibility of a fine wire-based laser metal deposition (FW-LMD) process for producing high-precision metal components with improved resolution, dimensional accuracy and surface finish.

The proposed FW-LMD AM process uses a fine stainless steel wire with a diameter of 100 µm as the additive material and a pulsed Nd:YAG laser as the heat source. The pulsed laser beam generates a melt pool on the substrate into which the fine wire is fed, and upon moving the X–Y stage, a single-pass weld bead is created during solidification that can be laterally and vertically stacked to create a 3D metal component. Process parameters including laser power, pulse duration and stage speed were optimized for the single-pass weld bead. The effect of lateral overlap was studied to ensure low surface roughness of the first layer onto which subsequent layers can be deposited. Multi-layer deposition was also performed and the resulting cross-sectional morphology, microhardness, phase formation, grain growth and tensile strength have been investigated.

An optimized lateral overlap of about 60-70% results in an average surface roughness of 8-16 µm along all printed directions of the X–Y stage. The single-layer thickness and dimensional accuracy of the proposed FW-LMD process was about 40-80 µm and ±30 µm, respectively. A dense cross-sectional morphology was observed for the multilayer stacking without any visible voids, pores or defects present between the layers. X-ray diffraction confirmed a majority austenite phase with small ferrite phase formation that occurs at the junction of the vertically stacked beads, as confirmed by the electron backscatter diffraction (EBSD) analysis. Tensile tests were performed and an ultimate tensile strength of about 700-750 MPa was observed for all samples. Furthermore, multilayer printing of different shapes with improved surface finish and thin-walled and inclined metal structures with a minimum achievable resolution of about 500 µm was presented.

To the best of the authors’ knowledge, this is the first study to report a directed energy deposition process using a fine metal wire with a diameter of 100 µm and can be a possible solution to improving surface finish and reducing the “stair-stepping” effect that is generally observed for wires with a larger diameter. The AM process proposed in this study can be an attractive alternative for 3D printing of high-precision metal components and can find application for rapid prototyping in a range of industries such as medical and automotive, among others.

The use of a gas metal arc welding-based weld-deposition, referred to as wire-direct energy deposition or wire-arc additive manufacturing, is one of the notable additive manufacturing methods for producing metallic components at high deposition rates. In this method, the near-net shape is manufactured through layer-by-layer weld-deposition on a substrate. However, as a result of this sequential weld-deposition, different layers are subjected to different types of thermal cycles and partial re-melting. The resulting microstructural evolution of the material may not be uniform. Hence, the purpose of this study is to assess microstructure variation along with the lamination direction (or build direction).

The study was carried out for two different boundary conditions, namely, isolated condition and cooled condition. The microstructural evolution across the layers is hypothesized based on experimental assessment; this included microhardness, scanning electron microscopy imaging and electron backscatter diffraction analysis. These conditions subsequently collaborated with the help of thermal modeling of the process.

During a new layer deposition, the previous layer also is subject to re-melt. While the newly added layer undergoes rapid cooling through a combination of convection, conduction and radiation losses, the penultimate layer, sees a slower cooling curve due to its smaller exposure area. This behavior of rapid-solidification and subsequent re-melting and re-solidification is a progressing phenomenon across the layers and the bulk of the layers have uniform grains due to this remelt-re-solidification phenomenon.

This paper studies the microstructure variation along with the build direction for thin-walled components fabricated through weld-deposition. This study would be helpful in addressing the issue of anisotropy resulting from the distinctive thermal history of each layer in the overall theme of metal additive manufacturing.

The unique aspect of this paper is the postulation of a generic hypothesis, based on experimental findings and supported by thermal modeling of the process, for remelt-re-solidification phenomenon followed by temperature raising/lowering repetitively in every layer deposition across the layers. This is implemented for different types of base plate conditions, revealing the role of boundary conditions on the microstructure evolution.

This paper aims to investigate the influence of different post-annealing cooling conditions, i.e. furnace cooling (heat treatment (HT) 1 – slow cooling) and air cooling (HT 2 – fast cooling), on the microstructure and mechanical properties of selective laser melting (SLM) built austenitic 316L stainless steel (SS).

Three sets of 316L SS samples were fabricated using a machine standard scanning strategy. Each set consists of three tensile samples and a cubic sample for microstructural investigations. Two sets were subsequently subjected to annealing HT with different cooling conditions, i.e. HT 1 and HT 2, whereas one set was used in the as-built (AB) condition. The standard metallographic techniques of X-ray diffraction, scanning electron microscopy and electron back-scattered diffraction were used to investigate the microstructural variations induced by different cooling conditions. The resultant changes in mechanical properties were also investigated.

The phase change of SLM fabricated 316L was observed to be independent of the investigated cooling conditions and all samples consist of austenite phase only. Both HT 1 and HT 2 lead to dissolved characteristic melt pools of SLM. Noticeable increase in grain size of HT 1 and HT 2 samples was also observed. Compared with AB samples, the grain size of HT 1 and HT 2 was increased by 12.5% and 50%, respectively. A decreased hardness and strength, along with an increased ductility was also observed for HT 2 samples compared with HT 1 and AB samples.

From previous studies, it has been noticed that most investigations on HT of SLM fabricated 316L were mainly focused on the HT temperature or holding time. However, the post-HT cooling rate is also an equally important factor in deciding the microstructure and mechanical properties of heat-treated components. Therefore, this paper investigates the influence of different post-annealing cooling conditions on microstructure and mechanical properties of SLM fabricated 316L components. This study provides a foundation for considering the post-HT cooling rate as an influential parameter that controls the properties of heat-treated SLM components.

In recent years, additive manufacturing (AM) has started to be used for manufacturing real functional parts and assemblies for critical applications in aerospace, automotive, and machinery industries. Most complex or assembled parts require internal features (IF) such as holes, channels, slots, or guides for locational and mating requirements. Therefore, it is critical to understand and compare the structural and mechanical properties of additively manufactured and conventionally machined IFs.

In this study, mechanical and microstructural properties of Inconel 718 (Inc718) alloy internal features, manufactured either as-built with AM or machining of additively manufactured (AMed) part thereafter were investigated.

The results showed that the average ultimate tensile strength (UTS) of additively manufactured center internal feature (AM-IF) is almost analogous to the machined internal feature (M-IF). However, the yield strength of M-IF is greater than that of AM-IF due the greater surface roughness of the internal feature in AM-IF, which is deemed to surpass the effect of microstructure on the mechanical performance. The results of digital image correlation (DIC) analysis suggest that AM-IF and M-IF conditions have similar strain values under the same stress levels but the specimens with as built IF have a more locally ductile region around their IF, which is confirmed by hardness test results. But this does not change global elongation behavior. The microstructural evolution starting from as-built (AB) and heat-treated (HT) samples to specimens with IF are examined. The microstructure of HT specimens has bimodal grain structure with d phase while the AB specimens display a very fine dendritic microstructure with the presence of carbides. Although they both have close values, machined specimens have a higher frequency of finer grains based on SEM images.

It was shown that the concurrent creation of the IF during AM can provide a final part with a preserved ultimate tensile strength and elongation but a decreased yield strength. The variation in UTS of AM-IF increases due to the surface roughness near the internal feature as compared to smooth internal surfaces in M-IF. Hence, the outcomes of this study are believed to be valuable for the industry in terms of determining the appropriate production strategy of parts with IF using AM and postprocessing processes.

Laser additive manufacturing is widely utilized to fabricate the Ti6Al4V alloy, but it requires post-processing to improve its performance. This paper aims to propose laser peening (LP) as an effective way to improve the surface characteristics of the Ti6Al4V alloy fabricated by direct laser deposition (DLD).

Surface integrity including surface roughness, porosity, residual stress and microhardness are investigated in detail before and after LP treatment. Microstructure evolution is characterized by the electron backscatter diffraction (EBSD) to analyze crystal phase, grain boundary misorientation and texture.

Multiple overlapping layers of LP treatment result in slight influence on the polished surface of DLD-built samples. Porosity measured by the Archimedes test is found to be greatly decreased after LP treatment. Compressive residual stresses are significantly induced, the magnitude of which is greatly increased by increasing layers of LP treatment. And, local weakening or enhancement of residual stress in depth is observed because of pore and inclusion defects in the DLD-built Ti6Al4V alloy. Favorable hardness property can be obtained after multiple overlapping layers of LP treatment. EBSD analysis shows that LP treatment with multiple layers can introduce a large amount of lower-angle boundaries, indicating that dislocations beneath the top surface could induce a strain-hardened layer. The microtexture of the DLD-built Ti6Al4V alloy cannot be eliminated to decrease the anisotropy of the mechanical property.

The variation of porosity observed after LP inside the DLD-built Ti-Al-4V is attractive but requires more detailed work to analyze the evolution of pore geometry.

Surface treatment of an additive manufactured titanium alloy was carried out to improve its fatigue resistance.

This work is original in proposing LP as an effective post process for the surface treatment of an additive manufactured titanium alloy through analyzing the surface integrity and microstructure evolution.

The purpose of this paper is to study the microstructure and mechanical behaviour of smaller microbumps for high density solder interconnects.

The microstructure was analyzed by scanning electron microscopy and electron backscatter diffraction tests to determine the Sn grain number of the resultant microbumps. The nanomechanical properties of Sn microbumps were investigated by the nanoindentation and shearing tests to understand the failure mechanism and assess the reliability of ultra-high density solder interconnects with numbered grains.

Only one Sn grain is observed in the interconnect matrix when the microbumps are miniaturized to 40 μm or less. Because of the body-centred tetragonal lattice of ß-Sn unit cell, the mechanical properties of the one-grain Sn microbumps are remarkably anisotropic, which are proved by the difference of the elastic modulus and the stiffness in the different orientations. The shearing tests show that the one-grain Sn microbump has a typical brittle sliding fracture of monocrystal at different shearing speeds.

The paper provides a comparable study for the performance of the bigger solder joints and also makes preliminary research on the microstructure and mechanical behaviour of Sn microbumps with the diameter of 40 μm.

The findings in this paper provide methods of microstructure study by combination of EBSD test and metallographic analysis, mechanical study by combination of nanoindentation test and shearing test, which can provide good guidelines for other smaller microbumps. The strain rate sensitivity exponent of the one-grain Sn microbumps is consistent with the Pb-free bulk solder. This implies that the one-grain Sn microbump has a comparable flow stress to Sn37Pb solder, which is beneficial for Pb-free replacement in higher density microelectronic packaging.

AlSi10Mg alloy is commonly used in laser powder bed fusion due to its printability, relatively high thermal conductivity, low density and good mechanical properties. However, the thermal conductivity of as-built materials as a function of processing (energy density, laser power, laser scanning speed, support structure) and build orientation, are not well explored in the literature. This study aims to elucidate the relationship between processing, microstructure, and thermal conductivity.

The thermal conductivity of laser powder bed fusion (L-PBF) AlSi10Mg samples are investigated by the flash diffusivity and frequency domain thermoreflectance (FDTR) techniques. Thermal conductivities are linked to the microstructure of L-PBF AlSi10Mg, which changes with processing conditions. The through-plane exceeded the in-plane thermal conductivity for all energy densities. A co-located thermal conductivity map by frequency domain thermoreflectance (FDTR) and crystallographic grain orientation map by electron backscattered diffraction (EBSD) was used to investigate the effect of microstructure on thermal conductivity.

The highest through-plane thermal conductivity (136 ± 2 W/m-K) was achieved at 59 J/mm³ and exceeded the values reported previously. The in-plane thermal conductivity peaked at 117 ± 2 W/m-K at 50 J/mm³. The trend of thermal conductivity reducing with energy density at similar porosity was primarily due to the reduced grain size producing more Al-Si interfaces that pose thermal resistance. At these interfaces, thermal energy must convert from electrons in the aluminum to phonons in the silicon. The co-located thermal conductivity and crystallographic grain orientation maps confirmed that larger colonies of columnar grains have higher thermal conductivity compared to smaller columnar grains.

The thermal properties of AlSi10Mg are crucial to heat transfer applications including additively manufactured heatsinks, cold plates, vapor chambers, heat pipes, enclosures and heat exchangers. Additionally, thermal-based nondestructive testing methods require these properties for applications such as defect detection and simulation of L-PBF processes. Industrial standards for L-PBF processes and components can use the data for thermal applications.

To the best of the authors’ knowledge, this paper is the first to make coupled thermal conductivity maps that were matched to microstructure for L-PBF AlSi10Mg aluminum alloy. This was achieved by a unique in-house thermal conductivity mapping setup and relating the data to local SEM EBSD maps. This provides the first conclusive proof that larger grain sizes can achieve higher thermal conductivity for this processing method and material system. This study also shows that control of the solidification can result in higher thermal conductivity. It was also the first to find that the build substrate (with or without support) has a large effect on thermal conductivity.