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Article
Publication date: 15 January 2020

Lorenzo Dall’Ava, Harry Hothi, Johann Henckel, Anna Di Laura, Sean Bergiers, Paul Shearing and Alister Hart

Three-dimensional (3D) printing is increasingly used to produce orthopaedic components for hip arthroplasty, such as acetabular cups, which show complex lattice porous structures…

Abstract

Purpose

Three-dimensional (3D) printing is increasingly used to produce orthopaedic components for hip arthroplasty, such as acetabular cups, which show complex lattice porous structures and shapes. However, limitations on the quality of the final implants are present; thus, investigations are needed to ensure adequate quality and patients safety. X-ray microcomputed tomography (micro-CT) has been recognised to be the most suitable method to evaluate the complexity of 3D-printed parts. The purpose of this study was to assess the reliability of a micro-CT analysis method comparing it with reference systems, such as coordinate measuring machine and electron microscopy.

Design/methodology/approach

3D-printed acetabular components for hip arthroplasty (n = 2) were investigated. Dimensions related to the dense and porous regions of the samples were measured. The micro-CT scanning parameters (voltage – kV, current – µA) were optimised selecting six combinations of beam voltage and current.

Findings

Micro-CT showed good correlation and agreement with both coordinate measuring machine and scanning electron microscopy when optimal scanning parameters were selected (130 kV – 100 µA to 180 kV – 80 µA). Mean discrepancies of 50 µm (± 300) and 20 µm (± 60) were found between the techniques for dense and porous dimensions. Investigation method such as micro-CT imaging may help to better understand the impact of 3D printing manufacturing technology on the properties of orthopaedic implants.

Originality/value

The optimisation of the scanning parameters and the validation of this method with reference techniques may guide further analysis of similar orthopaedic components.

Details

Rapid Prototyping Journal, vol. 26 no. 3
Type: Research Article
ISSN: 1355-2546

Keywords

Article
Publication date: 28 January 2020

James Robert Wingham, Robert Turner, Joanna Shepherd and Candice Majewski

X-Ray-computed micro-tomography (micro-CT) is relatively well established in additive manufacturing as a method to determine the porosity and geometry of printed parts and, in…

294

Abstract

Purpose

X-Ray-computed micro-tomography (micro-CT) is relatively well established in additive manufacturing as a method to determine the porosity and geometry of printed parts and, in some cases, the presence of inclusions or contamination. This paper aims to demonstrate that micro-CT can also be used to quantitatively analyse the homogeneity of micro-composite parts, in this case created using laser sintering (LS).

Design/methodology/approach

LS specimens were manufactured in polyamide 12 with and without incorporation of a silver phosphate glass additive in different sizes. The specimens were scanned using micro-CT to characterise both their porosity and the homogeneity of dispersion of the additive throughout the volume.

Findings

This work showed that it was possible to use micro-CT to determine information related to both porosity and additive dispersion from the same scan. Analysis of the pores revealed the overall porosity of the printed parts, with linear elastic fracture mechanics used to identify any pores likely to lead to premature failure of the parts. Analysis of the additive was found to be possible above a certain size of particle, with the size distribution used to identify any agglomeration of the silver phosphate glass. The particle positions were also used to determine the complete spatial randomness of the additive as a quantitative measure of the dispersion.

Practical implications

This shows that micro-CT is an effective method of identifying both porosity and additive agglomeration within printed parts, meaning it can be used for quality control of micro-composites and to validate the homogeneity of the polymer/additive mixture prior to printing.

Originality/value

This is believed to be the first instance of micro-CT being used to identify and analyse the distribution of an additive within a laser sintered part.

Details

Rapid Prototyping Journal, vol. 26 no. 4
Type: Research Article
ISSN: 1355-2546

Keywords

Article
Publication date: 18 January 2016

Davood Rouholamin and Neil Hopkinson

The purpose of this study was to assess the suitability of micro-computed tomography as a non-destructive method to investigate the morphology of nylon 12 parts produced by…

666

Abstract

Purpose

The purpose of this study was to assess the suitability of micro-computed tomography as a non-destructive method to investigate the morphology of nylon 12 parts produced by high-speed sintering (HSS). The investigation of the effect of changes in the lamp power on the properties of the fabricated parts was another purpose of this study.

Design/methodology/approach

Nylon 12 parts were manufactured using HSS with various lamp powers. Morphological properties of the parts were measured using micro-computed tomography. Ultimate tensile strength, elongation at break and Young’s modulus of the prepared parts were determined and compared. The effect of lamp power on the properties of the parts was then studied.

Findings

This paper proposes micro-computed tomography as a suitable technique to study the 3D structure of the parts produced by HSS. The effects of lamp power on the properties of the produced parts were also discussed.

Practical implications

The findings could result in an improvement in customisation of the parts for various applications through varying the lamp power. The level of lamp power could be tailored to obtain suitable part properties for a target application.

Originality/value

This study strengthens the fact that HSS is a promising additive manufacturing technique to produce nylon 12 parts, and the properties of the parts could be maximised using a suitable level of lamp power. The results showed that micro-computed tomography could be used as an efficient technique to investigate the morphology of the sintered parts.

Details

Rapid Prototyping Journal, vol. 22 no. 1
Type: Research Article
ISSN: 1355-2546

Keywords

Article
Publication date: 1 February 2004

F. Wang, L. Shor, A. Darling, S. Khalil, W. Sun, S. Güçeri and A. Lau

Successes in scaffold guided tissue engineering require scaffolds to have specific macroscopic geometries and internal architectures to provide the needed biological and…

3656

Abstract

Successes in scaffold guided tissue engineering require scaffolds to have specific macroscopic geometries and internal architectures to provide the needed biological and biophysical functions. Freeform fabrication provides an effective process tool to manufacture many advanced scaffolds with designed properties. This paper reports our recent study on using a novel precision extruding deposition (PED) process technique to directly fabricate cellular poly‐ε_rm;‐caprolactone (PCL) scaffolds. Scaffolds with a controlled pore size of 250 μm and designed structural orientations were fabricated.

Details

Rapid Prototyping Journal, vol. 10 no. 1
Type: Research Article
ISSN: 1355-2546

Keywords

Article
Publication date: 16 January 2017

Yihao Zheng, Yancheng Wang, Roland K. Chen, Sagar Deshpande, Noah S. Nelson, Steven R. Buchman and Albert J. Shih

To obtain a vascularized autologous bone graft by in-vivo tissue transformation, a biocompatible tissue transformation mold (TTM) is needed. An ideal TTM is of high geometric…

Abstract

Purpose

To obtain a vascularized autologous bone graft by in-vivo tissue transformation, a biocompatible tissue transformation mold (TTM) is needed. An ideal TTM is of high geometric accuracy and X-ray radiolucent for monitoring the bone tissue formation. The purpose of this study is to present the TTM design and fabrication process, using 3D reconstruction, stereolithography (SLA) and silicone molding.

Design/methodology/approach

The rat mandible, the targeted bone graft, was scanned by micro-computed tomography (CT). From the micro-CT images, the 3D mandible model was identified and used as the cavity geometry to design the TTM. The TTM was fabricated by molding the biocompatible and radiolucent silicone in the SLA molds. This TTM was implanted in a rat for in vivo tests on its biocompatibility and X-ray radiolucency.

Findings

SLA can fabricate the TTM with a cavity shape that accurately replicates that of the rat mandible. The bone formation inside of the silicone TTM can be observed by X-ray. The TTM is feasible for in vivo tissue transformation for vascularized bone reconstruction.

Research limitations/implications

Research of the dimensional and geometrical accuracy of the TTM cavity is required in the future study of this process.

Practical implications

The TTM fabricated in this presented approach has been used for in-vivo tissue transformation. This technique can be implemented for bone reconstruction.

Originality/value

The precision fabrication of the TTMs for in-vivo tissue transformation into autogenous vascularized bone grafts with complex structures was achieved by using SLA, micro-CT and silicone molding.

Details

Rapid Prototyping Journal, vol. 23 no. 1
Type: Research Article
ISSN: 1355-2546

Keywords

Article
Publication date: 19 January 2015

Eberhard Abele, Hanns A. Stoffregen, Klaus Klimkeit, Holger Hoche and Matthias Oechsner

This paper aims to develop a set of process parameters tailored for lattice structures and test them against standard process (SP) parameters. Selective laser melting (SLM) is a…

1507

Abstract

Purpose

This paper aims to develop a set of process parameters tailored for lattice structures and test them against standard process (SP) parameters. Selective laser melting (SLM) is a commonly known and established additive manufacturing technique and is a key technology in generating intricately shaped lattice structures. However, SP parameters used in this technology have building time and accuracy disadvantages for structures with a low area-to-perimeter ratio, such as thin struts.

Design/methodology/approach

In this research work, body-centred cubic structure specimens are manufactured using adapted process parameters. Central to the adapted process parameters is the positioning of the laser beam, the scan strategy and the linear energy density. The specimens are analysed with X-ray micro-computed tomography for dimensional accuracy. The final assessment is a comparison between specimens manufactured using adapted process parameters and those using SP parameters.

Findings

Standard parameters for lattice structures lead to a significant shift from the nominal geometry. An extensive manufacturing and computation time due to several exposure patterns (e.g. pre-contours, post-contours) was observed. The tailored process parameters developed had good dimensional accuracy, reproducible results and improved manufacturing performance.

Research limitations/implications

The results are based on a distinctive geometry of the lattice structure and a specific material. Future research should be extended to other geometries and materials.

Practical implications

Optimisation of process parameters for the part geometry is a critical factor in improving dimensional accuracy and performance of SLM processes.

Originality/value

This study demonstrates how application-tailored process parameters can lead to superior performance and improved dimensional accuracy. The results can be transferred to other lattice structure designs and materials.

Details

Rapid Prototyping Journal, vol. 21 no. 1
Type: Research Article
ISSN: 1355-2546

Keywords

Article
Publication date: 1 March 2003

Suman Das, Scott J. Hollister, Colleen Flanagan, Adebisi Adewunmi, Karlin Bark, Cindy Chen, Krishnan Ramaswamy, Daniel Rose and Erwin Widjaja

The aim of this research is to develop, demonstrate and characterize techniques for fabricating such scaffolds by combining solid freeform fabrication and computational design…

2974

Abstract

The aim of this research is to develop, demonstrate and characterize techniques for fabricating such scaffolds by combining solid freeform fabrication and computational design methods. When fully developed, such techniques are expected to enable the fabrication of tissue engineering scaffolds endowed with functionally graded material composition and porosity exhibiting sharp or smooth gradients. Results of bio‐compatibility and in vivo implantation are presented.

Details

Rapid Prototyping Journal, vol. 9 no. 1
Type: Research Article
ISSN: 1355-2546

Keywords

Article
Publication date: 24 August 2023

Fatih Yılmaz, Ercan Gürses and Melin Şahin

This study aims to evaluate and assess the elastoplastic properties of Ti-6Al-4V alloy manufactured by Arcam Q20 Plus electron beam melting (EBM) machine by a tensile test…

Abstract

Purpose

This study aims to evaluate and assess the elastoplastic properties of Ti-6Al-4V alloy manufactured by Arcam Q20 Plus electron beam melting (EBM) machine by a tensile test campaign and micro computerized tomography (microCT) imaging.

Design/methodology/approach

ASTM E8 tensile test specimens are designed and manufactured by EBM at an Arcam Q20 Plus machine. Surface quality is improved by machining to discard the effect of surface roughness. After surface machining, hot isostatic pressing (HIP) post-treatment is applied to half of the specimens to remove unsolicited internal defects. ASTM E8 tensile test campaign is carried out simultaneously with digital image correlation to acquire strain data for each sample. Finally, build direction and HIP post-treatment dependencies of elastoplastic properties are analyzed by F-test and t-test statistical analyses methods.

Findings

Modulus of elasticity presents isotropic behavior for each build direction according to F-test and t-test analysis. Yield and ultimate strengths vary according to build direction and post-treatment. Stiffness and strength properties are superior to conventional Ti-6Al-4V material; however, ductility turns out to be poor for aerospace structures compared to conventional Ti-6Al-4V alloy. In addition, micro CT images show that support structure leads to dense internal defects and pores at applied surfaces. However, HIP post-treatment diminishes those internal defects and pores thoroughly.

Originality/value

As a novel scientific contribution, this study investigates the effects of three orthogonal build directions on elastoplastic properties, while many studies focus on only two-build directions. Evaluation of Poisson’s ratio is the other originality of this study. Furthermore, another finding through micro CT imaging is that temporary support structures result in intense defects closer to applied surfaces; hence high-stress regions of structures should be avoided to use support structures.

Details

Rapid Prototyping Journal, vol. 29 no. 10
Type: Research Article
ISSN: 1355-2546

Keywords

Article
Publication date: 19 January 2015

Miguel Castilho, Barbara Gouveia, Inês Pires, Jorge Rodrigues and Manuel Pereira

This paper aims to study the influence of the binder saturation level on the accuracy and on the mechanical properties of three-dimensional (3D)-printed scaffolds for bone tissue…

1092

Abstract

Purpose

This paper aims to study the influence of the binder saturation level on the accuracy and on the mechanical properties of three-dimensional (3D)-printed scaffolds for bone tissue engineering.

Design/methodology/approach

To study the influence of the liquid binder volume on the models accuracy, two quality test plates with different macropore sizes were designed and produced. For the mechanical and physical characterisation, cylindrical specimens were used. The models were printed using a calcium phosphate powder, which was characterised in terms of composition, particle size and morphology, by X-ray diffraction (XRD), laser diffraction and Scanning electron microscopy (SEM) analysis. The sample’s physical characterisation was made using the Archimedes method (porosity), SEM, micro-computer tomography (CT) and digital scan techniques, while the mechanical characterisation was performed by means of uniaxial compressive tests. Strength distribution was analysed using a statistical Weibull approach, and the dependence of the compressive strength on the porosity was discussed.

Findings

The saturation level is determinant for the structural characteristics, accuracy and strength the models produced by three-dimensional printing (3DP). Samples printed with the highest saturation showed higher compressive strengths (24 MPa), which are over the human trabecular bone. The models printed with lower saturations presented the highest accuracy and pore interconnectivity.

Originality/value

This study allowed to acquire important knowledge concerning the effects of shell/core saturation on the overall performance of the 3DP. With this information it is possible to devise scaffolds with the required properties for bone scaffold engineering.

Details

Rapid Prototyping Journal, vol. 21 no. 1
Type: Research Article
ISSN: 1355-2546

Keywords

Article
Publication date: 15 June 2015

Anton Du Plessis, Ruhan Slabbert, Liani Colette Swanepoel, Johan Els, Gerrie J Booysen, Salima Ikram and Izak Cornelius

– The purpose of this paper is to present the first detailed three-dimensional (3D) print from micro-computed tomography data of the skeleton of an ancient Egyptian falcon mummy.

Abstract

Purpose

The purpose of this paper is to present the first detailed three-dimensional (3D) print from micro-computed tomography data of the skeleton of an ancient Egyptian falcon mummy.

Design/methodology/approach

Radiographic analysis of an ancient Egyptian falcon mummy housed at Iziko Museums of South Africa was performed using non-destructive x-ray micro-computed tomography. A 1:1 physical replica of its skeleton was printed in a polymer material (polyamide) using 3D printing technology.

Findings

The combination of high-resolution computed tomography scanning and rapid prototyping allowed us to create an accurate 1:1 model of a biological object hidden by wrappings. This model can be used to study skeletal features and morphology and also enhance exhibitions hosted within the museum.

Originality/value

This is the first replica of its kind made of an ancient Egyptian falcon mummy skeleton. The combination of computed tomography scanning and 3D printing has the potential to facilitate scientific research and stimulate public interest in Egyptology.

Details

Rapid Prototyping Journal, vol. 21 no. 4
Type: Research Article
ISSN: 1355-2546

Keywords

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