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This study aims to focus on the main materials used in consolidation processes of illuminated paper manuscripts and leather binding.

For each material, chemical structure, chemical composition, molecular formula, solubility, advantages, disadvantages and its role in treatment process are presented.

This study concluded that carboxy methyl cellulose, hydroxy propyl cellulose, methyl cellulose, cellulose acetate, nanocrystalline cellulose, funori, sturgeon glue, poly vinyl alcohol, chitosan, chitosan nanoparticles (NPs), gelatin, aquazol, paraloid B72 and hydroxyapatite NPs were the most common and important materials used for the consolidation of illuminated paper manuscripts. For the leather bindings, hydroxy propyl cellulose, polyethylene glycol, oligomeric melamine-formaldehyde resin, acrylic wax SC6000, pliantex, paraloid B67 and B72, silicone oil and collagen NPs are the most consolidants used.

Illuminated paper manuscripts with leather binding are considered one of the most important objects in libraries, museums and storehouses. The uncontrolled conditions and other deterioration factors inside the libraries and storehouses lead to degradation of these artifacts. The brittleness, fragility and weakness are considered the most common deterioration aspects of illuminated paper manuscripts and leather binding. Therefore, the consolidation process became vital and important to solve this problem. This study presents the main materials used for consolidation process of illuminated paper manuscripts and leather bindings.

The consolidation process and morphology evolution in ceramics-based additive manufacturing (AM) are still not well-understood. As a way to better understand the ceramic selective laser sintering (SLS), a dynamic three-dimensional computational model was developed to forecast thermal behavior of hydroxyapatite (HA) bioceramic.

AM has revolutionized automotive, biomedical and aerospace industries, among many others. AM provides design and geometric freedom, rapid product customization and manufacturing flexibility through its layer-by-layer technique. However, a very limited number of materials are printable because of rapid melting and solidification hysteresis. Melting-solidification dynamics in powder bed fusion are usually correlated with welding, often ignoring the intrinsic properties of the laser irradiation; unsurprisingly, the printable materials are mostly the well-known weldable materials.

The consolidation mechanism of HA was identified during its processing in a ceramic SLS device, then the effect of the laser energy density was studied to see how it affects the processing window. Premature sintering and sintering regimes were revealed and elaborated in detail. The full consolidation beyond sintering was also revealed along with its interaction to baseplate.

These findings provide important insight into the consolidation mechanism of HA ceramics, which will be the cornerstone for extending the range of materials in laser powder bed fusion of ceramics.

This paper aims to investigate the ability of traditional biopolymers, such as funori or the nanoscale form of cellulose nanocrystals, to consolidate fragile paper and preserve it for as long as possible.

Degraded papers dating back two centuries were separated into paper samples for consolidation processes. Funori – a marine spleen – was used as a traditional consolidation material and a mixture with ZnO NPs compared with modern materials, such as cellulose nanocrystals. The samples were aged for 25 years, examinations and analyses were performed using scanning electron microscopy and color change was assessed using the CIELAB system, X-ray diffraction and Fourier-transform infrared spectroscopy.

According to the results, using traditional materials to consolidate damage, such as funori, after aging resulted in glossiness on the surface, a color change and increased water content and oxidation. Furthermore, samples treated with a mixture of ZnO NPs and funori revealed that the mixture improved the sample properties and increased the degree of crystallization. Cellulose nanocrystals improved the surface, filled gaps, formed bridges between the fibers and acted as a protector from aging effects.

This paper highlights the ability of nanomaterials to enhance the properties of materials as additives and treat the paper manuscripts from weaknesses.

This study aims to outline the current challenges in ultrasonic additive manufacturing (AM). AM has revolutionized manufacturing and offers possible solutions when conventional techniques reach technological boundaries. Ultrasonic additive manufacturing (UAM) uses mechanical vibrations to join similar or dissimilar metals in three-dimensional assemblies. This hybrid fabrication method got attention due to minimum scrap and near-net-shape products.

This paper reviews significant UAM areas in process parameters such as pressure force, amplitude, weld speed and temperature. These process parameters used in different studies by researchers are compared and presented in tabular form. UAM process improvements and understanding of microstructures have been reported. This review paper also enlightens current challenges in the UAM process, process improvement methods such as heat treatment methods, foil-to-foil overlap and sonotrode surface roughness to increase the bond quality of welded parts.

Results showed that UAM could solve various problems and produce net shape products. It is concluded that process parameters such as pressure, weld speed, amplitude and temperature greatly influence weld quality by UAM. Post-weld heat treatment methods have been recommended to optimize the mechanical strength of ultrasonically welded joints process parameters. It has been found that the tension force is vital for the deformation of the pre-machined structures and for the elongation of the foil during UAM bonding. It is recommended to critically investigate the mechanical properties of welded parts with standard test procedures.

This study compiles relevant research and findings in UAM. The recent progress in UAM is presented in terms of material type, process parameters and process improvement, along with key findings of the particular investigation. The original contribution of this paper is to identify the research gaps in the process parameters of ultrasonic consolidation.

This paper aims to find a suitable solution to treat the solidification paper by using hydroxypropyl cellulose (HPC) to improve the mechanical, physical and chemical properties of paper.

The samples have gone several stages, starting with the manufacture of paper from the linen pulp and the same components of the hardened manuscript papers. It was subjected to artificial aging to reach an age comparable to the manuscript age, then it was subjected to natural aging by inoculation it with A. niger. Mechanical cleaning of the leaves was done with soft brushes. The samples have been consolidated by HPC 2%. Digital microscopy, scanning electron microscopy, mechanical properties measurement, color change, Fourier transform infrared and pH measurements were used to assess the effect of HPC on the qualities of leaves.

HPC succussed in strengthening and restoring the natural, chemical and mechanical properties for the solidified leaves.

The solidified papers phenomenon constitutes severe suffering for manuscripts and books conservators. The paper consolidation initial stage is one of the most important conservation stages because paper has lost many natural, mechanical and chemical properties. The most important feature of this study is providing a solution to the hardened leaves strengthening problem and restoring their chemical, natural and mechanical properties.

Paper aims to evaluate the efficiency of traditional chitosan, nano chitosan, and chitosan nanocomposites for consolidating aged papyrus samples. Cellulose-based materials, such as papyrus sheets and paper, which are the most common types of writing supports for works of art in many museums and archive. They are subjected to different types of deterioration factors that may lead to many conservation problems. Consolidation treatment is one of the most common conservation treatments, which should have perform after much testing to select the appropriate consolidants.

This research paper aims to evaluate the resistance of traditional chitosan, nanochitosan and chitosan/zinc oxide nanocomposite as an eco-friendly papyrus strengthening. Untreated and treated papyrus was thermally aged and characterized via scanning electron microscope (SEM) and Fourier transform infrared spectroscopy (FTIR). Antimicrobial activity of the papyrus specimens was also determined against four tested pathogenic bacteria by disc diffusion method: MRSA, Staphylococcus aureus, E. coli and P. aeruginosa.

The results revealed that chitosan nanocomposite showed a remarkable enhancement of papyrus tensile properties and presence of ZnO prevents the effects of biodeterioration.

Zinc oxide nanoparticles enhance the optical properties and increase the chemical reactions between the consolidating material and the treated papyrus.

This study aims to evaluate the efficiency of using some polymers at different concentrations in the consolidation of vegetable-tanned leather artifacts.

New vegetable-tanned leather samples were prepared. The consolidants used were polyacrylamide (PAM) and polymethyl methacrylate/hydroxyethyl methacrylate (MMA-HEMA). Accelerated heat aging was applied to the untreated and treated samples. Analytical techniques used were Fourier transform infrared spectroscopy (FTIR), digital microscope, scanning electron microscope (SEM), change of color and mechanical properties.

The characteristic FTIR bands showed the effect of accelerated heat aging on the molecular structure of the studied samples, but treated and aged treated samples used were better than aged untreated samples. Microscopic investigations (digital and SEM), and mechanical properties proved that 2% was the best concentration for polymers used. The change in the total color difference of the treated and aged treated samples was limited.

This study presents the important results obtained from PAM and poly(MMA-HEMA) used for the consolidation of vegetable-tanned leather artifacts. The best results of the studied polymers can be applied directly to protect historical vegetable-tanned leathers.

The purpose of this study is to find an applicable solution for the consolidation of petrified paper after disassembling it to complete other stages of treatment.

The samples were subjected to natural aging by being inoculated with Aspergillus niger until they reached the stage of adhesion and petrification. After that, the leaves were separated, and cellulose nanocrystals were applied, then the leaves were subjected to wet thermal aging for 21 days. Digital microscope, scanning electron microscope, mechanical properties measurement, measurement of color change, Fourier transform infrared spectroscopy and pH measurement were used to evaluate the effects of the cellulose nanocrystal on paper.

The results proved that cellulose nanocrystal (5%) successes consolidation of petrified paper Without affecting its natural, mechanical and chemical properties.

This study was based on the effectiveness of cellulose nanocrystal in strengthening the petrified papers and testing its effect on the physical, mechanical and chemical paper properties.

Natural gas hydrate (NGH) has been regarded as one of the most important resources due to NGH's large amounts of reserve. However, NGH development still faces many technical challenges, such as low production rate and reservoir instability resulting from NGH decomposition. Therefore, developing a fully coupled THMC model for simulating the hydrate decomposition and studying its mechanical behavior is very important and necessary. The purpose of this article is to develop and solve a multi-phase, strong nonlinearity and large-scale fully coupled thermal-hydro-mechanical–chemical (THMC) model for simulating the multi-physics processes involving solid-liquid-gas flow, heat transfer, NGH phase change and rock deformation during NGH decomposition.

In this paper, a multi-phase, strong nonlinearity and large-scale fully coupled THMC model is developed for simulating the multi-physics processes involving solid-liquid-gas flow, heat transfer, NGH phase change and rock deformation during NGH dissociation. The fully coupled THMC model is solved by using a fully implicit finite element method, in which the gas pressure, water pressure, temperature and displacement are taken as basic unknown variables. The proposed model is validated against with the experimental data, showing high accuracy and reliability.

A multi-phase, strong nonlinearity and large-scale fully coupled THMC model is developed for simulating the multi-physics processes involving solid-liquid-gas flow, heat transfer, NGH phase change and rock deformation during NGH decomposition. The proposed model is validated against with the experimental data, showing high accuracy and reliability.

Some assumptions are made to make the model tractable, including (1) the composition gas of hydrate is pure methane; (2) the gas-liquid multi-phase flow in the pore obeys Darcy's law; (3) hydrate occurs on the surface of soil particles, both of them form the composite consolidation material; (4) the small-strain assumption is applied to composite solid materials, which are treated as skeletons and cannot be moved; (5) momentum change caused by phase change is not considered.

NGH has been regarded as one of the most important resources due to its large amounts of reserve. However, NGH development still faces many technical challenges, such as low production rate and reservoir instability resulting from NGH decomposition. Most of the existing studies decouple the process with solid deformation and seepage behavior, but the accuracy of the numerical results will be sacrificed to certain extent. Therefore, it is very important and necessary to develop a fully coupled THMC model for simulating the hydrate decomposition and studying its mechanical behavior.

NGH, widely distributed in shallow seabed or permanent frozen region, has the characteristics of high energy density and high combustion efficiency (Yan et al., 2020). A total of around 7.5 × 1,018 m³ has been proved to exist around the world and 1 m³ of NGH can release about 160–180 m³ of natural gas (Kvenvolden and Lorenson) under normal conditions. Safely and sustainably extracting NGH commercially can effectively relieve global energy pressure and contribute to achieving carbon reduction goals.

The novelty of the present work lies in mainly two aspects. First, a fully coupled THMC model is developed for studying the multi-physics processes involving solid-liquid-gas flow, heat transfer, NGH phase change and solid deformation during NGH dissociation. Second, the numerical solution is obtained by using a fully implicit finite element method (FEM) and is validated against experimental data.