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Article
Publication date: 23 February 2024

Guangwei Liang, Zhiming Gao, Cheng-Man Deng and Wenbin Hu

The purpose of this study is to reveal the effect of nano-Al2O3 particle addition on the nucleation/growth kinetics, microhardness, wear resistance and corrosion resistance of…

Abstract

Purpose

The purpose of this study is to reveal the effect of nano-Al2O3 particle addition on the nucleation/growth kinetics, microhardness, wear resistance and corrosion resistance of Co–P–xAl2O3 nanocomposite plating.

Design/methodology/approach

The kinetics and properties of Co–P–xAl2O3 nanocomposite plating prepared by electroplating were investigated by electrochemical measurements, scanning electron microscopy, X-ray diffraction, X-ray photoelectron spectroscopy, Vickers microhardness measurement, SRV5 friction and wear tester and atomic force microscopy.

Findings

A 12 g/L nano-Al2O3 addition in the plating solution can transform the nucleation/growth kinetics of the plating from the 3D progressive model to the 3D instantaneous model. The microhardness of the plating increased with the increase of nano-Al2O3 content in plating. The wear resistance of the plating did not adhere strictly to Archard’s law. An even and denser corrosion product film was generated due to the finer grains, with a high corrosion resistance.

Originality/value

The effect of different nano-Al2O3 addition on the nucleation/growth kinetics and properties of Co–P–xAl2O3 nanocomposite plating was investigated, and an anticorrosion mechanism of Co–P–xAl2O3 nanocomposite plating was proposed.

Details

Anti-Corrosion Methods and Materials, vol. 71 no. 3
Type: Research Article
ISSN: 0003-5599

Keywords

Article
Publication date: 6 June 2023

Zhenbo Qin, Jiale Li, Yiwen Zhang, Zhong Wu and Wenbin Hu

The purpose of this paper is to improve the corrosion resistance of stainless-steel bipolar plate by magnetron sputtering.

Abstract

Purpose

The purpose of this paper is to improve the corrosion resistance of stainless-steel bipolar plate by magnetron sputtering.

Design/methodology/approach

TiC/amorphous carbon composite film was deposited by magnetron sputter at four different temperature of 25°C, 200°C, 300°C and 400°C. The morphology, composition and structure of the film were characterized by scanning electron microscopy, atomic force microscopy and X-ray photoelectron spectroscopy. And its corrosion behavior was analyzed through electrochemical impedance spectroscopy, potentiodynamic and potentiostatic polarization tests.

Findings

A compact TiC/amorphous carbon film was prepared by magnetron sputtering on 316L stainless steel, and the particles of the film were refined with the increase in sputtering temperature. High temperature promoted the formation of TiC and C–C sp2 hybrid carbon, but excessively high temperature caused the oxidation of Ti and a significant decrease in sp2 hybrid carbon. The corrosion resistance of the film increased with the temperature, and the corrosion current density polarization at 0.86 V and 1.8 V for TiC/a–C film prepared at 400 °C is only 1.2% and 43.2% of stainless steel, respectively.

Originality/value

The corrosion resistance of amorphous carbon films was improved by the doping of Ti carbide, and the appropriate sputtering temperature was obtained.

Details

Anti-Corrosion Methods and Materials, vol. 70 no. 4
Type: Research Article
ISSN: 0003-5599

Keywords

Article
Publication date: 26 May 2023

Chunhua Liu, Ming Li, Peng Chen and Chaoyun Zhang

This study aims to solve the problems of ambiguous localization, large calculation, poor real-time and limited applicability of bolt thread defect detection.

Abstract

Purpose

This study aims to solve the problems of ambiguous localization, large calculation, poor real-time and limited applicability of bolt thread defect detection.

Design/methodology/approach

First, the acquired ultrasound image is used to acquire the larger area of the image, which is set as the compliant threaded area. Second, based on the determined coordinates of the center point in each selected region, the set of coordinates on the left and right sides of the bolts is acquired by DBSCAN method with parameters eps and MinPts, which is determined by data set dimension D and the k-distance curve. Finally, the defect detection boundary line fitting is completed using the acquired coordinate set, and the relationship between the distance from each detection point to the curve and d, which is obtained from the measurement of the standard bolt sample with known thread defect, is used to locate the bolt thread defect simultaneously.

Findings

In this paper, the bolt thread defect detection method with ultrasonic image is proposed; meanwhile, the ultrasonic image acquisition system is designed to complete the real-time localization of bolt thread defects.

Originality/value

The detection results show that the method can effectively detect bolt thread defects and locate the bolt thread defect location with wide applicability, small calculation and good real-time performance.

Details

Anti-Corrosion Methods and Materials, vol. 70 no. 4
Type: Research Article
ISSN: 0003-5599

Keywords

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