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This paper aims to focus the synchronous chemical conversion technology–based titanium/zirconium composite on 6061, 7075 aluminum alloys and galvanized steel.

The effects of pH, temperature, reaction time and other process parameters on the corrosion resistance of the three metal surface coatings were investigated by copper sulfate drop and electrochemical corrosion performance tests under a certain content of H2TiF6 and H2ZrF6. The surface morphology and element distribution of the conversion coating were analyzed by scanning electron microscope and X-ray photoelectron spectroscopy.

The results show that the optimal synchronization chemical conversion conditions of 6061/7075 aluminum alloys/galvanized steel are controlled as follows: H2TiF6 2.2 mL/L, H2ZrF6 1 mL/L, pH 3.9, conversion temperature 35°C and conversion time 120 s.

Multi-metals chemical conversion coating can be obtained simultaneously with uniform corrosion resistance and surface morphology. The presence of microdomain features in multiple metals facilitates simultaneous chemical conversion into coatings.

High-performance wrought aluminum alloys, particularly AA6061, are pivotal in industries like automotive and aerospace due to their exceptional strength and good response to heat treatments. Investment casting offers precision manufacturing for these alloys, because casting AA6061 poses challenges like hot cracking and severe shrinkage during solidification. This study aims to address these issues, enabling crack-free investment casting of AA6061, thereby unlocking the full potential of investment casting for high-performance aluminum alloy components.

Nanotechnology is used to enhance the investment casting process, incorporating a small volume fraction of nanoparticles into the alloy melt. The focus is on widely used aluminum alloy 6061, utilizing rapid investment casting (RIC) for both pure AA6061 and nanotechnology-enhanced AA6061. Microstructural characterization involved X-ray diffraction, optical microscopy, scanning electron microscopy, differential scanning calorimetry and energy dispersive X-ray spectroscopy. Mechanical properties were evaluated through microhardness and tensile testing.

The study reveals the success of nanotechnology-enabled investment casting in traditionally challenging wrought aluminum alloys like AA6061. Achieving crack-free casting, enhanced grain morphology and superior mechanical properties, because the nanoparticles control grain sizes and phase growth, overcoming traditional challenges associated with low cooling rates. This breakthrough underscores nanotechnology's transformative impact on the mechanical integrity and casting quality of high-performance aluminum alloys.

This research contributes originality and value by successfully addressing the struggles in investment casting AA6061. The novel nano-treating approach overcomes solidification defects, showcasing the potential of integrating nanotechnology into rapid investment casting. By mitigating challenges in casting high-performance aluminum alloys, this study paves the way for advancements in manufacturing crack-free, high-quality aluminum alloy components, emphasizing nanotechnology's transformative role in precision casting.

Aluminum alloy is considered an ideal material in aerospace, automobile and other fields because of its lightweight, high specific strength and easy processing. However, low hardness and strength of the surface of aluminum alloys are the main factors that limit their applications. The purpose of this study is to obtain a composite coating with high hardness and lubricating properties by applying GO–PVA over MAO coating.

A pulsed bipolar power supply was used as power supply to prepare the micro-arc oxidation (MAO) coating on 6061 aluminum sample. Then a graphene oxide-polyvinyl alcohol (GO–PVA) composite coating was prepared on MAO coating for subsequent experiments. Samples were characterized by Fourier infrared spectroscopy, X-ray diffraction, Raman spectroscopy and thermogravimetric analysis. The friction test is carried out by the relative movement of the copper ball and the aluminum disk on the friction tester.

Results showed that the friction coefficient of MAO samples was reduced by 80% after treated with GO–PVA composite film.

This research has made a certain contribution to the surface hardness and tribological issues involved in the lightweight design of aluminum alloys.

The peer review history for this article is available at: https://publons.com/publon/10.1108/ILT-12-2023-0427/

The purpose of this study is to investigate the microstructure of fretting wear behavior in 6061-T6 aluminum alloy. The fretting wear of blind riveted lap joints of 6061-T6 aluminum alloy plates, which are widely used in aircraft construction, was investigated. Fretting damages were investigated between the contact surface of the plates and between the plate and the rivet contact surface.

Experiments were carried out using a computer controlled Instron testing machine with 200 kN static and 100 kN dynamic load capacity. Max package computer program was used for the control of the experiments. Fretting scars, width of wear scars, microstructure was investigated by metallographic techniques and scanning electron microscopy.

It was found that fretting damages were occurred between the plates contacting surface and between the plate and rivet contact surface. As load and cycles increased, fretting scars increased. Fretting wear initially begins with metal-to-metal contact. Then, the formed metallic wear particles are hardened by oxidation. These hard particles spread between surfaces, causing three-body fretting wear. Fretting wear surface width increases with increasing load and number of cycles.

The useful life of many tribological joints is limited by wear or deterioration of the fretting components due to fretting by oscillating relative displacements of the friction surfaces. Such displacements are caused by vibrations, reciprocating motion, periodic bending or twisting of the mating component, etc. Fretting also tangibly reduces the surface layer quality and produces increased surface roughness, micropits, subsurface microphone.

The majority of machine component failures are caused by load conditions that change with time. Under those circumstances, the component can function effectively for a long time but then breaks down unexpectedly and without warning. Therefore, the study of fatigue considerations in design becomes important. Also, to determine the component's long-term tenability, fatigue behavior must be investigated. This paper aims to investigate the fatigue life of aluminum 6061-T6 alloy under uniaxial loading using experiments and finite element simulation.

Both base metal (BM) and friction stir welding (FSW) configurations have been used to analyze fatigue behavior. The experimental tests were carried out using Instron-8801 hydraulic fatigue testing machine at frequency of 20 Hz and load ratio of 0.1. The yield strength, ultimate tensile strength, amplitude stress and fatigue life were used as input in simulation analysis software. Based on the findings of the tensile test, the maximum stress applied during the fatigue testing was estimated. Simulated and experimental results were also used to plot and validate the S-N curves. The fracture behavior of specimens was also examined using fractographic analysis.

The fractured surfaces indicate both brittle and ductile failure in the specimens. However, dimples dominated during the final fracture. The comparison between experimental and simulation results illustrates that the difference in fatigue cycles increases with an increase in the yield strength of both BM and FSWed specimens. This disparity is attributed to many factors such as scratches, rough surfaces and microstructural behavior. Aluminum 6061-T6 alloy is considered a noteworthy material where high strength with reduced weight contributes to the crash-worthy design of automobile structures.

The current study is significant in the prediction of the fatigue life of aluminum 6061-T6 alloy using experiments and simulation analysis. A good correlation was found when the experimental and simulation analysis were compared. The proposed simulation analysis approach can be used to anticipate a component's fatigue life.

The increasing interest in engineering structures made from multiple materials has led to corresponding interest in technologies, which can fabricate multi‐material parts. The purpose of this paper is to further explore of the multi‐material fabrication capabilities of ultrasonic consolidation (UC).

Various combinations of materials including titanium, silver, tantalum, aluminum, molybdenum, stainless steel, nickel, copper, and MetPreg^® were ultrasonically consolidated. Some of the materials were found to be effective as an intermediate layer between difficult to join materials. Elemental boron particles were added in situ between selected materials to modify the bonding characteristics. Microstructures of deposits were studied to evaluate bond quality.

Results show evidence of good bonding between many combinations of materials, thus illustrating increasing potential for multi‐material fabrication using UC.

Multi‐material fabrication capabilities using UC and other additive manufacturing processes is a critical step towards the realization of engineering designs which make use of functional material combinations and optimization.

This paper aims that optimization parameters depending on machining processes examine to define for the milling process of AL 6061-T6 aluminum alloy used in the aviation industry.

The Taguchi method was used to study the optimal parameters. Furthermore, the effects of machining parameters on surface roughness were also evaluated by performing variance analysis. Optimum parameter levels were determined by Signal/Noise analysis.

It was determined that the parameter levels that optimize the surface roughness were “4000 rev/min for the rotational speed of the cutting tool, 0.4 mm for the cutting depth and the optimum value for the feedrate 500 mm/min.”

It is limited by the precision of the manufacturing processes, the desired geometry and the exactness of the measurement make the machine productivity valuable in the production of parts.

By improving the optimal production parameters, reducing part production costs and waste amount in aviation has been seen as an important gain.

Improving production methods and optimization parameters in production technologies will ensure the minimization of loss and waste. These developed parameters with optimizing the surface roughness will add value in this context.

It was determined that the parameter levels that optimize the surface roughness of aluminum considering manufacturing processes. Especially as process parameters, optimum feed rate has been developed for effective rotation speed and cutting depth for cutting tools.

The purpose of this paper is to develop a chrome-free and phosphorus-free chemical conversion coating with good corrosion resistance, a novel chemical conversion coating was prepared by adding cerium nitrate hexahydrate and salicylic acid in the treatment solution containing titanium/zirconium ions on 6061 aluminum alloy.

Compared with the AA6061 aluminum alloy matrix, the self-corrosion potential of the conversion coating is significantly positively shifted, the self-corrosion current density is greatly reduced and its corrosion resistance is significantly improved. Morphology and composition of the conversion coatings were observed by scanning electron microscopy and energy-dispersive X-ray spectroscopy. The microdomain structure of conversion coatings at different formation stages was analyzed by electron probe microanalyzer.

An optimized preparation technique of titanium–zirconium chemical conversion coating for AA6061 aluminum alloy is obtained: H₂TiF₆ 4 mL/L, H₂ZrF₆ 0.4 mL/L, salicylic acid 0.35 g/L, Ce(NO₃)₃·6H₂O 0.14 g/L, reaction temperature 30°C, reaction time 120 s and pH 4.0.

The coating forms on the Al(Fe)Si intermetallic compound, and Ce³⁺ is preferentially adsorbed on the intermetallic compound. The hydrolysis of Ce³⁺ causes the local pH of the solution to decrease, which promotes matrix dissolution and charge migration. As the microanode/microcathode reaction occurs, the local pH of the solution increases, and Al₂O₃/ZrO₂/TiO₂ begins to deposit on the surface of the metal substrate.

Additive manufacturing (AM) can achieve significant weight savings with only minor compromises in strength if high-performance wrought aluminum alloys are used as feedstock. Despite the advantages in strength that aluminum alloys (AA) 6061 offer, they cannot be manufactured via printing because of hot cracking and other solidification problems. The purpose of this study is to achieve high-quality printing of AA6061 with nanotreated wires.

Nanotreating was used to modify the AA6061 alloy composition by adding a small fraction of nanoparticles to enhance the alloy’s manufacturability and resultant properties. Wire arc additive manufacturing (WAAM) was used to print the nanotreated AA6061 wire feedstock. The microstructure of the printed AA6061 was characterized by X-ray crystallography, optical microscopy, scanning electron microscopy and energy dispersive spectroscopy mapping. The microhardness profile, tensile behavior and fracture surface were analyzed.

This work successfully used WAAM to print nanotreated AA 6061 components. The resulting AA6061 parts were crack-free, with exceptional grain morphology and superior mechanical properties. Owing to the excellent size control capabilities of nanoparticles, a homogeneous distribution of small grains was maintained in all deposited layers, even during repeated thermal cycles.

Previous studies have not successfully printed AA6061 using WAAM. Conventional WAAM products exhibit anisotropic mechanical properties. The nanotreated AA6061 was successfully printed to achieve homogeneous microhardness and isotropic tensile properties. The promising results of this study reflect the great potential of nanotech metallurgy as applied to the WAAM process.

Friction stir welding (FSW) is considered an environmentally sound process compared to traditional fusion welding processes. It is a complex process in which various parameters influence weld strength. Therefore, it is essential to identify the best parameter settings for achieving the desired weld quality. This paper aims to investigate the multi-response optimization of process parameters of the FSWed 6061-T6 aluminum (Al) alloy.

The input process parameters related to FSW have been sorted out from a detailed literature survey. The properties of weldments such as yield strength, ultimate tensile strength, percentage elongation and microhardness have been used to evaluate weld quality. The process parameters have been optimized using the Taguchi-based grey relational analysis (GRA) methodology. Taguchi L16 orthogonal array has been considered to design the experiments. The effect of input parameters on output responses was also determined by the analysis of variance (ANOVA) method. Finally, to corroborate the results, a confirmatory experiment was carried out using the optimized parameters from the study.

The ANOVA result indicates that the tool rotation speed was the most significant parameter followed by tool pin profile and welding speed. From the confirmation test, it was observed that the optimum FSW process parameters predicted by the Taguchi method improved the grey relational grade by 13.52%. The experimental result also revealed that the Taguchi-based GRA method is feasible in finding solutions to multi-response optimization problems in the FSW process.

The present study is unique in the multi-response optimization of FSWed 6061-T6 Al alloy using the Taguchi and GRA methodology. The weld material having better mechanical properties is essential for the material industry.