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The purpose of this paper is to establish an automated microscopic imaging database system using a set of Radio Frequency Identification (RFID) management functions to provide a secure storage for hispathology images.

The automated microscopy imaging system is composed mainly of four parts, which include: first, tissue biopsy image acquisition system, second, image processing system, third, RFID system, and fourth, SQL database system. The system has two modes of operation to store and manage hispathology images. First, the hispathology slide undergoes fluorescence staining before acquiring images directly from an external CCD camera connected to the system. Second, the hispathogical slides that have undergone fluorescence staining undergo another microscopic imaging system, and the contents are extracted into a digitized image archive and imported to the system. Also, the system not only acquires images but also performs functions such as displacement correction, image superimposition, and calculation of the total number of fluorescence points. The two methods mentioned above produce the hispathology image files and are tagged using an RFID string index to establish and manage the database system.

The results demonstrated that in the impurities were effectively eliminated in the red fluorescence staining after binarization processing. However, the blue ones remained the same and to solve this problem an adjustable threshold allows users to select the appropriate threshold. Using an additional eigenvalue code to the RFID string provides better encryption mechanism for the patient files and any attempt to tamper the file can easily be detected through the comparison of the eigenvalues.

This paper proposes a novel method to implement a more comprehensive, safe, fast, and automated management system for hispathological images using RFID management and image processing techniques. Additional security is provided by including eigenvalues as encryption mechanisms in the Tag string of the RFID.

Two corrosion inhibitors for closed cooling water systems, nitrite-based and mixture of nitrite and molybdate corrosion inhibitor, are often compared to each other. This study aims to optimize these two inhibitors in terms of concentration and pH for carbon steel protection, with insights into the double layer structure on surface and its impact on corrosion inhibition.

Electrochemical analysis including electrochemical impedance spectroscopy and potentiodynamic test are carried out for quick assessment of corrosion inhibition efficiency and optimization, which is confirmed by immersion test and microscopic analysis. The electronic properties of the surface film are analyzed through Mott–Schottky method which provides new insights into the inhibition mechanism and the role of each component in mixture inhibitor.

Mixture of nitrite and molybdate is shown to present higher inhibition efficiency, owning to the double layer structure. Nitrite alone can form a protective surface film, whereas molybdate leads to an n-type semiconductive film with lower donor density, hence giving rise to a better inhibition effect.

Surface after inhibitor treatment has been carefully characterized to the microscopic scale, implying the effect of micro-structure, chemical composition and electronic properties on the corrosion resistance. Inorganic corrosion inhibitors can be tuned to provide higher efficiency by careful design of surface film structure and composition.

Almost every study on corrosion inhibitor applies such method for quick assessment of corrosion inhibition effect. Mott–Schottky test is one of electrochemical methods that reveals the electronic properties of the surface film. Previous works have studied the surface layer mainly through X-ray photoelectron spectroscopy. This study provides another insight into the surface film treated by nitrite and molybdate through Mott–Schottky analysis, and relates this structure to the corrosion inhibition effect based on multiple analysis including electrochemistry, microscopic characterization, thermodynamics and interface chemistry.

The purpose of this paper is to develop an automated phase segmentation model from complex microstructure. The mechanical and physical properties of metals and alloys are influenced by their microstructure, and therefore the investigation of microstructure is essential. Coexistence of random or sometimes patterned distribution of different microstructural features such as phase, grains and defects makes microstructure highly complex, and accordingly identification or recognition of individual phase, grains and defects within a microstructure is difficult.

In this perspective, computer vision and image processing techniques are effective to help in understanding and proper interpretation of microscopic image. Microstructure-based image processing mainly focuses on image segmentation, boundary detection and grain size approximation. In this paper, a new approach is presented for automated phase segmentation from 2D microstructure images. The benefit of the proposed work is to identify dominated phase from complex microstructure images. The proposed model is trained and tested with 373 different ultra-high carbon steel (UHCS) microscopic images.

In this paper, Sobel and Watershed transformation algorithms are used for identification of dominating phases, and deep learning model has been used for identification of phase class from microstructural images.

For the first time, the authors have implemented edge detection followed by watershed segmentation and deep learning (convolutional neural network) to identify phases of UHCS microstructure.

This study aims to comprehensively investigate the mixed-mode fracture behavior and mechanical properties of selective laser sintering (SLS) polyamide 12 (PA12) components, considering different build orientations and layer thicknesses. The primary objectives include the following. Conducting mixed-mode fracture and mechanical analyses on SLS PA12 parts. Investigating the influence of build orientation and layer thickness on the mechanical properties of SLS-printed components. Examining the fracture mechanisms of SLS-produced Arcan fracture and tensile specimens through experimental methods and finite element analyses.

The research used a combination of experimental techniques and numerical analyses. Tensile and Arcan fracture specimens were fabricated using the SLS process with varying build orientations (X, X–Y, Z) and layer thicknesses (0.1 mm, 0.2 mm). Mechanical properties, including tensile strength, modulus of elasticity and critical stress intensity factor, were quantified through experimental testing. Mixed-mode fracture tests were conducted using a specialized fixture, and finite element analyses using the J-integral method were performed to calculate fracture toughness. Scanning electron microscopy (SEM) was used for detailed morphological analysis of fractured surfaces.

The investigation revealed that the highest tensile properties were achieved in samples fabricated horizontally in the X orientation with a layer thickness of 0.1 mm. Additionally, parts manufactured with a layer thickness of 0.2 mm exhibited favorable mixed-mode fracture behavior. The results emphasize the significance of build orientation and layer thickness in influencing mechanical properties and fracture behavior. SEM analysis provided valuable insights into the failure mechanisms of SLS-produced PA12 components.

This study contributes to the field of additive manufacturing by providing a comprehensive analysis of the mixed-mode fracture behavior and mechanical properties of SLS-produced PA12 components. The investigation offers novel insights into the influence of build orientation and layer thickness on the performance of such components. The combination of experimental testing, numerical analyses and SEM morphological observations enhances the understanding of fracture behavior in additive manufacturing processes. The findings contribute to optimizing the design and manufacturing of high-quality PA12 components using SLS technology.

Polyurethane concrete has a high strength-to-weight ratio in the short term, and the strength-to-weight ratio stage during the maintenance period is critical. Freeze-thaw cycles have a noticeable damaging effect on the durability of polyurethane concrete. The engineering specification of polyurethane concrete with incomplete hydration reaction must be studied, as well as the development of internal structure during curing. In this paper, the polyurethane concrete tests were set up under eight distinct maintenance settings based on the climate features of the northern area and the service environment. The test results were evaluated to determine the effect of the number of early freeze-thaw cycles and the time node of early freeze-thaw cycles on the mechanical characteristics of polyurethane concrete, which revealed that the time node of freeze-thaw damage impacted the freeze-thaw resistance of polyurethane concrete susceptible to early freeze-thaw damage.

The early-age freeze-thaw damage polyurethane concrete was experimentally studied by controlling the time node of the freeze-thaw cycle and the curing environment. The test considered the time node, frequency of freeze-thaw damage of polyurethane concrete and the influence of subsequent curing environment and observed the mass change, relative dynamic elastic modulus, relative durability index, compressive strength and apparent damage of polyurethane concrete. The early mechanical properties of polyurethane concrete were studied by analyzing the change of numerical value. The microscopic mechanism of strength formation of polyurethane concrete was analyzed by XRD, FTIR and SEM image.

The closer the time of freeze-thaw damage was to the specimen hardening, the worse the mechanical properties and structure were, according to SEM photographs. For specimens with serial number of 12-groups, its compressive strength is only 82.39% of that of the standard group, even if the curing process continues after 20 times thawing, which increased early environment exacerbate strength loss in polyurethane concrete and also reduced freeze-thaw resistance. The findings of the tests reveal that curing can restore the freeze-thaw resistance of damaged polyurethane concrete. Curing in water has a better recovery impact than curing in air; the mechanical properties can be restored by sufficient re-curing time and good re-curing conditions.

By studying the freeze-thaw cycle test and test results of polyurethane concrete in different curing time nodes, the relationship between the mechanical properties of polyurethane concrete and the time node, number of freeze-thaw cycles, and subsequent maintenance environment was explored. Considering the special mechanism of strength formation of polyurethane concrete, the polyurethane concrete damaged by freeze-thaw has the ability to continue to form strength under subsequent maintenance. This experimental study can provide an analytical basis for the strength formation and reconditioning of polyurethane concrete structures subjected to freeze-thaw environments during the curing time under extreme natural conditions in fall and winter in actual projects.

The prime task of research in hot forging industry is to improve the service life of forging dies. The in-service microstructural changes that may occur in a die during hot forging is expected to significantly affect the service life. The purpose of this work is to analyse the microstructural evolution of double tempered hot forging dies in a real industrial environment, and the correlation of microstructural and microhardness evolution to the in-service wear and plastic deformation.

Specific hot forging tests were carried out on double tempered AISI H11 chromium tool steel for 100, 500 and 1,000 forging strokes. Macro analysis was conducted on die cross section to analyse the wear and plastic deformation at different stages of forging cycles. Microhardness and microstructural analyses were performed on the die surface after these forging tests.

The macro analysis on the transverse section of dies shows that wear is predominant during initial forging strokes, whereas plastic deformation is observed in later stages. Microstructural analyses demonstrate that during first 500 forging cycles, carbide population decreases at 63 per cent higher rate as compared to corresponding drop during 501 to 1,000 forging cycles. Additionally, the carbide size increases at all stages of forging cycle. Further, microstructural images from dies after 1,000 forging strokes show clustering and spherodisation of carbides by which the “blocky”-shaped carbides in pre-forging samples had spherodised to form “elongated spherical” structures.

The findings of this work can be used in hot forging industries to predict amount of wear and plastic deformation at different stages of service. From the results of this work, the service life of double tempered H11 hot forging dies used in forging without lubrication is within 501 to 1,000 forgings.

Most of the literatures are focussed on the cyclic softening of material at constant temperature. This work analyses the microstructural evolution of double tempered hot forging dies in a real industrial environment and correlates the microstructural and microhardness evolution to the in-service wear and plastic deformation.

The purpose of this research is to design 3D print and analyze mechanical as well as microstructural behavior of interlaced fibrous structures using Dremel 3D45 additive manufacturing (AM) machine.

A series of plain and twill weave fabrics are designed using computer-aided design software Solidworks and printed using fused deposition modeling machines to determine the best model that could be printable. The structures were designed in such a way that the fabricated yarns with pure (PLA) were not sticking to each other in the fabric structure. The specimens were printed in vertical orientation and then tensile and three-point bending (flexural) tests were conducted for twill weave fabrics.

The tests showed that the mechanical strength was higher in the warp direction than in the weft direction. This difference was because of printing of continuous filament-like yarns in the warp direction and staple-like yarns in the weft direction. This orthotropic property of the material was verified by analyzing its microscopic structures via optical microscope.

Future work should include improvement of the structure and exploration of different polymers and their composites to increase the tensile, bending and other strengths to make the 3D-printed structures more flexible and stronger. Future research should also focus on the large-scale manufacturing of 3D printed fabrics.

This paper supports work on wearable 3D-printed fabrics. The 3D-printed fabric will also contribute to new applications and products such as liquid filters.

The research done in this work is new and original. This paper contributes to new knowledge by providing a better understanding of polymers and their 3D printing capabilities to form a complex fabric structure.

This paper aims to investigate the wear mechanisms, formations and effectiveness of tribofilms of new developed, antiwear additive which is called mercapthocarboxylate. The mercapthocarboxylate is a sulphur-based and non-phosphorus additive.

The effectiveness of the additive was examined through a set of laboratory endurance tests that applied with single cylinder spark ignition engine. Two types of lubricants were used to compare the engine tests which were thiophosphate (ZDDP) containing engine lubricant (phosphorus containing) and mercapthocarboxylate containing non-phosphorus and non-ash crankcase oil. Lubricants were tested under identical operating conditions for 100 hrs. The surfaces of cylinder liner and piston rings were inspected through optical microscopy, scanning electron microscopy and energy dispersive X-ray spectroscopy techniques.

Catalysis-friendly and sulphur-based mercapthocarboxylate additive can be an alternative antiwear additive package for lubrication oil due to better wear performance when compared to ZDDP.

Sulphur-based mercapthocarboxylate is a new developed antiwear additive and was applied to lubrication oil in this study. This lubrication oil was tested in the real engine environment by using 100-hr engine bench tests.

The purpose of this paper is to introduce different methods for measuring the porosity of metal foams, and especially present a new method for conveniently measuring the open porosity that has a stronger impact on a number of physical properties of the porous product.

Metal foam is a kind of material that utilizes the function of pores inside the porous body. For such materials, the porosity is an important factor or even a key factor to determine a number of the practical parameters, such as the conductivity, acoustic properties and mechanical performances. Especially, the open porosity has a stronger impact on the sound absorption, electromagnetic shielding, heat transfer of the porous product, as well as the performances of using the internal pore surface. Therefore, it would be meaningful to find the simple and convenient to well measure the open porosity of metal foams.

In the present new method, the open porosity can be obtained directly by different volume parameters of the porous sample, while it can only by some weight indexes of the porous sample in other measuring methods.

The characteristic of this new method makes the measurement simpler and more convenient in this new method than in the other methods.

PolyJet technology allows printing complex multi-material composite configurations using Voxel digital designs' capability, thus allowing rapid prototyping of 3D printed structural parts. This paper aims to investigate the processing and mechanical characteristics of composite material configurations formed from soft and hard materials with different distributions and sizes via voxel digital print design.

Voxels are extruded representations of pixels and represent different material information similar to each pixel representing colors in digital images. Each geometric region of a digitally designed part represented by a voxel can be printed with a different material. Multi-material composite part configurations were formed and rapidly prototyped using a PolyJet printer Stratasys J750. A design of experiments composite part configuration of a soft material (Tango Plus) within a hard material matrix (Vero Black) was studied. Composite structures with different hard and soft material distributions, but at the same volume fractions of hard and soft materials, were rapidly prototyped via PolyJet printing through developed Voxel digital printing designs. The tensile behavior of these formed composite material configurations was studied.

Processing and mechanical behavior characteristics depend on materials in different regions and their distributions. Tensile characterization obtained the fracture energy, tensile strength, modulus and failure strength of different hard-soft composite systems. Mechanical properties and behavior of all different composite material systems are compared.

Tensile characteristics correlate to digital voxel designs that play a critical role in additive manufacturing, in addition to the formed material composition and distributions.

Results clearly indicate that multi-material composite systems with various tensile mechanical properties could be created using voxel printing by engineering the design of material distributions, and sizes. The important parameters such as inclusion size and distribution can easily be controlled within all slices via voxel digital designs in PolyJet printing. Therefore, engineers and designers can manipulate entire morphology and material at each voxel level, and different prototype morphologies can be created with the same voxel digital design. In addition, difficulties from AM process with voxel printing for such material designs is addressed, and effective digital solutions were used for successful prototypes. Some of these difficulties are extra support material or printing the part with different dimension than it designed to achieve the final part dimension fidelity. Present work addressed and resolved such issued and provided cyber based software solutions using CAD and voxel discretization. All these increase broad adaptability of PolyJet AM in industry for prototyping and end-use.