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The purpose of this paper is to characterize three-dimensional (3D) printing filaments commonly used in fused deposition modeling (FDM) to determine their viability for restoration and conservation treatments.

Eight current filaments for FDM from six polymeric materials have been characterized to determine their suitability for restoration and conservation treatments. For testing these filaments, specimens are printed with acrylonitrile-butadiene-styrene; polylactic acid; polylactic acid with CaCO3 (E.P.); polyethylene terephthalate glycol; polypropylene; and high-impact polystyrene. Suitability of a filament was verified using the Oddy test by detecting the action of volatile pollutants released from the filaments. The morphological and color changes were observed after allowing them to degrade under the exposure of UV radiation. The samples were then analyzed using Fourier-transform infrared spectroscopy. In addition, gas chromatography-mass spectroscopy technique was applied to complete the characterization of the printed filaments.

Materials investigated are suitable for restoration purposes ensuring long-term stability. Rapid prototyping using FDM is appropriate for restoring sensitive archaeological objects allowing reconstruction of parts and decreasing risk while manipulating delicate artifacts.

Rapid prototyping using FDM was chosen for the restoration of a fragile and sensitive archaeological glass bowl from Manises Ceramic Museum.

This study aims to describe the preparation of antimicrobial material usable in 3D printing of medical devices. Despite the wealth of technological progress at the time of the crisis caused by SARS-CoV-2 virus: Virus that causes current Pandemic situation (COVID-19), the global population had long been exposed beforehand to an acute absence of essential medical devices. As a response, a new type of composite materials intended for rapid prototyping, based on layered silicate saponite (Sap), antimicrobial dye phloxine B (PhB) and thermoplastics, has been recently developed.

Sap was modified with a cationic surfactant and subsequently functionalized with PhB. The hybrid material in powder form was then grounded with polyethylene terephthalate-glycol (PETG) or polylactic acid (PLA) in a precisely defined weight ratio and extruded into printing filaments. The stability and level of cytotoxicity of these materials in various physiological environments simulating the human body have been studied. The applicability of these materials in bacteria and a yeast-infected environment was evaluated.

Ideal content of the hybrid material, with respect to thermoplastic, was 15 weight %. Optimal printing temperature and speed, with respect to maintaining antimicrobial activity of the prepared materials, were T = 215°C at 50 mm/s for PETG/SapPhB and T = 230°C at 40 mm/s for PLA/SapPhB. 3 D-printed air filters made of these materials could keep inner air flow at 63.5% and 76.8% of the original value for the PLA/SapPhB and PETG/SapPhB, respectively, whereas the same components made without PhB had a 100% reduction of airflow.

The designed materials can be used for rapid prototyping of medical devices.

The new materials have been immediately used in the construction of an emergency lung ventilator, Q-vent, which has been used in different countries during the COVID-19 crisis.

This paper aims to design and test a system capable of coaxial fused deposition modelling (FDM) and assess the coaxial fibres produced for their coaxial concentricity. The goal is to achieve concentricity values below the literature standard of 15 per cent.

This research discusses the design of the coaxial nozzle internal geometry and validates the modelling process by using computational fluid dynamics to assess its flow profile. Sequentially, this paper discusses the abilities of current additive manufacturing (AM) technology in the production of the coaxial nozzle.

The methodology followed has produced coaxial fibres with concentricity values as low as 2.89 per cent and also identifies a clear speed suitable for coaxial printing using polylactic acid (PLA) as the internal and external materials.

The concentricity of the printed fibres is heavily influenced by the feed rate for the thermoplastic feedstock. This in turn alters the viscosity of the material to be printed, implying that a relationship exists between feed rate and print temperature, which can be further optimised to potentially obtain higher concentricity values.

This paper adds reliability and repeatability to the production of coaxially printed structures, the likes of which has numerous potential applications for biological printing.

The outcomes of this study will provide an AM platform to alter the paradigm of biofabrication by introducing a new level of versatility to the construction of biofabricated structures.

This paper aims to provide a review of four-dimensional (4D) printing using fused-deposition modeling (FDM). 4D printing is an emerging innovation in (three-dimensional) 3D printing that encompasses active materials in the printing process to create not only a 3D object but also a 3D object that can perform an active function. FDM is the most accessible form of 3D printing. By providing a review of 4D printing with FDM, this paper has the potential in educating the many FDM 3D printers in an additional capability with 4D printing.

This is a review paper. The approach was to search for and review peer-reviewed papers and works concerning 4D printing using FDM. With this discussion of the shape memory effect, shape memory polymers and FDM were also made.

4D printing has become a burgeoning area in addivitive manufacturing research with many papers being produced within the past 3-5 years. This is especially true for 4D printing using FDM. The key findings from this review show the materials and material composites used for 4D printing with FDM and the limitations with 4D printing with FDM.

Limitations to this paper are with the availability of papers for review. 4D printing is an emerging area of additive manufacturing research. While FDM is a predominant method of 3D printing, it is not a predominant method for 4D printing. This is because of the limitations of FDM, which can only print with thermoplastics. With the popularity of FDM and the emergence of 4D printing, however, this review paper will provide key resources for reference for users that may be interested in 4D printing and have access to a FDM printer.

Practically, FDM is the most popular method for 3D printing. Review of 4D printing using FDM will provide a necessary resource for FDM 3D printing users and researchers with a potential avenue for design, printing, training and actuation of active parts and mechanisms.

Continuing with the popularity of FDM among 3D printing methods, a review paper like this can provide an initial and simple step into 4D printing for researchers. From continued research, the potential to engage general audiences becomes more likely, especially a general audience that has FDM printers. An increase in 4D printing could potentially lead to more designs and applications of 4D printed devices in impactful fields, such as biomedical, aerospace and sustainable engineering. Overall, the change and inclusion of technology from 4D printing could have a potential social impact that encourages the design and manufacture of such devices and the treatment of said devices to the public.

There are other 4D printing review papers available, but this paper is the only one that focuses specifically on FDM. Other review papers provide brief commentary on the different processes of 4D printing including FDM. With the specialization of 4D printing using FDM, a more in-depth commentary results in this paper. This will provide many FDM 3D printing users with additional knowledge that can spur more creative research in 4D printing. Further, this paper can provide the impetus for the practical use of 4D printing in more general and educational settings.

The purpose of this paper is to fabricate the scaffolds with different pore architectures using additive manufacturing and analyze its mechanical and biological properties for bone tissue engineering applications.

The polylactic acid (PLA)/composite filament were fabricated through single screw extrusion and scaffolds were printed with four different pore architectures, i.e. circle, square, triangle and parallelogram with fused deposition modelling. Afterwards, scaffolds were coated with hydroxyapatite (HA) using dip coating technique. Various physical and thermo-mechanical tests have been conducted to confirm the feasibility. Furthermore, the biological tests were conducted with MG63 fibroblast cell lines to investigate the biocompatibility of the developed scaffolds.

The scaffolds were successfully printed with different pore architectures. The pore size of the scaffolds was found to be nearly 1,500 µm, and porosity varied between 53% and 63%. The fabricated circular pore architecture resulted in highest average compression strength of 13.7 MPa and modulus of 525 MPa. The characterizations showed the fidelity of the work. After seven days of cell culture, it was observed that the developed composites were non-toxic and supported cellular activities. The coating of HA made the scaffolds bioactive, showing higher wettability, degradation and high cellular responses.

The research attempts highlight the development of novel biodegradable and biocompatible polymer (PLA)/bioactive ceramic (Al₂O₃) composite for additive manufacturing with application in the tissue engineering field.

The purpose of this paper is to study the functionality of additively manufactured (AM) parts, mainly depending on their dimensional accuracy and surface finish. However, the products manufactured using AM usually suffer from defects like roughness or uneven surfaces. This paper discusses the various surface quality improvement techniques, including how to reduce surface defects, surface roughness and dimensional accuracy of AM parts.

There are many different types of popular AM methods. Unfortunately, these AM methods are susceptible to different kinds of surface defects in the product. As a result, pre- and postprocessing efforts and control of various AM process parameters are needed to improve the surface quality and reduce surface roughness.

In this paper, the various surface quality improvement methods are categorized based on the type of materials, working principles of AM and types of finishing processes. They have been divided into chemical, thermal, mechanical and hybrid-based categories.

The review has evaluated the possibility of various surface finishing methods for enhancing the surface quality of AM parts. It has also discussed the research perspective of these methods for surface finishing of AM parts at micro- to nanolevel surface roughness and better dimensional accuracy.

This paper represents a comprehensive review of surface quality improvement methods for both metals and polymer-based AM parts.

The limited strength of polylactic acid (PLA) hinders its extensive engineering applications. This paper aims to enhance its strength and realize diverse applications.

Here, the continuous fiber reinforced PLA composites are fabricated by a customized fused filament fabrication three-dimensional printer. Uniaxial tensile and three-point flexural tests have been conducted to analyze the reinforcement effect of the proposed composites. To unveil the adhering mechanism of optic fiber (OF) and PLA, post failure analysis including the micro imaging and morphology have been performed. The underlying mechanism is that the axial tensile strength of the OF and the interfacial adhesion between PLA and OF compete to enhance the mechanical properties of the composite.

It is found that 10%–20% enhancement of strength, ductility and toughness due to the incorporation of the continuous OF.

The continuous OFs are put into PLA first time to improve the strength. The fabrication method and process reported here are potentially applied in such engineering applications as aerospace, defense, auto, medicine, etc.

The purpose of this study is to investigate the thermoforming process of 3D-printed parts made from polylactic acid (PLA) and explore its application in producing wrist-hand orthoses. These orthoses were 3D printed flat, heated and molded to fit the patient’s hand. The advantages of such an approach include reduced production time and cost.

The study used both experimental and numerical methods to analyze the thermoforming process of PLA parts. Thermal and mechanical characteristics were determined at different temperatures and infill densities. An equivalent material model that considers infill within a print is proposed. Its practical use was proven using a coupled finite-element analysis model. The simulation strategy enabled a comparative analysis of the thermoforming behavior of orthoses with two designs by considering the combined impact of natural convection cooling and imposed structural loads.

The experimental results indicated that at 27°C and 35°C, the tensile specimens exhibited brittle failure irrespective of the infill density, whereas ductile behavior was observed at 45°C, 50°C and 55°C. The thermal conductivity of the material was found to be linearly related to the temperature of the specimen. Orthoses with circular open pockets required more time to complete the thermoforming process than those with hexagonal pockets. Hexagonal cutouts have a lower peak stress owing to the reduced reaction forces, resulting in a smoother thermoforming process.

This study contributes to the existing literature by specifically focusing on the thermoforming process of 3D-printed parts made from PLA. Experimental tests were conducted to gather thermal and mechanical data on specimens with two infill densities, and a finite-element model was developed to address the thermoforming process. These findings were applied to a comparative analysis of 3D-printed thermoformed wrist-hand orthoses that included open pockets with different designs, demonstrating the practical implications of this study’s outcomes.

This paper aims to understand the effect of extrusion conditions on the degree of foaming of polylactic acid (PLA) during three-dimensional (3D) printing. It was also targeted to optimize the slicing parameters for 3D printing and to study how the properties of printed parts are influenced by the extrusion conditions.

This study used a commercially available PLA filament that undergoes chemical foaming. An extrusion 3D printer was used to produce individual extrudates and print samples that were characterized using an optical microscope, scanning electron microscope and custom in-house apparatuses.

The degree of foaming of the extrudates was found to strongly depend on the extrusion temperature and the material feed speed. Higher temperatures significantly increased the number of nucleation sites for the blowing agent as well as the growth rate of micropores. Also, as the material feed speed increased, the micropores were allowed to grow bigger which resulted in higher degrees of foaming. It was also found that, as the degree of foaming increased, the porous parts printed with optimized slicing parameters were lightweight and thermally less conductive.

This study fills the gap in literature where it examines the foaming behavior of individual extrudates as they are extruded. By doing so, this work distinguishes the effect of extrusion conditions from the effect of slicing parameters on the foaming behavior which enhances the understanding of extrusion of chemically foamed PLA.

The purpose of this study is to investigate the influences of extruder temperatures and raster orientations on the mechanical properties of polylactic-acid (PLA) material processed by using fused filament fabrication (FFF).

In this research, the PLA specimens were first printed with nozzle or extruder temperatures of 205°C, 215°C and 225°C and then evaluated in terms of their physical, chemical and mechanical properties. An appropriate extruder temperature was then selected based on this experiment and used for the printing of the other PLA specimens having various raster orientations. A series of tensile tests were carried out again to investigate the influence of raster orientations on the tensile strength, tensile strain and elastic modulus of those FFF-processed PLA materials. In the end, the one-way ANOVA was applied for the statistical analysis and the Mohr’s circle was established to aid in the analysis of the data obtained in this experiment.

The result of this study shows that the chemistry, porosity, degree of crystallinity and mechanical properties (tensile strength, strain and elastic modulus) of the PLA material printed with a raster angle of 0° were all insensitive to the increasing extruder temperature from 205°C to 225°C. Meanwhile, the mechanical properties of such printed PLA material were obviously influenced by its raster orientation. In this case, a PLA material with a raster orientation parallel to its loading axis, i.e. those with a raster angle of θ = 0°, was found as the strongest material. Meanwhile, the raster configuration-oriented perpendicular to its loading axis or θ = 90° yielded the weakest PLA material. The results of the tensile tests for the PLA material printed with bidirectional raster orientations, i.e. θ = 0°/90° and 45°/−45° demonstrated their strengths with values falling between those of the materials having unidirectional raster θ = 0° and 90°. Furthermore, the result of the analysis by using a well-known Mohr’s circle confirmed the experimental tensile strengths and the failure mechanisms of the PLA material that had been printed with various raster orientations.

This study presented consistent results on the chemistry, physical, degree of crystallinity and mechanical properties of the FFF-processed PLA in responding to the increasing extruder temperature from 205°C to 225°C applied during the printing process. Unlike the results of the previous studies, all these properties were also found to be insensitive to the increase of extruder temperature. Also, the result of this research demonstrates the usability of Mohr’s circle in the analysis of stresses working on an FFF-processed PLA material in responding to the changes in raster orientation printed in this material.