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This paper aims to investigate the effects of epoxy resin on the rheological and mechanical properties and water absorption rate of wood flour/high-density polyethylene (HDPE) composites (wood-plastic composite [WPC]).

The reactive mixing of various epoxy resins with 60 Wt.% wood flour and HDPE was carried out in a twin-screw extruder with a special screw element arrangement. Polyethylene-grafted maleic anhydride (MAPE) was used as a coupling agent to improve the interfacial interaction between wood flour, epoxy resin and HDPE.

The tensile, flexural and impact properties of the composites increased initially and then decreased with the increasing content of epoxy resin. The complex viscosity decreased with increasing epoxy resin content, but a trend reversal was observed at 8 Wt.% epoxy resin. The epoxy resin-modified wood-HDPE composites chemically coupled by MAPE showed minimal water absorption.

The cured epoxy resins impart high-aspect-ratio and plate-like polymeric fillers, affect the rheological behavior of the WPC and can also be oriented in a flow direction. Epoxy resin has good interaction with the cellulose structure of wood flour because of the polar functional groups within the cellulose.

This method provided a simple and practical solution to improve the performance of WPC.

The WPC modified by epoxy resin in this study had high performance in rheological and mechanical properties, and thus can be widely used for domestic, packaging and automotive applications.

The purpose of this paper is to study the effects of water immersion‐freeze‐thaw treatment on the physical properties, flexural strength (FS) and morphology of wood‐polypropylene composites containing pigments.

Wood‐polypropylene composites containing brown, green and grey pigments were compounded in a conical twin‐screw extruder. A composite manufactured without any pigment addition was used as a reference. The amount of pelletized wood, polypropylene and coupling agent (MAPP) was kept constant. The moisture content, thickness swelling (TS), FS and surface colour of the composites were measured before and after water immersion‐freeze‐thaw cycling. Scanning electron microscopy (SEM) was used to study the morphology of the composites.

FS and dimensional stability were reduced after exposure to water immersion‐freeze‐thaw cycling for all composites. The surface properties (colour and roughness) of the composites also changed after exposure to water immersion‐freeze‐thaw cycling. The degree of change depended on the presence of pigment and the type of polypropylene (neat or recycled), however.

This study is a part of an ongoing study on weathering of wood‐polymer composites (WPC) containing different additives. The results of this study were obtained from accelerated laboratory experiments.

Inorganic pigments are widely used as additives in plastics, because they have an excellent UV absorption, good IR‐reflective properties and heat stability. The research revealed that metal‐containing pigments had an effect on degradation in quality of wood‐polypropylene composites exposed to water immersion‐freeze‐thaw cyclic treatment. The addition of metal‐containing pigments to composite formulation resulted in a higher susceptibility of wood‐polypropylene composites to water absorption, and as a consequence to a higher drop of FS compared to composites made without pigment. The polymer matrix plays an important role in the protection of WPC against weathering.

This paper will help in understanding possible problems in the durability of wood‐polypropylene composites compounded with metal‐based pigments when they are exposed to water immersion‐freeze‐thaw cyclic treatment.

To investigate the effects of moisture and freeze‐thaw cycling on the absorption and flexural properties of rice‐hull‐polyethylene (PE) composite.

Various rice‐hull‐PE composite specimens were submerged in water at various temperatures and subjected to various freeze‐thaw cycles. Various characterisations including water absorption, bending strength and stiffness, Fourier transform infrared spectroscopy and scanning electron microscope imaging were performed.

High temperatures accelerated the water sorption of the rice‐hull‐PE composite and increased the equilibrium moisture content. The uncoated surface was not significantly more easily permeated than the coated surface, contrary to expectations. However, more water was absorbed from the cut surface than from the original extruded surface. This was attributed to the tiny checks left on the surface by the sawing action, which indicated the importance of protecting the original surface layer from scraping or other damage. Bending strength and stiffness of the rice‐hull‐PE composite decreased significantly after the freeze‐thaw cycling treatment. The modulus of elasticity decreased more than the modulus of rupture. Compared to the effect of water immersion alone, freeze‐thaw cycling treatment slightly accelerated this decrease.

The results of this study were obtained from accelerated laboratory experiments. Further research could be carried out to evaluate the properties of this rice‐hull‐PE composite in practical application.

The research revealed a possible degradation in quality when the rice‐hull‐PE composite is used in moist or freezing conditions. The resin layer on the extruded surface provides an important protection.

In China, rice‐hull powder is widely used as a reinforcing component in plastic composite. However, the durability of rice‐hull/PE composites has rarely been investigated. Results from this study will help users apply rice‐hull‐PE composites correctly and encourage the development of other agro‐fibre/polymer materials.

The purpose of this study is to manufacture composites from sawdust and polymer high-density polyethylene (HDPE) with different loading from alum as natural and cheap flame retardant and subsequently characterized using standard analytical tools.

Artificial wood plastic composites (WPCs) were prepared by mixing HDPE with sawdust as a filler with constant ratio (2:1) using hot press. Polyethylene-graft-maleic anhydride (PE-g-MAH) used as a coupling agent between two parents of the composites with different ratios (2.5, 5, 7 and 10). Alum as a flame retardant was incorporated into HDPE with 5 phr polyethylene grafted with maleic anhydride (PE-g-MAH) with different ratios (10, 15 and 20). Flame retardant efficiency was investigated using differential scanning calorimetry, thermal gravimetric analysis and the technique of ASTM E162.

The results revealed that the composite containing 5 phr from (PE-g-MAH) exhibited higher mechanical properties and this proved that (PE-g-MAH) act as an efficient coupling agent using the aforementioned ratio. The results also revealed that incorporation of alum as a flame retardant increased the thermal stability of the composites.

Artificial WPCs are ecofriendly materials with a wide range of applications in the constructions field. Moreover, they have high mechanical and physical properties with low cost. Evaluate alum as a natural and cheap flame retardant.

This paper aims to investigate the flexural properties i.e. the flexural strength and the flexural modulus under the influence of selected input variables, namely; fiber type, fiber loading and fiber size in fabricated natural fiber polymeric composites through using Taguchi’s design of experiment methodology.

The Taguchi’s design of experiment approach has been used to scheme a suitable combination to fabricate the polymeric composites. Pure polypropylene (PP) has been chosen as a matrix material, whereas two types of fibers, namely; wood powder (WP) i.e. sawdust and rice husk powder (RHP), have been used as a reinforcement in the matrix. Microstructure analysis of fabricated and tested samples has also been evaluated and analyzed using a scanning electron microscope. This analysis has divulged that at moderate fiber size and higher fiber loading, no gap or cavities presented between the fillers and matrix particles, which illustrates the good interfacial bonding between the materials.

The flexural strength of the wood powder pure polypropylene (WPPP) composite decreases if the fiber content gets increased beyond 20 Wt.%. In addition, the flexural strength of hybrid composite (WPRHPPP) has been revealed to get improved more in comparison to composites with single fiber as reinforcement. Furthermore, the flexural modulus of WPPP composite has also increased with the increase in fiber loading. It has been concluded that reinforcement size plays an imperative role in influencing the flexural modulus. The optimum parametric setting for the flexural strength and the flexural modulus has been devised as; fiber type – WPRHP, fiber loading – 10 Wt.% and fiber size – 600 µm; and fiber type – WP, fiber loading – 30 Wt.% and fiber size – 1,180 µm, respectively. The microstructure images clearly revealed that during conducted flexural tests, some particles get disturbed from their bonded position that mainly represents the plastic deformation.

The fabricated polymer materials proposed in the research work are green and environmentally friendly.

The natural fiber-based composites are possessing wide-spread requirements in today’s competitive structure of manufacturing and industrial applications. The fabrication of the natural fiber-based composites has also been planned through the designed experiments (namely; Taguchi Methodology- L₉ orthogonal array matrix), which, further, makes the analysis more fruitful and qualitative too. The fabricated polymer materials proposed in the research work are green and environmentally friendly. Shisham WP has been rarely used in the past researches; therefore, this factor has been included for the present work. The injection molding process is used to fabricate the three different polymer composite by varying the fiber weight percentage and fiber size.

This paper aims to summarize the up-to-date research performed on combinations of various biofibers and resin systems used in different three-dimensional (3D) printing technologies, including powder-based, material extrusion, solid-sheet and liquid-based systems. Detailed information about each process, including materials used and process design, are described, with the resultant products’ mechanical properties compared with those of 3D-printed parts produced from pure resin or different material combinations. In most processes introduced in this paper, biofibers are beneficial in improving the mechanical properties of 3D-printed parts and the biodegradability of the parts made using these green materials is also greatly improved. However, research on 3D printing of biofiber-reinforced composites is still far from complete, and there are still many further studies and research areas that could be explored in the future.

The paper starts with an overview of the current scenario of the composite manufacturing industry and then the problems of advanced composite materials are pointed out, followed by an introduction of biocomposites. The main body of the paper covers literature reviews of recently emerged 3D printing technologies that were applied to biofiber-reinforced composite materials. This part is classified into subsections based on the form of the starting materials used in the 3D printing process. A comprehensive conclusion is drawn at the end of the paper summarizing the findings by the authors.

Most of the biofiber-reinforced 3D-printed products exhibited improved mechanical properties than products printed using pure resin, indicating that biofibers are good replacements for synthetic ones. However, synthetic fibers are far from being completely replaced by biofibers due to several of their disadvantages including higher moisture absorbance, lower thermal stability and mechanical properties. Many studies are being performed to solve these problems, yet there are still some 3D printing technologies in which research concerning biofiber-reinforced composite parts is quite limited. This paper unveils potential research directions that would further develop 3D printing in a sustainable manner.

This paper is a summary of attempts to use biofibers as reinforcements together with different resin systems as the starting material for 3D printing processes, and most of the currently available 3D printing techniques are included herein. All of these attempts are solutions to some principal problems with current 3D printing processes such as the limit in the variety of materials and the poor mechanical performance of 3D printed parts. Various types of biofibers are involved in these studies. This paper unveils potential research directions that would further widen the use of biofibers in 3D printing in a sustainable manner.

Wetting wood plastic composites (WPCs) prior to testing can be challenging because of the inherent water repellency of the plastic. The purpose of this paper is to explore the use of heating and wetting to accelerate moisture uptake on two WPCs.

Full size samples of the two WPCs were immersed in water at various temperatures or heated in an autoclave. Samples were removed periodically and dissected to determine the moisture profile by oven drying and weighing.

Moisture uptake is accelerated by heating, but the effect is mainly confined to the outer 5 mm of the samples. Moisture levels deeper in the samples are largely unaffected.

Moisture uptake can be enhanced by heating, but the inability to increase moisture levels deeper in the wood suggests that tests assessing the role of moisture on WPC properties should use thinner specimens to ensure that moisture is well distributed in the materials.

The results suggest the need for a re‐evaluation of test methodologies for WPCs where moisture uptake is an integral part of the procedures to more closely align the methods to the WPC/moisture behaviour.

This paper will help researchers develop better methods for assessing the role of moisture in WPC behaviour.

The growing environmental awareness all through the world has motivated a standard change toward planning and designing better materials having good performance, which are very much suited to the environmental factors. The purpose of this study is to investigate the impact on mechanical, thermal and water absorption properties of sawdust-based composites reinforced by epoxy, and the amount of sawdust in each form.

Manufacturing of the sawdust reinforced epoxy composites is the main area of the research for promoting the green composite by having good mechanical properties, biodegradability or many applications. Throughout this research work, the authors emphasize the importance of explaining the methodology for the evaluation of the mechanical and water absorption properties of the sawdust reinforced epoxy composites used by researchers.

In this paper, a comprehensive review of the mechanical properties of sawdust reinforced epoxy composite is presented. This study is reported about the use of different Wt.% of sawdust composites prepared by different processes and their mechanical, thermal and water absorption properties. It is studied that after optimum filler percentage, mechanical, thermal properties gradually decrease, but water absorption property increases with Wt.% of sawdust. The changes in the microstructure are studied by using scanning electron microscopy.

The novelty of this study lies in its use of a systematic approach that offers a perspective on choosing suitable processing parameters for the fabrication of composite materials for persons from both industry and academia. A study of sawdust reinforced epoxy composites guides new researchers in the fabrication and characterization of the materials.

The purpose of this study is to carry out an investigation of the role of the wood particle size on the mechanical properties of poly lactic acid (PLA)-reinforced neem fiber biocomposite.

Composite test specimens were processed by reinforcing neem wood flour (NWF) in two different particle sizes, micro-sized NWF (MNWF) and nano-sized NWF (NNWF) separately into PLA. Composites were extruded at four different fiber loadings (10, 15, 20 and 25 Wt.%) into PLA matrix. The MNWF and NNWF had particle sizes varying from 5 to 15 µm and 10 to 15 nm, respectively.

Tensile strength, flexural strength and impact strength of PLA increased with fiber reinforcement for both the MNWF and NNWF cases. The NNWF-reinforced PLA composite at 20 Wt.% fiber loading proved to be the best composite that had outstanding mechanical properties in this research.

The developed composite can be used as a substitute for conventional plywood for furniture, building infrastructure and interior components for the automobile, aircraft and railway sectors.

A new biocomposite had been fabricated by using PLA and NWF and had been tested for its mechanical characteristics.

A pine/co-PES composite (PCPES composite) was proposed as the feedstock for powder bed fusion (laser sintering, LS). This paper aims to provide some necessary experimental data and the theoretical foundation for LS of pine/co-PES, especially for the application of using the laser-sintered pine/co-PES parts as complex structural patterns in investment casting.

The PCPES composites with different pine loadings were mixed mechanically. The composite’s preheating temperature and processing temperature during LS were determined experimentally based on the material’s thermal behavior. The effects of pine powder on the binding mechanism of PCPES composites were discussed through analyzing the microstructure of the laser-sintered parts’. Mechanical properties and dimensional precision of laser-sintered PCPES parts in different pine loadings were tested, and the parts’ mechanical properties were strengthened by wax-infiltration post-processing. The influence extents of process parameters on the mechanical properties of laser-sintered 20 Wt.% pine/co-PES parts were investigated using a 1/2 fractional factorials experiment.

20 Wt.% pine/co-PES is considered to be a promising wood-plastic composite for laser sintering. The relationship between mechanical strength of its laser-sintered parts and process parameters was built up using mathematical formulas. Experimental results show density, tensile strength, flexural strength and surface roughness of laser-sintered 20 Wt.% pine/co-PES parts are improved by 72.7-75.0%, 21.9-111.3%, 26.8-86.2%, 27.0-29.1% after post-process infiltration with a wax. A promising application of the wax-infiltrated laser-sintered parts is for investment casting cores and patterns.

The proper process parameters and forming properties of laser-sintered parts are limited to the results of laser sintering experiments carried on using AFS 360 rapid prototyping device.

This investigation not only provides a new feedstock for laser sintering with the advantages of low cost and fabricability but also uses an advanced technique to produce personalized wood-plastic parts efficiently. Mathematical models between mechanical properties of laser-sintered PCPES parts and LS process parameters will guide the further LS experiments using the 20 Wt.% pine/co-PES composite. Besides, the laser-sintered PCPES parts after wax-infiltration post-processing are promising as complex structural patterns for use in investment casting.