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The purpose of this study is to investigate the thermomechanical condition on the shape memory property of Polybutylene adipate-co-terephthalate (PBAT). PBAT is a widely researched and rapidly developed biodegradable copolyester. In a tensile test, we found that the fractured PBAT samples had a heat-driven shape memory effect which piqued our interest, and it will lay a foundation for the application of PBAT in new fields (such as heat shrinkable film).

The shape memory effect of PBAT and the effect of the thermomechanical condition on its shape memory property were confirmed and systematically investigated by a thermal mechanical analyzer and tensile machine.

The results showed that the PBAT film had broad shape memory transform temperature and exhibited excellent thermomechanical stability and shape memory properties. The shape memory fixity ratio (Rf) of the PBAT films was increased with the prestrain temperature and prestrain, where the highest Rf exceeded 90%. The shape memory recovery ratio (Rr) of the PBAT films was increased with the shape memory recovery temperature and decreased with the prestrain value, and the highest Rr was almost 100%. Moreover, the PBAT films had high shape memory recovery stress which increased with the prestrain value and decreased with the prestrain temperature, and the highest shape memory recovery stress can reach 7.73 MPa.

The results showed that PBAT had a broad shape memory transform temperature, exhibited excellent thermomechanical stability and shape memory performance, especially for the sample programmed at high temperature and had a larger prestrian, which will provide a reference for the design, processing and application of PBAT-based heat shrinkable film and smart materials.

This study confirmed and systematically investigated the shape memory effect of PBAT and the effect of the thermomechanical condition on the shape memory property of PBAT.

Thermomechanical behavior of intermediate-size beam-to-wall assemblies including Glulam-beams connected to cross-laminated timber (CLT) walls with T-shape steel doweled connections was investigated at ambient temperature (AT) and after and during non-standard fire exposure.

Three AT tests were conducted to evaluate the load-carrying capacity and failure modes of the assembly at room temperature. Two post-fire performance (PFP) tests were performed to study the impact of 30-min (PFP30) and 60-min (PFP60) partial exposure to a non-standard fire on the residual strength of the assemblies. The assemblies were exposed to fire in a custom-designed frame, then cooled and loaded to failure. A fire performance (FP) test was conducted to study the fire resistance (FR) during non-standard fire exposure by simultaneously applying fire and a mechanical load equal to 65% of the AT load carrying capacity.

At AT, embedment failure of the dowels followed by splitting failure at the Glulam-beam and tensile failure of the epoxy between the layers of CLT-walls were the dominant failure modes. In both PFP tests, the plastic bending of the dowels was the only observed failure mode. The residual strength of the assembly was reduced 14% after 30 min and 37% after 60 min of fire exposure. During the FP test, embedment failure of timber in contact with the dowels was the only major failure mode, with the maximum rate of displacement at 51 min into the fire exposure.

This is the first time that the thermomechanical performance of such an assembly with a full-contact connection is presented.

This study aims to investigate the reliability issues of microvoid cracks in solder joint packages exposed to thermal cycling fatigue.

The specimens are subjected to JEDEC preconditioning level 1 (85 °C/85%RH/168 h) with five times reflow at 270°C. This is followed by thermal cycling from 0°C to 100°C, per IPC-7351B standards. The specimens' cross-sections are inspected for crack growth and propagation under backscattered scanning electronic microscopy. The decoupled thermomechanical simulation technique is applied to investigate the thermal fatigue behavior. The impacts of crack length on the stress and fatigue behavior of the package are investigated.

Cracks are initiated from the ball grid array corner of the solder joint, propagating through the transverse section of the solder ball. The crack growth increases continuously up to 0.25-mm crack length, then slows down afterward. The J-integral and stress intensity factor (SIF) values at the crack tip decrease with increased crack length. Before 0.15-mm crack length, J-integral and SIF reduce slightly with crack length and are comparatively higher, resulting in a rapid increase in crack mouth opening displacement (CMOD). Beyond 0.25-mm crack length, the values significantly decline, that there is not much possibility of crack growth, resulting in a negligible change in CMOD value. This explains the crack growth arrest obtained after 0.25-mm crack length.

This work's contribution is expected to reduce the additional manufacturing cost and lead time incurred in investigating reliability issues in solder joints.

The work investigates crack propagation mechanisms of microvoid cracks in solder joints exposed to moisture and thermal fatigue, which is still limited in the literature. The parametric variation of the crack length on stress and fatigue characteristics of solder joints, which has never been conducted, is also studied.

This study aims to develop a four-dimensional (4D) textile composite that self-forms upon thermal stimulation while eliminating thermomechanical programming steps by using fused deposition modeling (FDM) 3D printing technology, and tries to refine the product development path for this composite.

Polylactic acid (PLA) printing filaments were deposited on prestretched Lycra-knitted fabric using desktop-level FDM 3D printing technology to construct a three-layer structure of thermally responsive 4D textiles. Subsequently, the effects of different PLA thicknesses and Lycra knit fabric relative elongation on the permanent shape of thermally responsive 4D textiles were studied. Finally, a simulation program was written, and a case in this study demonstrates the usage of thermally responsive 4D textiles and the simulation program to design a wrist support product.

The constructed three-layer structure of PLA and Lycra knitted fabric can self-form under thermal stimulation. The material can also achieve reversible transformation between a permanent shape and multiple temporary shapes. Thinner PLA deposition and higher relative elongation of the Lycra-knitted fabric result in the greater curvature of the permanent shape of the thermally responsive 4D textile. The simulation program accurately predicted the permanent form of multiple basic shapes.

The proposed method enables 4D textiles to directly self-form upon thermal, which helps to improve the manufacturing efficiency of 4D textiles. The thermal responsiveness of the composite also contributes to building an intelligent human–material–environment interaction system.

The purpose of this study is to quantify the vertical shrinkage rates and the mechanical strength of three-dimensional (3D) printed parts for a variety of wood-based materials for liquid deposition modeling.

The overall hypothesis was that a well-chosen combination of binders, fibers and fillers could reduce shrinkage in the Z dimension and increase compressive and flexural strength (DIN 52185, 52186). To test this assumption, eight sub-hypotheses were formulated. Mixtures of the ingredients were chosen in different ratios to measure the performance of prints. For time efficiency, an iterative heuristic approach was used – not testing all variations of all variables in even increments, but cutting off lines of testing when mixtures were clearly performing poorly.

The results showed that some mixtures had high dimensional accuracy and strength, while others had neither, and others had one but not the other. Shrinkage of 3D printed objects was mainly caused by water release during drying. An increase of the wood as well as the cement, sand, salt and gypsum content led to reduced vertical shrinkage, which varied between 0 and 23%. Compressive and flexural strength showed mixed trends. An increase in wood and salt content worsened both strength properties. The addition of fibers improved flexural, and the addition of cement improved compression strength. The highest strength values of 14 MPa for compressive and 8 MPa for flexural strength were obtained in the test series with gypsum.

This paper is an important milestone in the development of environmentally friendly materials for additive manufacturing. The potential of many ingredients to improve physical properties could be demonstrated.

This study delineates the effect of cover thickness on reinforced concrete (RC) columns and beams under an elevated fire scenario. Columns and beams are important load-carrying structural members of buildings. Under all circumstances, the columns and beams were set to be free from damage to avoid structural failure. Under the high-temperature scenario, the RC element may fail because of the material deterioration that occurs owing to the thermal effect. This study attempts to determine the optimum cover thickness for beams and columns under extreme loads and fire conditions.

Cover thicknesses of 30, 40, 45, 50, 60 and 70 mm for the columns and 10, 20, 25, 30, 35, 40, 50, 60 and 70 mm for the beams were adopted in this study. Both steady-state and transient-state conditions under thermomechanical analysis were performed using the finite element method to determine the heat transfer through the RC section and to determine the effect of thermal stresses.

The results show that the RC elements have a greater influence on the additional cover thickness at extreme temperatures and higher load ratios than at the service stages. The safe limits of the structural members were obtained under the combined effects of elevated temperatures and structural loads. The results also indicate that the compression members have a better thermal performance than the flexural members.

Numerical investigations concerning the high-temperature behavior of structural elements are useful. The lack of an experimental setup encourages researchers to perform numerical investigations. In this study, the finite element models were validated with existing finite element models and experimental results.

The obtained safe limit for the structural members could help to understand their resistance to fire in a real-time scenario. From the safe limit, a suitable design can be preferred while designing the structural members. This could probably save the structure from collapse.

There is a lack of both numerical and experimental research works. In numerical modeling, the research works found in the literature had difficulties in developing a numerical model that satisfactorily represents the structural members under fire, not being able to adequately understand their behavior at high temperatures. None of them considered the influence of the cover thickness under extreme fire and loading conditions. In this paper, this influence was evaluated and discussed.

The purpose of this paper is to assess the feasibility of analytical models, specifically the radial basis function method, Akbari–Ganji method and Gaussian method, in conjunction with the finite element method. The aim is to examine the impact of processing parameters on temperature history.

Through analytical investigation and finite element simulation, this research examines the influence of processing parameters on temperature history. Simufact software with a thermomechanical approach was used for finite element simulation, while radial basis function, Akbari–Ganji and Gaussian methods were used for analytical modeling to solve the heat transfer differential equation.

The accuracy of both finite element and analytical methods was validated with about 90%. The findings revealed direct relationships between thermal conductivity (from 100 to 200), laser power (from 400 to 800 W), heat source depth (from 0.35 to 0.75) and power absorption coefficient (from 0.4 to 0.8). Increasing the values of these parameters led to higher temperature history. On the other hand, density (from 7,600 to 8,200), emission coefficient (from 0.5 to 0.7) and convective heat transfer (from 35 to 90) exhibited an inverse relationship with temperature history.

The application of analytical modeling, particularly the utilization of the Akbari–Ganji, radial basis functions and Gaussian methods, showcases an innovative approach to studying directed energy deposition. This analytical investigation offers an alternative to relying solely on experimental procedures, potentially saving time and resources in the optimization of DED processes.

Even though it is widely used, reinforced concrete (RC) is susceptible to damage from various environmental factors. The hazard of a fire attack is particularly severe because it may cause the whole structure to collapse. Furthermore, repairing and strengthening existing structures with high-performance concrete (HPC) has become essential from both technical and financial points of view. In particular, studying the postfire behavior of HPC with normal strength concrete substrate requires experimental and numerical investigations. Accordingly, this study aims to numerically investigate the post-fire behavior of reinforced composite RC slabs.

Consequently, in this study, a numerical analysis was carried out to ascertain the flexural behavior of simply supported RC slabs strengthened with HPC and exposed to a particularly high temperature of 600°C for 2 h. This behavior was investigated and analyzed in the presence of a number of parameters, such as HPC types (fiber-reinforced, 0.5% steel, polypropylene fibers [PPF], hybrid fibers), strengthening side (tension or compression), strengthening layer thickness, slab thickness, boundary conditions, reinforcement ratio and yield strength of reinforcement.

The results showed that traction-separation and full-bond models can achieve accuracy compared with experimental results. Also, the fiber type significantly affects the postfire performance of RC slab strengthened with HPC, where the inclusion of hybrid fiber recorded the highest ultimate load. While adding PPF to HPC showed a rapid decrease in the load-deflection curve after reaching the ultimate load.

The proposed model accurately predicted the thermomechanical behavior of RC slabs strengthened with HPC after being exposed to the fire regarding load-deflection response, crack pattern and failure mode. Moreover, the considered independent parametric variables significantly affect the composite slabs’ behavior.

Shape memory materials are functional materials having a good number of applications due to their unique features of programmable material technology such as self-stretching, self-assembly and self-tightening. Advancements in today’s technology led to the easy fabrication of such novel materials using 3D printing techniques. When an external stimulus causes a 3D printed specimen to change shape on its own, this process is known as 4D printing. This study aims to investigate the effect of graphene nano platelet (GNPs) on the shape memory behaviour of shape memory photo polymer composites (SMPPCs) and to optimize the shape-changing response by using the Taguchi method.

SMPPCs are synthesized by blending different weight fractions (Wt.%) of flexible or soft photopolymer (FPP) resin with hard photopolymer (HPP) resin, then reinforced with GNPs at various Wt.% to the blended PP resin, and then fabricated using masked stereolithography (MSLA) apparatus. The shape memory test is conducted to assess the shape recovery time (T), shape fixity ratio (R_f), shape recovery ratio (R_r) and shape recovery rate (V_r) using Taguchi analysis by constructing an L9 orthogonal array with parameters such as Wt.% of a blend of FPP and HPP resin, Wt.% of GNPs and holding time.

SMPPCs with A3, B3 and C2 result in a faster T with 2 s, whereas SMPPCs with A1, B1 and C3 result in a longer T with 21 s. The factors A and B are ranked as the most significant in the Pareto charts that were obtained, whereas C is not significant. It can be seen from the heatmap plot that when factors A and B increase, T is decreasing and V_r is increasing. The optimum parameters for T and V_r are A3, B3 and C2 at the same time for R_f and R_r are A1, B3 and C1.

Faster shape recovery results from a higher Wt.% of FPP resin in a blend than over a true HPP resin. This is because the flexible polymer links in FPP resin activate more quickly over time. However, a minimum amount of HPP resin also needs to be maintained because it plays a role in producing higher R_f and V_r. The use of GNPs as reinforcement accelerates the T because nanographene conducts heat more quickly, releasing the temporary shape of the specimen more quickly.

The use of FPP and HPP resin blends, fabricating the 4D-printed SMPPCs specimens with MSLA technology, investigating the effect of GNPs and optimizing the process parameters using Taguchi and the work was validated using confirmation tests and regression analysis, which increases the originality and novelty.

This study aims to produce homogenously prepared polymer composites by adding two different strontium aluminate derivatives (Sr4Al14O25 and SrAl2O4) to urea-formaldehyde (UF) at different mass concentrations. In the context of this work those strontium-based derivatives were compared in terms of mechanical and luminescent characteristics. Additionally, sodium bicarbonate was integrated with the prepared composites to eliminate/minimize darkening problem, which might arise from the oxidation of Eu +2 to Eu2O3, on the surface of strontium aluminate/urea-formaldehyde composites.

In this study, strontium aluminate/UF composite materials were produced using a compression molding technique. Their mechanical, thermomechanical and luminescence properties were investigated via various characterization methods. Particle size analysis was used to characterize phosphor derivatives, whereas scanning electron microscopy with energy dispersive X-ray spectroscopy (SEM-EDX) was conducted for morphological examination.

The darkening problem was prevented by the introduction of sodium bicarbonate into the composite systems. Based on the characterization and test results, the only addition of strontium aluminate reduced the mechanical properties. However, it was seen that the introduction of sodium bicarbonate into the composites improved those properties positively. The appropriate amounts of strontium aluminate and sodium bicarbonate were determined by conducting an experimental optimization study. The optimum composition of the composite materials was obtained by introducing 2% phosphor and 3% NaHCO₃.

The approach used in this study has provided a method to solve the darkening problem, which degrades the aesthetic appearance in industrial production.