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The key purpose of this study was to investigate the effects of different ultrasonic irradiation times on the wettability and other properties of the resulting water-based coating. The subject water-based coating was prepared using water-soluble polyester and amino resins by ultrasonic oscillation.

The coating was prepared by polymerising polyester and amino resins in water using ultrasonic oscillation. The coating was baked for 40 seconds at 350°C to coalesce and solidify the film. The contact angle, thermal stability and mechanical properties of the film, as well as the molecular weight (MW) and structure of the polyester resin, were determined.

The contact angle of the coating was found to decrease with ultrasonic irradiation; the mechanical properties and thermal stability were not altered when the irradiation time was longer than 5 hours. The MW of the polyester initially decreased then increased and stabilized with ultrasonic irradiation. The structure of polyester molecule and aggregated state of the solidified coating were not changed by ultrasonic irradiation.

In the study reported here, the effects of different ultrasonic irradiation times were investigated. Results of this research could benefit in-depth understanding of the influence of ultrasonic treatment on polyester resins and polyester coatings and could further promote the development of water-based coatings.

The contact angle of the water-based coating decreased by mechanical means. The effects of ultrasound on microstructure and properties of the coating and resin were discussed in detail.

The purpose of this paper is to show how to precisely control the liquid resin coating thickness in stereolithography (SL).

A vacuum adsorption coating equipment and technology are developed to precisely control the liquid resin coating thickness in SL. Dual‐electrode device is used, so adsorption can be precisely controlled and the electrode polarization can be avoided.

It turns out that the apparatus can control coating thickness effectively, and thickness uniformity is increased remarkably, which induces the standard deviation thickness decrease from 0.00547 to 0.00243 mm, and efficiency of rapid prototyping production increase by 53 percent.

The paper demonstrates that the apparatus can control coating thickness effectively.

This paper aims to exploit shape memory polymer (SMP) composite as multifunctional coatings for protecting substrates from surface wear and bacterial. The efficiency of added nano or micro-sized particles in enhancing the properties of SMP was investigated. This study also attempts to use a low-cost and effective spraying approach to fabricate the coatings. The coatings are expected to have good conformability with the substrate and deliver multi-functional performance, such as wrinkle free, wear resistance, thermal stability and antimicrobial property.

High-performance SMP composite coatings or thin films were fabricated by a home-made continuous spray-deposition system. The morphologies of the coatings were studied using the scanning electron microscope and the transmission electron microscope. The abrasion properties were evaluated by Taber Abraser test, and thermo-gravimetric analysis was carried out to investigate the thermal properties of prepared composites. The antimicrobial property was determined by the inhibition zone method using E. coli. The thermally responsive shape memory effect of the resulting composites was also characterized.

The morphology analysis indicated that the nanoclay was distributed on the surface of the coating which resulted in a significant improvement of the wear property. The wear resistance of the coatings with nanoclay was improved as much as 40 per cent compared with that of the control sample. The thermo-gravimetric analysis revealed that the weight loss rate of composites with nanoclay was dropped over 40 per cent. The SMP coating with zinc oxide (ZnO) showed excellent antimicrobial effect. The shape recovery effect of SMP/nanoclay and SMP/ZnO composites can be triggered by external heating and the composites can reach a full shape recovery within 60 s.

This study proposed a continuous spray-deposition fabrication of SMP composite coatings, which provides a new avenue to prepare novel multi-functional coatings with low cost.

Most studies have emphasized on the sole property of SMP composites. Herein, a novel SMP composite coating which could deliver multi-functionality such as wrinkle free, wear resistance, thermal stability and antimicrobial property was proposed.

Recently, the constrained surface projection stereolithography (SL) technology is gaining wider attention and has been widely used in the 3D printing industry. In constrained surface projection SL systems, the separation of a newly cured layer from the constrained surface is a historical technical barrier. It greatly limits printable size, process reliability and print speed. Moreover, over-large separation force leads to adhesion failures in manufacturing processes, causing broken constrained surface and part defects. Against this background, this paper investigates the formation of separation forces and various factors that affect the separation process in constrained surface projection SL systems.

A bottom-up projection SL testbed, integrated with an in-situ separation force measurement unit, is developed for experimental study. Separation forces under various manufacturing process settings and constrained surface conditions are measured in situ. Additionally, physical models are constructed by considering the liquid resin filling process. Experiments are conducted to investigate influences of manufacturing process settings, constrained surface condition and print geometry on separation forces.

Separation forces increase linearly with the separation speed. The deformation and the oxygen inhibition layer near the constrained surface greatly reduce separation forces. The printing area, area/perimeter ratio and the degree of porousness of print geometries have a combined effect on determining separation forces.

This paper studied factors that influence separation force in constrained surface SL processes. Constrained surface conditions including oxygen inhibition layer thickness, deformation and oxygen permeation capability were investigated, and their influences on separation forces were revealed. Moreover, geometric factors of printing layers that are significant on determining separation forces have been identified and quantified. This study on separation forces provides a solid base for future work on adaptive control of constrained surface projection SL processes.

This paper aims to investigate the wear behaviour of different materials for cylinder liners and piston rings in a linear reciprocating tribometer with special focus on the wear of the cylinder liner in the boundary lubrication regime.

Conventional nitrided steel, as well as diamond-like carbon and chromium nitride-coated piston rings, were tested against cast iron, AlSi and Fe-coated AlSi cylinder liners. The experiments were carried out with samples produced from original engine parts to have the original surface topography available. Radioactive tracer isotopes were used to measure cylinder liner wear continuously, enabling separation of running-in and steady-state wear.

A ranking of the material pairings with respect to wear behaviour of the cylinder liner was found. Post-test inspection of the cylinder samples by scanning electron microscopy (SEM) revealed differences in the wear mechanisms for the different material combinations. The results show that the running-in and steady-state wear of the liners can be reduced by choosing the appropriate material for the piston ring.

The use of original engine parts in a closely controlled tribometer environment under realistic loading conditions, in conjunction with continuous and highly sensitive wear measurement methods and a detailed SEM analysis of the wear mechanisms, forms an intermediate step between engine testing and laboratory environment testing.

Background In the language of the steel industry, the term coated steel means, for all practical purposes, mild steel sheet or strip which is coated before it leaves the steel mill. Various coatings are employed depending upon product end use but basically they divide up into metallic coatings such as tin, zinc or aluminium; and organic coatings which are essentially paints or plastic films. Organic coatings are very often applied on top of metallic coatings, so that in the most advanced coated products there may be as many as five separate layers of material between the underlying steel and the exposed outer surface.

A kind of the Z-6020/E-44 modified waterborne hydroxyl acrylate resin (Z-WEA) and its application in volatile organic compound-free waterborne coatings were prepared.

The Z-6020/E-44 modified waterborne hydroxyl acrylate resin (Z-WEA) was obtained dropwise by adding a mixed solution of methyl methacrylate, n-butyl acrylate, hydroxyethyl methacrylate, acrylic acid and an initiator into a pre-prepared solution of isopropyl alcohol and E-44 and by semi-continuous solution polymerization, and this chain was further extended with organosiloxane (Z-6020) through graft copolymer, which was then neutralized with organic base and dispersed with water, with waterborne amino resin curing agent to form a film, and the properties were tested.

The results showed that when the dosage of initiator was 2.5% accounts for the total acrylic monomer, the hydroxyl content was 10%; the dosage of E-44 was 16%; the dosage of Z-6020 was 6%; the mass ratio of hard and soft monomer was 2.0:1; the neutralization was 100%; Z-6020/E-44 modified waterborne hydroxyl acrylate resin (Z-WEA) had excellent dispersion performance in water and storage stability; water absorption of cured film was 7.8%; pencil hardness reached 5H; adhesive force was 1 level; and the film was uniform and endowed with remarkable heat resistance, high gloss and good fullness.

This paper established a method to synthesize Z-6020/E-44 modified waterborne hydroxyl acrylate resin (Z-WEA) with green surfactants that can be used in the coatings, adhesives, finishing agents and so on.

This paper provides a method of preparing Z-6020/E-44 modified waterborne hydroxyl acrylate resin (Z-WEA) and with waterborne amino resin curing agent to form a film, and the film is uniform and endowed with remarkable heat resistance, high gloss and good fullness and meets the requirements of high-grade paint.

The purpose of this paper is to study the use of titanium as a protecting element for aluminum in alkaline conditions.

Aluminum coatings containing up to 20 weight per cent Ti6Al4V were produced using laser cladding and were investigated using light optical microscope, scanning electron microscope – energy-dispersive X-ray spectroscopy and X-Ray Diffraction, together with alkaline exposure tests and potentiodynamic measurements at pH 13.5.

Cladding resulted in a heterogeneous solidification microstructure containing an aluminum matrix with supersaturated titanium (<1 weight per cent), Al₃Ti intermetallics and large partially undissolved Ti6Al4V particles. Heat treatment lowered the titanium concentration in the aluminum matrix, changed the shape of the Al₃Ti precipitates and increased the degree of dissolution of the Ti6Al4V particles. Corrosion testing showed significant localized dissolution of the aluminum matrix.

Increased titanium concentration and heat treatment gave improved alkaline corrosion properties. At pH 13.5, the Al₃Ti phases were protected, while the aluminum matrix corroded.

For alkaline corrosion-protection of aluminum in the automobile industry, titanium might be useful at pH values below 13.5 or by using other coating techniques.

This is the first study testing the use of titanium as a protective element of aluminum in stringent alkaline conditions.

Nature provides a wide range of structures with different functions, which can serve as a source of research concepts. Based on the bionics principle, a bionic structure was applied to drill pipe specimens to compare the bond strength of paint coatings with and without a bionic ring groove pattern machined on the substrate.

Using the Revetest Xpress Plus scratch tester, the bond strengths of the coatings on the drill pipe with and without the bionic structure were measured and the difference in bond strength was observed.

The critical scratch loads of the surface coatings were 12.77 and 5.4 N. Furthermore, the scratch curve from the plain sample had a larger fluctuation compared to the curve of the samples with bionic ring grooves.

This indicated that the application of a bionic pattern to the surface of the substrate could enhance the bond strength and the degree of mechanical adhesion between the coating and the surface of the drill pipe, which is beneficial for the anti-corrosion performance of the drill pipe.

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