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Dyeing of silk fabric was studied to increase dye uptake using eco-friendly glycerine based eutectic solvent (GES), which acts as a swelling agent.

The swelling behaviour of silk fabric in GES was analyzed using three-dimensional laser scanning microscope. Dyeing parameters such as time, temperature and GES concentration were optimized using design of experiments.

In total, 5.34 F-value and 0.0014 p-value of ANOVA represent that the model is significant. An optimized GES assisted dyeing was carried out with two different classes of dyes such as Acid Blue 281 and Acid Red 151 and further compared with that of conventional aqueous dyeing method.

At 70°C, silk fabric achieves desired colour strength after 35 min of dyeing (10 min lesser than conventional) using GES assisted dyeing method. % Dye exhaustion of GES assisted dye bath was carried out and found to be very good. Fastness properties such as washing, light and rubbing fastness of conventional and GES assisted dyed silk fabric showed comparable results.

This paper aims to focus on the optimisation of dyeing recipe for dyeing of silk fabric with semisynthetic azo dyes synthesised by chemical modification of areca nut extract.

The response surface model (Box–Behnken design) was used to establish the relation between the parameters of dyeing such as time, temperature and material to liquor ratio. Their output responses in terms of colour strength (K/S values) are reported. Their relationship was tested for predictability and the experimental values and found to match closely, which confirms the model suitability.

Dyed fabrics were tested for their fastness properties such as wash, rub and lightfastness. The results of the fastness tests indicate that modified dyes have good dyeability towards silk fabric. The dyed fabrics were also tested for ultraviolet protection factor and antimicrobial activity, which showed very promising results.

Banned amine testing was done, which confirms the absence of banned amine in synthesised dyes, which indicates the potential of its sustainability. Also, such an approach of modification of natural dyes as semi-synthetic dyes can be surely considered to be a step towards its widespread acceptability and further commercialisation.