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This paper aims to develop efficient and simple models for thermal distribution, melt pool dimensions and controlled phase change in the laser additive manufacturing (AM) of bulk and powder particles ceramic materials.

This paper proposes new analytical models for the AM of bulk and powder bed ceramic materials. A volumetric moving heat source, along with the complete melting of bulk and powder particle materials, is taken into account. Different values of laser absorption coefficient in solid and liquid states have been used to investigate the phase transformation. Furthermore, the pores and voids dimensions are also included in the modeling. Theoretical predictions have been compared with the experimental analyses and finite element simulations in laser to silicon nitride and laser to alumina interaction. The analysis focuses on the impact of laser power and scanning speed on the melt pool width and depth evolution into the bulk substrate and powder bed.

This study shows that the powder particles exhibit a higher thermal distribution value than the bulk substrate because of voids in the powder layer. The laser beam experiences multiple reflections in the presence of porosity/voids, thus increasing the surface absorption coefficient, which becomes relevant with the increment in the pore/void dimension. A direct relationship has been found between the laser power and melt pool dimensions, while the scanning speed displayed an inverse relationship for the melt pool width and length. Larger melt dimensions were inferred in the case of laser–powder particle interaction compared with laser–bulk substrate interaction. A close correlation was found between the analytical simulations, experimental investigations and numerical simulation results within the range of 4%–8%.

This paper fulfills an identified need to develop efficient and simplified models for ceramics laser AM by taking into account different laser absorption coefficients in solid and liquid form, voids and pores dimensions and controlled phase transformation to avoid vapors and plasma formation. The limitation of the finite element simulation model is that the solution is strongly dependent on the mesh quality and accuracy directly linked to the computation efficiency and time. A finer mesh requires a longer computing time than a coarse mesh. Finite element simulations require, however, specialized skills.

The purpose of this paper is to develop an efficient numerical method to study the complex crack initiation and propagation in linear elastic multiphase composites.

A phase field method is developed to study the complex fracture behavior in multiphase composites. A damage threshold is introduced for referring crack initiation in the proposed method. The damage threshold is assigned as a material property so that different composite components possess different thresholds. In this manner, smooth transition from crack initiation to propagation is revealed.

The proposed method is used to investigate complex crack evolution in mesoscale cementitious composite, which consists of aggregates, matrix and void pores. From a mesoscale point of view, it is found that cracks prefer to evolve within the matrix phase. As a crack encounters an aggregate, it tends to bypass the aggregate and evolve along the interface. Cracks tend to avoid to penetrate through aggregates. Also, cracks tend to be attracted by void pores. From a mesoscale point of view, it is revealed that the elastic modulus and strength of concrete models are closely related to porosity.

A criterion with a damage threshold is introduced to the proposed method. The criterions with and without a damage threshold are compared with each other in details. The proposed method is proven to be a useful tool to study mechanical behavior and crack evolution of brittle multiphase composites.

The purpose of this paper is to predict a suitable paper substrate which has high capillary pressure with the tendency of subsequent fluid wrenching in onward direction for the fabrication of microfluidics device application.

The experiment has been done on the Whatman^TM grade 1, Whatman^TM chromatography and nitrocellulose paper samples which are made by GE Healthcare Life Sciences. The structural characterization of paper samples for surface properties has been done by scanning electron microscope and ImageJ software. Identification of functional groups on the surface of samples has been done by Fourier transform infrared analysis. A finite elemental analysis has also been performed by using the “Multiphase Flow in Porous Media” module of the COMSOL Multiphysics tool which combines Darcy’s law and Phase Transport in Porous Media interface.

Experimentally, it has been concluded that the paper substrate for flexible microfluidic device application must have large number of internal (intra- and interfiber) pores with fewer void spaces (external pores) that have high capillary pressure to propel the fluid in onward direction with narrow paper fiber channel.

Surface structure has a dynamic impact in paper substrate utilization in multiple applications such as paper manufacturing, printing process and microfluidics applications.

The purpose of this paper is to investigate the density, surface quality, microstructure and mechanical properties of the components of the selective laser melting (SLM) parts made at different building orientations. SLM is an additive manufacturing technique for three-dimensional parts. The process parameters are known to affect the properties of the eventual part. In this study, process parameters were investigated in the building of 316L structures at a variety of building orientations and for which the fracture toughness was measured.

Hardness and tensile tests were carried out to evaluate the effect of consolidation on the mechanical performance of specimens. Optical and electron microscopy were used to characterise the microstructure of the SLM specimens and their effects on properties relating to fracture and the mechanics. It was found that the density of built samples is 96 per cent, and the hardness is similar in comparison to conventional material.

The highest fracture toughness value was found to be 176 MPa m^(1/2) in the oz. building direction, and the lowest value was 145 MPa m^(1/2) in the z building direction. This was due to pores and some cracks at the edge, which are slightly lower in comparison to a conventional product. The build direction does have an effect on the microstructure of parts, which subsequently has an effect upon their mechanical properties and surface quality. Dendritic grain structures were found in oz. samples due to the high temperature gradient, fast cooling rate and reduced porosity. The tensile properties of such parts were found to be better than those made from conventional material.

The relationship between the process parameters, microstructure, surface quality and toughness has not previously been reported.

This paper aims to present a geometrical void model in conjunction with a multiscale method to evaluate the effect of interraster distance, bead (raster) width and layer height, on the voids concentration (volume) and subsequently calculate the final mechanical properties of the fused deposition modeling parts at constant infill.

A geometric model of the voids inside the representative volume element (RVE) is combined with a two-scale asymptotic homogenization method. The RVEs are subjected to periodic boundary conditions solved by finite element (FE) to calculate the effective mechanical properties of the corresponding RVEs. The results are validated with literature and experiments.

Bead width from 0.2 to 0.3 mm, reported a decrease of 25% and 24% void volume for a constant layer height (0.1 and 0.2 mm – 75% infill). It is reported that the void’s volume increased up to 14%, 32% and 36% for 75%, 50% and 25% infill by varying layer height (0.1–0.2  and 0.3 mm), respectively. For elastic modulus, 14%, 9% and 10% increase is reported when the void’s volume is decreased from 0.3 to 0.1 mm at a constant 75% infill density. The bead width and layer height have an inverse effect on voids volume.

This work brings values: a multiscale-geometric model capable of predicting the voids controllability by varying interraster distance, layer height and bead width. The idealized RVE generation slicer software and Solidworks save time and cost (<10 min, $0). The proposed model can effectively compute the mechanical properties together with the voids analysis.

The purpose of this paper is to elucidate if there is a loss in bond strength between galvanized steel used as reinforcement, and concrete of water‐to‐cement (w/c) ratio of 0.4 and 0.5, after both types of sample were cured for seven, 21 and 28 days in saturated calcium hydroxide solution, and without curing. The air permeability of the concrete was investigated at the interfacial zone.

Structural low‐carbon steel and galvanized steel were embedded in concrete samples, prepared with Portland cement type I and limestone (calcite 94‐97 percent) aggregates. The bond strength between the concrete and the reinforcing bars was measured by means of pull‐out tests.

In concrete of w/c=0.4 the bond for galvanized steel was 5.4±0.5 MPa, while the bond for black steel was 5.8±0.5 MPa, which is 7 percent higher than bond strength measured for samples with galvanized steel rebars. The bond strength for galvanized steel in concrete with a w/c ratio 0.5 was 5.5±0.6 MPa, which was 9 percent higher than the values obtained for black steel, which was 5.0±1 MPa. The total average bond strength of galvanized steel in concrete of w/c ratio 0.4 (5.4±0.5 MPa) and w/c ratio 0.5 (5.5±0.6 MPa) was very similar. They differed by only 2 percent. No decrease in the air permeability at the interfacial zone concrete/galvanized steel was found due to curing.

This research gives quantitative data on the behavior of galvanized steel used as reinforcing bars in concrete, prepared with limestone aggregates. The results might help to increase the reliability of galvanized reinforcing steel used in infrastructure exposed to very aggressive tropical humid marine environments.

The purpose of this paper is to supplement and upgrade existing research on LPBF of NiTi alloys. Laser powder bed fusion (LPBF) is a promising method for fabricating nickel–titanium (Ni–Ti) alloys. It is well known that the energy density is mainly adjusted through the scanning speed and laser power. Nevertheless, there is lack in research on the effects of separately adjusting the scanning speed and laser power on the properties of the final Ni–Ti components. On the other hand, although Ni-rich Ni–Ti alloys [such as Ni54(at.%)Ti] have great potential in structural applications because of their high hardness and good shape stability, at present, there are few studies focusing on this grade of Ni–Ti alloy.

In this work, the energy density was adjusted by changing the laser power and scanning speed separately, and the corresponding process parameters were used to fabricate Ni54(at.%)Ti alloys. The formability (including the relative density, impurity content, etc.) and tensile properties of the LPBF Ni54(at.%)Ti alloys fabricated with different combinations of process parameters were analyzed.

The effects of increasing the laser power and reducing the scanning speed on the properties of the LPBF Ni54(at.%)Ti alloys and the property differences between components manufactured with different combinations of laser power and scanning speed under the same energy density were analyzed. The optimal process parameters were selected to fabricate the components that achieved the highest ultimate tensile strength of 537 MPa, a high relative density of 98.23%, a relatively low impurity content (0.073 Wt.% of carbon and 0.06 Wt.% of oxygen) and an ideal pseudoelasticity (95% recovery rate loaded at 300 MPa).

The effects of increasing the laser power and reducing the scanning speed on the properties of LPBF Ni54(at.%)Ti alloys were studied in this paper. This work is an upgrade and supplement to the existing research on fabricating Ni-rich Ni–Ti alloys by the LPBF method.

The paper aims to examine the inhibition effect of NiO nanoparticles and the influence of liquid nitrogen immersion on the corrosion behavior of (NiO)_x(Bi_1.6 Pb_0.4)Sr₂Ca₂Cu₃O_10-δ and (NiO)_x (Bi, Pb 2223), where x = 0.00 and 0.05 Wt.% phase superconductor in 0.1 M Na₂SO₄ at 30°C.

This study was done using open-circuit potential electrochemical impedance spectroscopy, potentiodynamic polarization curves and chronoamperometry measurements.

Potentiodynamic polarization technique showed that NiO nanoparticles suppress both the anodic and cathodic parts of the polarization curves of (NiO)_x(Bi, Pb)-2223 superconductor in 0.1 M Na₂SO₄ solution. A significant enhancement in the corrosion resistance of the prepared superconductors is observed on immersing them in liquid nitrogen. This is owing to the fact that immersion in liquid nitrogen increases the volume contraction of the superconductor matrix, causing the shrinkage of the pores and voids present in the samples and thus reducing the active surface area for the dissolution of (NiO)_x(Bi, Pb)-2223 superconductor matrix.

This paper fulfills the need to investigate the corrosion behavior of superconductors and the influence of liquid nitrogen immersion on such behavior.

Regardless of the materials used, additive manufacturing (AM) is one of the most popular emerging fabrication processes used for creating complex and intricate structural components. This study aims to investigate the effects of process parameters – namely, nozzle diameter, layer thickness and infill density on microstructure as well as the mechanical properties of 17–4 PH stainless steel specimens fabricated via material extrusion AM.

The experimental approach investigates the effects of printing parameters, including nozzle diameter, layer thickness and infill density, on surface roughness, physical and mechanical properties of the printed specimens. The tests were triplicated to ensure reproducibility of the experimental results.

The highest ultimate tensile strength, 795.26 MPa, was obtained on specimen that was fabricated with a 0.4 mm nozzle diameter, 0.14 mm layer thickness and 30% infill density. Furthermore, a 0.4 mm nozzle diameter also provided slightly better ductility. This came at the expense of surface finishing, as a 0.25 mm nozzle diameter exhibited better surface finishing over a 0.4 mm nozzle diameter. Infill density was shown to slightly influence the tensile properties, whereas layer thickness showed a significant effect on surface roughness. By contrast, hardness and ductility were independent of nozzle diameter, layer thickness and infill density.

This paper presents a comprehensive analysis relating to various input printing parameters on microstructural, physical and mechanical properties of additively manufactured 17–4 PH stainless steel to improve the printability and processability via AM.

Microwave curing (MC) can facilitate rapid concrete repair in cold climates without using conventional accelerated curing technologies which are environmentally unsustainable. Accelerated curing of concrete under MC can contribute to the decarbonisation of the environment and provide economies in construction in several ways such as reducing construction time, energy efficiency, lower cement content, lower carbonation risk and reducing emissions from equipment.

The paper investigates moisture loss and pore properties of six cement-based proprietary concrete repair materials subjected to MC. The impact of MC on these properties is critically important for its successful implementation in practice and current literature lacks this information. Specimens were microwave cured for 40–45 min to surface temperatures between 39.9 and 44.1 °C. The fast-setting repair material was microwave cured for 15 min to 40.7 °C. MC causes a higher water loss which shows the importance of preventing drying during MC and the following 24 h.

Portland cement-based normal density repair mortars, including materials incorporating pfa and polymer latex, benefit from the thermal effect of MC on hydration, resulting in up to 24% reduction in porosity relative to normal curing. Low density and flowing repair materials suffer an increase in porosity up to 16% due to MC. The moisture loss at the end of MC and after 24h is related to the mix water content and porosity, respectively.

The research on the application of MC for rapid repair of concrete is original. The research was funded by the European commission following a very rigorous and competitive review process which ensured its originality. Original data on the parameters of porosity and moisture loss under MC are provided for different generic cementitious repair materials which have not been studied before. Application of MC to concrete construction especially in cold climates will provide environmental, economic and energy benefits.