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The purpose of this paper is to form high density interconnection (HDI) of backboard for press-fit applications with the pre-curing conditions of conductive paste. The best condition of pre-curing conductive paste should be found to obtain good electrical and physical performance of the conductive paste and avoid the simultaneous curing behavior of prepreg.

A novel structure of backboard was designed by using the connection of conductive paste-filled through holes to connect two multilayers. Pre-curing conditions of conductive paste were investigated to find their effects on resistance, bond strength and volume shrinkage. The reliability of pre-curing conductive paste was also analyzed.

Pre-curing conditions led to a great influence on the resistance, bond strength and volume shrinkage of the conductive paste. The best condition of pre-curing conductive paste was chosen as the low curing temperature of 60°C and a curing time of 30 min. Cured conductive paste exhibited square resistance of 4.205 mΩ/□ and bonding strength of 22.86 N. The as-obtained pre-curing condition could improve the reliability of conductive paste. Pre-curing process of conductive paste at extremely low temperature to interconnect two multilayer structures improved the density interconnection of backboard for press-fit applications.

The use of HDI of backboard could lead to good assembly for high-speed signal transmission of electronic products with press-fitting components. The connection of pre-curing conductive paste for multilayers could have important function for improving the application for communication backboard.

The increased interest in the electronics industry to search for alternatives to lead‐containing solders is evidenced by the number of recently published articles on lead‐free solders in this journal and other journals. At the latest Surface Mount International conference, several papers were presented on lead‐free solder alloys, conductive adhesives and organic preservatives, all in search of replacements for lead‐containing finishes. The efforts to find a replacement for tin/lead are in response to possible legislation banning lead or possible taxation on the use of lead. In an attempt to reduce the use of lead in this company's assembly operation, five lead‐free solder pastes and four corresponding flux vehicles (for A, B, C and E pastes) were evaluated. All of the flux vehicles passed the standard industry tests except for two flux vehicles (pastes B and C) that failed the copper mirror test. An assembly trial of the lead‐free pastes was carried out by building liquid crystal display panels with minimal process modification. Printability, process compatibility and solder joint reliability were assessed. This paper describes the preliminary results of the authors' investigation.

The purpose of this paper is to characterize and understand the effects of polymer binder, thixotropic agent, solvent and organic medium content on the rheological properties of silver pastes for screen printing front electrode films of solar cells.

Dispersions of silver particles (surface modified with oleic acid) in ethyl cellulose (EC) polymer solutions with and without thixotropic agent were prepared, and yield stress values were measured by setting shear stress to characterize the inter-particle interaction strength of pastes. Steady-state flow, three interval thixotropy shear test and oscillatory measurements were conducted to study the effect of EC polymer and thixotropic agent on viscosity, structure rebuilding and viscoelastic properties of electrode pastes. The effect of solvent was studied by investigating the steady viscosity of cellulose acetate butyrate (CAB) polymer solutions and Ag dispersions.

Weak flocculation network of silver particles was produced because of depletion flocculation. Besides the interaction between thixotropic agent micelles, EC polymer also has a significant interaction with thixotropic agent. Merely increasing EC polymer or thixotropic agent content is not the best way to prevent the layer printed from laying down. The effect of solvent on the viscosity of paste is mainly attributed to the difference of hydromechanics radius and configuration of CAB polymer in solvents. With the increase of organic medium content, the properties of electrode pastes were converted from rigidity to flexibility.

It is still a challenge to obtain high-quality front electrode films for crystalline silicon solar cells by screen printing, because of the difficulty in reducing shadowing losses while ensuring a low series resistance and high filling factor. The paste rheological properties are the key properties related to the paste’s passing ability through the meshes and resistance of paste spreading on the substrate. Organic medium as an important component of the paste is acknowledged to be used to tailor the paste’s rheological properties and have a great role in screen printing.

This paper examines the rôle that the squeegee plays in the solder paste printing process. Although the printing of solder paste is only one stage of many in the surface mount assembly process, it is crucial to deposit the correct amounts of solder paste cleanly onto the substrate. The amount of solder paste deposited affects the reliability and strength of the reflowed solder joint. Surface mount component lead pitches are continually being reduced due to the requirements of packing more and more components into a given space on the PCB, and this necessitates a proper understanding of the printing process and in particular of the squeegee which plays an important part in determining paste heights and the occurrence of defects. The paper outlines a model which predicts scooping and skipping in the stencil printing of solder pastes used in the reflow soldering of surface mounted devices. The model is based on the forces acting on the squeegee blade, which determines the paste flow pattern ahead of the squeegee, and on the stencil aperture geometry. The paper also examines the interactions between the paste properties and squeegee material properties. These interactions produce printing defects such as scooping, skipping and wet bridging. Results of an experimental comparison of different types of squeegee blade used in the stencil printing of solder pastes for reflow soldering in SMT, as well as the experimental results for squeegee deformation into stencil apertures, were used for validating the model. The empirically enhanced model which results takes into account the force on the squeegee due to solder paste flow and some of the non‐Newtonian properties of the solder paste. The main utility of the proposed model is the control of solder paste printing quality.

This study aims to focus on the surface mount technology (SMT) mass production process of Sn-9Zn-2.5Bi-1.5In solder. It explores it with some components that will provide theoretical support for the industrial SMT application of Sn-Zn solder.

This study evaluates the properties of solder pastes and selects a more appropriate reflow parameter by comparing the microstructure of solder joints with different reflow soldering profile parameters. The aim is to provide an economical and reliable process for SMT production in the industry.

Solder paste wettability and solder ball testing in a nitrogen environment with an oxygen content of 3,000 ppm meet the requirements of industrial production. The printing performance of the solder paste is good and can achieve a printing rate of 100–160 mm/s. When soldering with a traditional stepped reflow soldering profile, air bubbles are generated on the surface of the solder joint, and there are many voids and defects in the solder joint. A linear reflow soldering profile reduces the residence time below the melting point of the solder paste (approximately 110 s). This reduces the time the zinc is oxidized, reducing solder joint defects. The joint strength of tin-zinc joints soldered with the optimized reflow parameters is close to that of Sn-58Bi and SAC305, with high joint strength.

This study attempts to industrialize the application of Sn-Zn solder and solves the problem that Sn-Zn solder paste is prone to be oxidized in the application and obtains the SMT process parameters suitable for Sn-9Zn-2.5Bi-1.5In solder.

This paper aims to investigate the effect of physical vapor deposition (PVD)-coated stencil wall aperture on the life span of fine-pitch stencil printing.

The fine-pitch stencil used in this work is fabricated by electroform process and subsequently nano-coated using the PVD process. Stencil printing process was then performed to print the solder paste onto the printed circuit board (PCB) pad. The solder paste release was observed by solder paste inspection (SPI) and analyzed qualitatively and quantitatively. The printing cycle of up to 80,000 cycles was used to investigate the life span of stencil printing.

The finding shows that the performance of stencil printing in terms of solder printing quality is highly dependent on the surface roughness of the stencil aperture. PVD-coated stencil aperture can prolong the life span of stencil printing with an acceptable performance rate of about 60%.

Stencil printing is one of the important processes in surface mount technology to apply solder paste on the PCB. The stencil’s life span greatly depends on the type of solder paste, stencil printing cycles involved and stencil conditions such as the shape of the aperture, size and thickness of the stencil. This study will provide valuable insight into the relationship between the coated stencil wall aperture via PVD process on the life span of fine-pitch stencil printing.

The study aims to assess the efficiency of nanocomposite to improve the properties of gap-filling materials for pottery artifacts.

Five different pastes were used in the laboratory studies. The pastes consist mainly of pottery powder (grog), dental plaster, microballoons and an adhesive of Primal AC33, nano-silica and nano kaolinite in various concentrations. The prepared samples were subjected to accelerated heat and light aging. Besides, some investigations were used to evaluate the efficacy of the additive nanomaterials, such as TEM, digital and scanning electron microscopy microscopes. Contact angle, color change, shrinkage degree, physical properties and compressive strength tests were also conducted.

The results indicated that using Nano-silica considerably improves the mechanical strength and decreases the shrinkage of gap-filling materials. According to the results, a mixture of grog, microballoons and Primal AC33/Nano-silica Nanocomposites is the optimal gap-filling paste for archaeological pottery. Moreover, this paste showed a higher contact angle (120°), lower color change (ΔE = 2.62), lower shrinkage (3.3%), lower water absorption (3.36%), lower porosity (5.05%) and higher compressive strength (5124 N/mm²).

This paper attains to develop an economic polymer-nanocomposite that can be used with gap-filling materials for pottery artifacts.

The purpose of this paper is to study the rheological behaviours of lead‐free solder pastes used for flip‐chip assembly applications and to correlate rheological behaviours with the printing performance.

A range of rheological characterization techniques including viscosity, yield stress, oscillatory and creep‐recovery tests were carried out to investigate the rheological properties and behaviours of four different solder paste formulations based on no‐clean flux composition, with different alloy composition, metal content and particle size. A series of printing tests were also conducted to correlate printing performance.

The results show that in the viscosity test, all solder pastes exhibited a shear thinning behaviour in nature with different highest maximum viscosity. The yield stress test has been used to study the effect of temperature on the flow behaviour of solder pastes. A decrease in yield stress value with temperature was observed. The results from the oscillatory test were used to study the solid‐ and liquid‐like behaviours of solder pastes. Creep‐recovery testing showed that the solder paste with smaller particle size exhibited less recovery.

More extensive research is needed to simulate the paste‐roll, aperture‐filling and aperture‐emptying stages of the stencil printing process using rheological test methods.

Implementation of these rheological characterization procedures in product development, process optimization and quality control can contribute significantly to reducing defects in the assembly of flip‐chip devices and subsequently increasing the production yield.

The paper shows how the viscosity, yield stress, oscillatory and creep‐recovery test methods can be successfully used to characterize the flow behaviour of solder pastes and also to predict their performance during the stencil printing process.

A try to find some useful applications for some products prepared from agricultural waste by mixing them with cement to act as reinforcement agents. The paper aims to discuss these issues.

Cement was mixed with microcrystalline cellulosic (MCC) fibres prepared from baggase, soaked in mixing water, followed by cubic pastes formation. The mixing was performed using different ratios of MCC; 0.5, 0.75, 1 and 3 per cent. The cement properties were followed at timed intervals, up to 90 days. The initial and final setting times of the pastes were determined. Bulk density, apparent porosity and compressive strength of the harden cement pastes were also identified. The hydration kinetic was followed by identifying free lime ratio and chemically combined water content. The structure of the hard cement pastes was followed by SEM, FTIR, DSC and XRD.

It was noticed that the weight of the prepared cement pastes using MCC was reduced, while the compressive strength was increased. In addition, lower ratios of MCC have shown better results at early ages of hydration and reported higher compressive strength than control. No interaction was reported between the fibres and cement constituents based on the performed analysis.

Different types of agricultural wastes can be compared in producing the best type of MCC for the same purpose of this research.

This piece of work has suggested a simple way to convert a product prepared from agricultural wastes in a small uniform size to a reinforcement agent to cement. Consuming this type of waste reduces the risks resulting from its burning at some countries such as Egypt.

MCC fibres have well-known binding properties and used successfully on wide range in medical applications for tablets production with low costs. These fibres have reduced the pastes weight and increased the compressive strength using low ratios of them. Moreover, there is no indication of a reaction between these fibres and cement constituents.

The purpose of this paper is to study the manufacturing of SAC 305 solder paste with multiwall carbon nanotubes (MWCNT) before and after structure modification and also to investigate the added carbon nanotubes' influence on the technological properties and the microstructure of “nano” solder pastes. This work is a continuation of similar previous studies of SAC solder pastes with silver nanopowder additions.

The authors applied functionalization and esterification methods for the structural modification of the carbon nanotubes. The “nano” solder paste preparation was performed with the use of a two‐stage method of carbon nanotube dispersion in “own‐manufactured” SAC 305 solder paste. To determine the technological properties of the “nano” solder paste, slump, solder ball, wetting and spreading tests were applied according to the existing standards. Standard metallographic procedures were applied for microstructural analysis.

As expected on the basis of the previous studies of SAC solder pastes with silver nanopowders, positive results were obtained for the own‐manufactured SAC 305 solder paste with carbon nanotubes by applying the dispersion method. Also applied were functionalization and esterification methods, whose results showed microstructural changes in the carbon nanotubes. The “nano” SAC solder pastes showed a positive influence on the slump properties, compared to the basic SAC solder paste. The authors proved a negative influence of the carbon nanotubes' addition (dependent on their concentration) on the spreading and wetting of the SAC solder paste on a copper substrate, which provoked the non‐wetting and dewetting phenomena. A slight improvement was observed for the “nano” SAC solder pastes with modified carbon nanotubes. The carbon nanotubes' presence in the solder paste showed a positive effect on the growth reduction of the IMCs' thickness, which depended on the type.

The authors intend to verify the reinforcement effect of the alloys with carbon nanotubes suggested in the literature (the aim of Part II). For this purpose, an assembly process with RC electronic elements on PCBs with Ni/Au and SAC (HASL) finishes will be performed, with the use of the SAC 305 solder paste with modified carbon nanotubes, for the purpose of reflow soldering. Next, measurements of the mechanical strength of the solder joints and their microstructures will be conducted.

It is suggested that further studies of the mechanical properties and the reliability of solder joints are necessary for the practical implementation of the “nano” SAC solder pastes, but taking into account the wetting data, the investigation should be performed only for “nano” pastes with the lowest additions of modified carbon nanotubes.

The paper demonstrates a method of “nano” solder paste preparation by means of a two‐stage dispersion of carbon nanotubes in the own‐manufactured SAC 305 solder paste and a comparison study of the properties of “nano” pastes with the basic SAC solder paste.