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Studies were carried out on the modification of silica with 3‐aminopropyltriethoxysilane in various solvents. The modified silica obtained was subjected to comprehensive evaluations of physicochemical properties, including the bulk density and the capacities to absorb water, dibutyl phthalate and paraffin oil. Particle size, particle size distribution, uniformity of the particles, tendency to form agglomerates, as well as particle surface morphology, were also examined using SEM and dynamic light scattering (DLS) techniques. The properties of the modified silica obtained were compared to evaluate the effects of the solvents used during the surface modification of the silica.

The purpose of this paper is to study the effects of particle size distribution, component ratio, particle packing arrangement, and chemical constitution on the laser sintering behaviour of blended hypoeutectic Al‐Si powders.

A range of bimodal and trimodal powder blends were created through mixing Al‐12Si and pure aluminium powder. The powder blends were then processed using selective laser sintering to investigate the effect of alloy composition, powder particle size and bed density on densification and microstructural evolution.

For all of the powder blends the sintered density increases with the specific laser energy input until a saturation level is reached. Beyond this saturation level no further increase in sintered density is obtained for an increase in specific laser energy input. However, the peak density achieved for a given blend varied significantly with the chemical constitution of the alloy, peaking at approximately 9 wt% Si. The tap density of the raw powder mixture (assumed to be representative of bed density) was also a significant factor.

This is the first study to consider the usefulness of silicon as an alloying element in aluminium alloys to be processed by selective laser sintering. In addition the paper outlines the key factors in optimising processing parameters and powder properties in order to attain sound sinterability for direct laser sintered parts.

This paper aims to report on production of the colour digital printing toners cyan, magenta and yellow. Colour digital electrophotographic printing is currently in high demand. The provision of a large colour gamut depends on appropriate selection of precise colourants to produce toner capable of producing a thin layer on paper.

Printing toners were synthesised by the emulsion aggregation method, and then evaluated for chemical constitution and effects of the colourant substituents.

Results demonstrated that increasing the polarity of a pigment produced better dispersion and lower particle size with narrower distribution and even better colour reproduction. While, changing a pigment’s characteristics did not affect the toner shape or its thermal properties.

The developed method provides a simple way to synthesise colour printing toner.

Emulsion aggregation toners provide less hazardous materials during printing.

Evaluations of the influence of solid-state parameters and physicochemical properties of the pigments on printing toner characteristics were done for the first time.

Soy beverage is becoming more and more popular because it is touted as a healthy food containing useful phytochemicals and is free from lactose and cholesterol. The purpose of this paper is to optimize the spray drying process parameters for obtaining soy beverage powder with good reconstitution and handling properties.

Pre-concentrated soy beverage was dried in a laboratory model spray dryer, and the effects of inlet air temperature (180-220°C), feed rate (20-40 ml/min) and feed solid content (15-25 per cent) on some physical parameters and reconstitution properties (wettability and dispersibility) of spray-dried soy beverage powders were investigated. Second order polynomial response surface model was selected for the analysis of data and optimization of the process.

Spray drying of soy beverage at different processing conditions resulted in powders with particle size (volume mean diameter) in the range of 86 to 156 µm. Dispersibility and wetting time of the spray-dried soy beverage powders was found to be in the range of 56 to 78 per cent and 30 to 90 s respectively, under various drying conditions. Inlet air temperature was found to be the main factor affecting most of the quality parameters, followed by solid content of the feed. Temperature significantly affected the wettability, dispersibility, colour parameters, particle size and flowability of the powder at p ≤ 0.01. Lower temperature and higher feed solid content produced bigger-sized powder particles with better handling properties in terms of flowability and cohesiveness. A moderate inlet air temperature (196°C), higher feed solid content (24 per cent) and lower feed rate (27 ml/min) were found suitable for drying of soy beverage.

The study implied the possibility of producing powder from soy beverage using the spray-drying method and optimized drying conditions for obtaining soy beverage powder with good reconstitution properties.

The finding of this study demonstrated for the first time how the inlet air temperature, feed solid content and feed rate during spray-drying influenced different quality parameters of soy beverage powder. Further, an optimized drying condition has been identified.

Two types of amorphous silica namely, the precipitated silica and the pyrogenic silica, were studied. The surfaces of such silica were modified with silane coupling agents such as 3‐aminopropyltriethoxysilane, N‐2‐(aminoethyl)‐3‐aminopropyltrimethoxysilane and 3‐ureidopropyltrimethoxysilane. Pigments were obtained by the adsorption of organic dyes, C.I. Reactive Blue 19 and C.I. Acid Green 16, onto the modified silica surface. Structural properties of the modified silica and the pigments obtained were evaluated using scanning electron microscopy, zeta potential analysis and particle size measurement techniques. Moreover, colour of the pigments obtained was evaluated using the CIE L *a*b* colour space system. The specific surface area of the pigment obtained was estimated using the BET method.

This study aims to investigate the influence of commercially available resins in water-based magenta pigment inkjet ink formulations on the properties of ink printability and the characteristics of ink application in food packaging. The impact of the resin on the jettability of the existing printability phase diagrams was also assessed.

Inks with different resin loadings were tested for selected properties, such as viscosity, particle size and surface tension. Stability was determined using a Turbiscan AGS turbidimeter and LumiFuge photocentrifuge analyzer. The ink layer fastness against abrasion and foodstuffs was evaluated using an Ugra device and according to PN-EN 646, respectively. JetXpert was used to assess Ricoh printhead jetting performance.

Printability diagrams successfully characterized the jettability of polyurethane inkjet inks on a multi-nozzle printhead and the binder improved droplet formation and printing precision.

Magenta water-based inkjet inks with commercial resins have been developed for printing on paper substrates. To the best of the authors’ knowledge, for the first time, inkjet ink stability was evaluated using the Turbiscan AGS and LumiFuge analyzers, and jettability models were verified using an industrial multi-nozzle printhead.

This paper aims to present a methodology for the detection and categorisation of metal powder particles that are partially attached to additively manufactured lattice structures. It proposes a software algorithm to process micro computed tomography (µCT) image data, thereby providing a systematic and formal basis for the design and certification of powder bed fusion lattice structures, as is required for the certification of medical implants.

This paper details the design and development of a software algorithm for the analysis of µCT image data. The algorithm was designed to allow statistical probability of results based on key independent variables. Three data sets with a single unique parameter were input through the algorithm to allow for characterisation and analysis of like data sets.

This paper demonstrates the application of the proposed algorithm with three data sets, presenting a detailed visual rendering derived from the input image data, with the partially attached particles highlighted. Histograms for various geometric attributes are output, and a continuous trend between the three different data sets is highlighted based on the single unique parameter.

This paper presents a novel methodology for non-destructive algorithmic detection and categorisation of partially attached metal powder particles, of which no formal methods exist. This material is available to download as a part of a provided GitHub repository.

This study aims to demonstrate for the first time that the cheap, commodity polymer, poly(propylene), can be successfully processed using high speed sintering, and that it can be recycled several times through the process, with little to no detriment to either the polymer itself or the parts obtained. This is significant as a step towards the realisation of high speed sintering as a technology for high-volume manufacturing.

A poly(propylene) powder designed for laser sintering was used to build parts on a high speed sintering machine. The unsintered powder was then collected and reused. Repeating this process allowed creation of seven generations of aged powder. A variety of characterisation techniques were then used to measure polymer, powder and part properties for each generation to discern any effects arising from ageing in the machine.

It was found that poly(propylene) could be used successfully in high speed sintering, albeit with a low build success rate. Increased powder age was found to correlate to an increase in the build success rate, changes in microscopic and bulk powder properties and improvement to the dimensional accuracy of the parts obtained. By contrast, no discernible correlations were seen between powder age and polymer molecular weight, or between powder age and the tensile properties of parts.

This is the first report of the use of poly(propylene) in high speed sintering. It is also first study regarding powder recyclability in high speed sintering, both in general and using poly(propylene) specifically.

The purpose of this paper is to present a simple non‐symmetric shape, the poly‐ellipsoid, to describe particles in discrete element simulations that incur a computational cost similar to ellipsoidal particles.

Particle shapes are derived from joining octants of eight ellipsoids, each having different aspect ratios, across their respective principal planes to produce a compound surface that is continuous in both surface coordinate and normal direction. Because each octant of the poly‐ellipsoid is described as an ellipsoid, the mathematical representation of the particle shape can be in the form of either an implicit function or as parametric equations.

The particle surface is defined by six parameters (vs the 24 parameters required to define the eight component ellipsoids) owing to dependencies among parameters that must be imposed to create continuous intersections. Despite the complexity of the particle shapes, the particle mass, centroid and moment of inertia tensor can all be computed in closed form.

The particle can be implemented in any contact algorithm designed for ellipsoids with minor modifications to determine in which pair of octants the potential contact occurs.

The poly‐ellipsoid particle is a computational device to represent non‐spherical particles in DEM models.