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Nanoparticles as the grease additives play an important role in anti-wear and friction-reducing property during the mechanical operation. To improve the lubrication action of grease, the tribological behavior of lithium-based greases with single (nanometer Al₂O₃ or nanometer ZnO) and composite additives (Al₂O₃–ZnO nanoparticles) were investigated in this paper.

The morphology and microstructure of nanoparticles were characterized by means of transmission electron microscope and X-ray diffraction. Tribological properties of different nanoparticles as additives in lithium-based greases were evaluated using a universal friction and wear testing machine. In addition, the friction coefficient (COF) and wear scar diameter were analyzed. The surface morphology and element overlay of the worn steel surface were analyzed by scanning electron microscopy (SEM) and energy dispersive spectrometer (EDS), respectively.

The results show that the greases with nanometer Al₂O₃ or nanometer ZnO and the composite nanoparticles additives both exhibit lower COFs and wear scar diameters than those of base grease. And the grease with Al₂O₃–ZnO composite nanoparticles possesses much lower COF and shows much better wear resistance than greases with single additives. When the additives contents are 0.4 Wt.% Al₂O₃ and 0.6 Wt.% ZnO, the composite nanoparticles-based grease exhibits the lowest mean COF (0.04) and wear scar diameter (0.65 mm), which is about 160% and 28% lower than those of base grease, respectively.

The main innovative thought of this work lies in dealing with the grease using single or composite nanoparticles. And through a serial contrast experiments, the anti-wear and friction-reducing property with different nanoparticles additives in lithium grease are evaluated.

The purpose of this paper is to prepare structural colors of fabrics coated with Silver/Zinc Oxide (Ag/ZnO) composite films by magnetron sputtering and analyze the relationship between the colors and the thickness of Zinc Oxide (ZnO) film in Ag/ZnO composite film and the photocatalytic property of the fabrics coated with Ag/ZnO composite film.

Ag/ZnO composite films deposited on polyester fabrics were prepared by magnetron sputtering technology. The structural colors of textiles coated with Ag/ZnO composite films and the relationship between the colors and Ag/ZnO composite films were analyzed, and the photocatalytic property of Ag/ZnO composite films was also discussed.

The results indicated that the colors varied with the thicknesses of the ZnO film in Ag/ZnO composite films. The reactive sputtering time of ZnO film was 5, 8, 10 and 14 min, respectively, and the colors of the corresponding fabrics were purple, blue, blue-green and yellow. Meanwhile, the polyester fabrics coated with Ag/ZnO composite films showed the excellent photocatalytic properties, and silver (Ag) films deposited under the ZnO films in Ag/ZnO composite films could also improve the photocatalytic activities of ZnO films, and the formaldehyde degradation rates was 77.5%, which was higher than the 69.9% for the fabrics coated only with the ZnO film.

The polyester fabrics coated with Ag/ZnO composite films not only created various structural colors using change the thicknesses of the ZnO film, but also achieved the multifuctionality, which will have a broad application prospect in textile fields.

The purpose of this paper is to investigate the effect of hexagonal boron nitride (h-BN) and poly (phenyl p-hydroxybenzoate) (PHBA) on improving the torsional tribological behavior of polytetrafluoroethylene (PTFE).

This paper investigates the torsional tribological behavior of PTFE composites filled with h-BN and PHBA under different angular displacements with a plane-on-plane torsional friction tester. The worn surface of PTFE composites was investigated by using a scanning electron microscope.

The shape of T–Θ curves of PTFE composites was influenced by both content fillers and torsional angule. The material with a higher coefficient of sliding friction exhibited the larger torsional angle under which the torsional regime transited from a partial slip to a gross slip. PTFE composites filled with 20 weight per cent PHBA and 10 weight per cent h-BN showed the best anti-wear properties. The specific wear rate of composites exhibits a negative correlation with material hardness. The wear volume loss presents a positive correlation with friction dissipation energy. The specific wear rate of all composites decreased with increasing torsional angle. The dominant wear mechanism of pure PTFE was adhesive wear. The slight plastic flow and plowing occurred on the worn surfaces of PTFE composites because of the higher hardness of composites and the lubrication of h-BN particles with layer crystal structure.

This paper put forward a kind of PTFE composite with low torsional wear rate, which can be used in the sliding slewing bearing or the center plate of a bogie.

The purpose of this paper is to explore the geometric parameter difference of the terrace-like structural transfer film under different working parameters [pressure and velocity (PV) values] and filled particle types (three fillers: SiO₂, TiO₂ and ZnO), and find the geometric parameter related to the wear of polytetrafluoroethylene (PTFE)-based composites.

PTFE composites were filled with SiO₂, TiO₂ and ZnO particles, and the morphology parameter of the PTFE composite transfer film under different PV values obtained from the rotary reciprocating pin-on-disk frictional tester was quantified by using a three-dimensional laser scanning microscope.

The results showed that the effective layer coverage rate and effective thickness of the transfer film had a good relationship with the wear of the three PTFE composites. On the whole, increasing the speed or load was helpful to increase the effective thickness of the three PTFE composite transfer films, but reduced the effective layer coverage rate. The greater the effective layer coverage rate and effective thickness of the transfer film, the better the wear resistance of the PTFE composites in the entire speed and load range.

This work will promote further understanding of the transfer film and lay a foundation for realizing its morphology regulation and improving the wear of the PTFE composites.

The purpose of this paper is to achieve attractive fabric composites with excellent tribological performance and investigate the wear mechanisms of these fabric composites sliding against bearing steel pins under dry sliding process.

Five different weave density composites were prepared, and the tribological behaviors of these composites were studied at different testing conditions. Scanning electron microscopy, laser microscopy (three-dimensional profile measurements) and energy-dispersive X-ray spectrometry were used to analyze the worn surface morphology, wear volume and elemental content of the transfer films, respectively.

The composite weave density serves an important influence on tribological behavior. Generally, the wear rate of each composite increased with increasing weave density, and the friction coefficient of each composite decreased with increasing weave density.

Nanoparticle-filled hybrid polytetrafluoroethylene/Kevlar fabric composites with proper weave density have exhibited superior tribological properties in dry sliding conditions. The results that obtained in this paper may offer a reference for others who intend to achieve attractive fabric composites with excellent tribological performance.

The purpose of this paper is to propose a simple physical evaporation route in which catalyst‐free zinc oxide (ZnO) nanoscrewdrivers were deposited on silicon (Si) (111) substrates.

Prior to the deposition, the Si (111) wafer was cut into pieces of 2×2 cm². Then, the wafers were dipped for 1 min into mixture buffered oxide etchant to remove native oxide. Then, the samples were rinsed in an ultrasonic bath cleaned with boiling acetone, ethanol, and de‐ionized (DI) water for 10 min. Lastly, the wafers were rinsed in 25 ml DI water in stirred and then were blown dry with nitrogen. In this technique, the starting material is high‐purity metallic zinc (Zn) powder (99.99 per cent pure). Following, the Zn films were then annealed under air environment in the furnace at 500°C for 1 h deprived of any catalysts.

These ZnO samples were studied by scanning electron microscopy, high‐resolution X‐ray diffraction (HR‐XRD), and photoluminescence (PL) spectroscopy. Atomic force microscope (AFM) images were applied to ascertain surface morphology of produced ZnO nanoscrewdrivers. XRD pattern confirmed that the ZnO nanoscrewdrivers were of polycrystalline structure in universe with a hexagonal close packed type and c‐axis is perpendicular to the substrate. The peak at 34° correspond to the reflection planes of ZnO(002) crystallographic plane is perceived. The AFM surface images disclosed that the surfaces of produced ZnO thin films are not smooth. The PL spectrum of as‐synthesized nanoscrewdrivers shows a UV emission peak at 380 nm and a broad green emission peak at 500 nm.

The paper reports on a simple physical evaporation route, ZnO nanoscrewdrivers were synthesized via the thermal evaporation of the high‐purity Zn powders and annealed at 500°C under air atmosphere without introducing any hetero‐metal catalysts or other carrier gases approach.

The purpose of this paper is to construct an array of sensors using polypyrrole–zinc oxide (PPy–ZnO) and PPy–vanadium (V; chemical formula: V₂O₅) fibers. To test responses of sensors, a central composite design (CCD) has been used. The results of the CCD technique revealed that the developed sensors are orthogonally sensitive to diacetyl, lactic acid and acetic acid. In total, 20 different mixtures of diacetyl, lactic acid and acetic acid were prepared, and the responses of the array sensors were recorded for each mixture.

A response surface regression analysis has been used for correlating the responses of the sensors to diacetyl, lactic acid and acetic acid concentrations during the gas phase in food samples. The developed multivariate model was used for simultaneous determination of diacetyl, lactic acid and acetic acid concentrations. Some food samples with unknown concentrations of diacetyl, lactic acid and acetic acid were provided, and the responses of array sensors to each were recorded.

The responses of each sensor were considered as target response in a response optimizer, and by an overall composite desirability, the concentration of each analyte was predicted. The present work suggests the applicability of the response surface regression analysis as a modeling technique for correlating the responses of sensor arrays to concentration profiles of diacetyl, lactic acid and acetic acid in food samples.

The PPy–ZnO and PPy–V₂O₅ nanocomposite fibers were synthesized by chemical polymerization. The provided conducting fibers, PPy–ZnO and PPy–V₂O₅, were used in an array gas sensor system for the analysis of volatile compounds (diacetyl, lactic acid and acetic acid) added to yogurt and milk samples.

This paper aims to report a novel preparation method of ZnO particles with different structures and their photocatalytic activity.

ZnO powders are prepared by a facile, economical and environment-friendly aqueous solution route. X-ray diffraction, field emission scanning electron microscopy, energy dispersive spectroscopy, transmission electron microscopy and UV-vis diffuse reflectance spectra are used to characterize the products. Photocatalytic activity of the samples is evaluated by degradation of organic pollutant pentachlorophenol under UV-vis irradiation.

It is found that three-dimensional ZnO hierarchical structures can be prepared via aqueous solution route without using any template or structure-directing agent, and the alkalinity of reaction solution is the key factor. All the as-prepared ZnO products have good catalytic activity under UV-vis light irradiation.

This report presents a simple method for the preparation of ZnO particles with excellent photocatalytic activity. Experimental results could provide useful reference for the treatment of chlorophenols in the future.

The purpose of this paper is to improve the properties of metal nanoparticles which are easy to agglomerate and hard to disperse evenly, thus limiting the application of metal nanoparticles in grease. A novel technology was proposed for modifying metal oxide to improve the dispersibility of nanoparticles.

SA-TiO2 nanoparticles were synthesized using an in-situ esterification method followed by surface modification with stearic acid. The microstructure of the nanoparticles was characterized by scanning electron microscope, transmission electron microscope and Fourier transform infrared spectroscopy and their thermal stability was evaluated by thermogravimetric analyzer. The tribological properties of the SA-TiO2 nanoparticles as additives in lithium grease were evaluated with a four-ball tester and TE77 reciprocating friction tester. The worn surfaces of the steel balls were investigated by EDS and XPS.

The prepared nanoparticles can be well dispersed in the lithium grease and possess much better tribological properties compared to traditional nanoparticles. The results indicated that the excellent tribological performance of SA-TiO2 was attributed to the chemical reaction film composing of Fe2O3, iron oxide and other organic compounds.

This paper provides a method to prevent the agglomeration of nano-TiO2 by surface modification with stearic acid. And the prepared nanoparticles can effectively improve the tribology performance of lithium grease.

Renewable energy alternatives and nanoscale materials have gained huge attention in recent years due to the problems associated with fossil fuels. The recyclable battery is one of the recent developments to address the energy requirement issues. In this work, the development of nanoscale materials is focused on using green synthesis methods to address the energy requirements of hybrid electric vehicles.

The current research focuses on developing metal oxide nanoscale materials (NANO-SMs). The Zno-Aloe vera NANO-SM is prepared using the green synthesis method. The developed nanoscale materials are characterized using analysis methods like FESEM, TEM, XRD and FTIR.

The average size of ZnO-Aloe vera mono-crystalline was recorded as 60–70 nm/Hexagonal shape. The nanoscale materials are used for the detection of LPG gases. The sensitivity observed was 48%. The response time and recovery time were recorded as 8–10 s and 230–250 s, respectively. The average size of SnO₂-green papaya leaves poly-crystalline was recorded as 10–20 nm/powder form.

Nanoscale materials are developed using green synthesis methods for hybrid vehicle applications. The nanoscale materials are used for the detection of harmful gases in hybrid vehicles.