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Article
Publication date: 12 August 2020

The effect of cryogenic treatment on dry sliding wear mechanisms in hard coatings

Bilal Kurşuncu

The effect of cryogenic heat treatment on the mechanical properties of different materials has been frequently investigated by researchers in recent years. The purpose of…

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Abstract

Purpose

The effect of cryogenic heat treatment on the mechanical properties of different materials has been frequently investigated by researchers in recent years. The purpose of this paper is to investigate wear behaviour of monolayer, multilayer and nanocomposite coatings after cryogenic heat treatment. It is a first in its field in terms of both the heat treatment used and the coatings examined.

Design/methodology/approach

The aCN/TiAlN, TiAlN and ncTiAlSiN hard coatings deposited on the AISI D2 steel substrate were subjected to cryogenic heat treatment at −145oC and −196oC for 24 h and then tempered at 200oC for 2 h. Then, the samples were subjected to wear tests of 5, 10 and 15 N three different load values. The wear mechanisms occurring on the wear surfaces were determined by scanning electron microscope supported by EDS.

Findings

Oxidation, fatigue and delamination wear mechanisms were realized on the surfaces of the samples subjected to dry sliding wear test. The wear resistance of S1 increased with cryogenic heat treatment. According to the wear test results of the untreated samples, it was found that the samples with lower hardness than the others had higher wear resistance. The wear resistance of S1 and S2 samples was increased by cryogenic heat treatment. The best wear resistance in all parameters was obtained by S1. Oxidation in the S1 was found to have a positive effect on wear resistance. According to EDS results after wear of S2, chromium-rich layer was found on the surface of the material. It is understood that cryogenic heat treatment causes carbide precipitation in the inner structure of the substrate material.

Originality/value

The effect of cryogenic heat treatment on the mechanical properties of different materials has been frequently investigated by researchers in recent years. In this study, wear behaviour of monolayer, multilayer and nanocomposite coatings after cryogenic heat treatment was investigated. It is a first in its field in terms of both the heat treatment used and the coatings examined.

Peer review

The peer review history for this article is available at: https://publons.com/publon/10.1108/ILT-03-2020-0111/

Details

Industrial Lubrication and Tribology, vol. ahead-of-print no. ahead-of-print
Type: Research Article
DOI: https://doi.org/10.1108/ILT-03-2020-0111
ISSN: 0036-8792

Keywords

  • Dry sliding wear
  • DLC coating
  • Nanocomposite hard coating
  • Cryogenic treatment
  • Wear mechanism
  • Nano-layer coating

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Article
Publication date: 1 August 2010

Aerospace and aircraft structures research at the National Research Council of Canada (NRC)

Jerzy Komorowski

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Abstract

Details

International Journal of Structural Integrity, vol. 1 no. 3
Type: Research Article
DOI: https://doi.org/10.1108/ijsi.2010.43601caa.002
ISSN: 1757-9864

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Article
Publication date: 7 May 2019

Effects of mass ratios on salt spray corrosion and electrochemical corrosion behaviors of laser cladded Cr–Ni coatings

Li Jiahong and Kong Dejun

The purpose of this paper is to improve the salt spray corrosion and electrochemical corrosion performances of H13 hot work mould steel, Cr–Ni coatings with the different…

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Abstract

Purpose

The purpose of this paper is to improve the salt spray corrosion and electrochemical corrosion performances of H13 hot work mould steel, Cr–Ni coatings with the different Cr and Ni mass ratios are fabricated using a laser cladding (LC), which provides an experimental basis for the surface modification treatment of H13 steel.

Design/methodology/approach

Cr–Ni coatings with the different Cr and Ni mass ratios were firstly fabricated on H13 hot work mould steel using a laser cladding (LC). The salt spray corrosion (SSC) and electrochemical corrosion performances of Cr–Ni coatings in 3.5 Wt.% NaCl solution were investigated to analyze the corrosion mechanism, and the effect of mass ratios of Cr and Ni on their corrosion mechanism was discussed.

Findings

The laser cladded Cr–Ni coatings with the different Cr and Ni mass ratios are composed of Cr–Ni compounds, which are metallurgically combined with the substrate. The SSC resistance of Cr–Ni coating with the Cr and Ni mass ratios of 24:76 is the highest. The electrochemical corrosion resistance of Cr–Ni coating with the Cr and Ni mass ratio of 24:76 is the best among the three kinds of coatings.

Originality/value

In this study, the corrosion resistance of laser cladded Cr–Ni coatings with the Cr and Ni mass ratios of 17: 83, 20: 80 and 24: 76 was first evaluated using salt spray corrosion (SSC) and electrochemical tests, and the effect of mass ratios of Cr and Ni on their corrosion mechanism was discussed.

Details

Anti-Corrosion Methods and Materials, vol. 66 no. 3
Type: Research Article
DOI: https://doi.org/10.1108/ACMM-10-2018-2015
ISSN: 0003-5599

Keywords

  • Corrosion mechanism
  • Electrochemical corrosion
  • Cr–Ni coating
  • Laser cladding (LC)
  • Mass ratio
  • Salt spray corrosion (SSC)

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Article
Publication date: 4 September 2017

Effects of nano-layered silicates on mechanical and chemical properties of acrylic-melamine automotive clear coat

Zaker Bahreini, Vahid Heydari and Zahra Namdari

Mechanical and chemical properties of acrylic-melamine automotive clear coat in the presence of different percentages of well dispersed nano-layered sodium montmorillonite…

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Abstract

Purpose

Mechanical and chemical properties of acrylic-melamine automotive clear coat in the presence of different percentages of well dispersed nano-layered sodium montmorillonite (Na-MMT) silicate particles were investigated. For this purpose, prepared dry clear coat film samples were subjected to the entire standard test series, usually carried out in automotive coating industry.

Design/methodology/approach

Effects of adding different percentages of nano-layered silicate on mechanical and chemical properties of acrylic-melamine automotive clear coat were investigated. To increase the compatibility of nanoclays with polymer matrix of clear coat, the surface of nanoclays was modified by benzalkonium chloride as a cationic surfactant. Scanning electron microscopy (SEM) and X-ray diffraction (XRD) were used for characterization and comparison between clays before and after modification, and also after dispersion in coating. Prepared dry clear coat film samples subjected to the test series are usually carried out in automotive coating industry.

Findings

The results indicated that incorporation of 1 and 2 Wt.% of nano-layered silicate caused desired improvement in chemical and physical properties of the acrylic-melamine clear coat. Increasing the percentage of nanoclay to over 2 Wt.% caused damage in some properties such as hardness, cupping and gloss.

Research limitations/implications

All materials and methods were used in this research are industrial grade. Therefore, the introduced modified clear coat sample has potential for commercial production as an automotive clear coat.

Originality/value

As far as it was searched in the literature, effects of adding nanoclay particles on mechanical and physical properties of different clear coats, such as epoxy clear coat, have been investigated in a few researches, but in this research, common and special tests which are necessary in automotive coating industry have been ignored. In the present study for the first time, acrylic-melamine clear coat was subjected to modification using nano-clay, and also, the most common industrial test methods were used for investigation of mechanical and chemical properties.

Details

Pigment & Resin Technology, vol. 46 no. 5
Type: Research Article
DOI: https://doi.org/10.1108/PRT-07-2016-0077
ISSN: 0369-9420

Keywords

  • Nanotechnology
  • Mechanical properties
  • Automotive components industry
  • Impact strength
  • Coatings technology
  • Electrodeposition

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Article
Publication date: 8 July 2019

Characterization of the friction and wear effects of graphene nanoparticles in oil on the ring/cylinder liner of internal combustion engine

Selman Demirtas, Hakan Kaleli, Mahdi Khadem and Dae-Eun Kim

This study aims to investigate the tribological characteristics of a Napier-type second piston ring against a cylinder liner in the presence of graphene nano-additives…

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Abstract

Purpose

This study aims to investigate the tribological characteristics of a Napier-type second piston ring against a cylinder liner in the presence of graphene nano-additives mixed into 5W40 fully synthetic engine oil.

Design/methodology/approach

Wear tests were carried out in the boundary lubrication condition using a reciprocating tribometer, and real engine tests were performed using a single spark ignition Honda GX 270 test engine for a duration of 75 h.

Findings

The experimental results of the tribometer tests revealed that the nano-additives formed a layer on the rubbed surfaces of both the piston ring and the cylinder liner. However, this layer was only formed at the top dead center of the cylinder liner during the engine tests. The accumulation of carbon (C) from the graphene was heavily detected on the rubbed surface of piston ring/cylinder liner, mixed with other additive elements such as Ca, Zn, S and P. Overall, the use of graphene nano-additives in engine oil was found to improve the frictional behavior in the boundary and mixed lubrication regimes. Abrasive wear was found to be the main mechanism occurring on the surface of both piston rings and cylinder liners.

Originality/value

Though many researchers have discussed the potential benefits of graphene as a nano-additive in oil to reduce the friction and wear in laboratory tests using tribometers, to date, no actual engine tests have been performed. In this paper, both tribometer and real engine tests were performed on a piston ring and cylinder liner using a fully formulated oil with and without graphene nano-additives in the boundary lubrication condition. It was found that a graphene nano-additive plays an active role in lowering the coefficient of friction and increasing surface protection and lubrication by forming a protective layer on the rubbing surfaces.

Details

Industrial Lubrication and Tribology, vol. 71 no. 5
Type: Research Article
DOI: https://doi.org/10.1108/ILT-05-2018-0170
ISSN: 0036-8792

Keywords

  • Lubrication
  • Piston ring
  • Friction wear
  • Engine test
  • Graphene nanoparticles

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Article
Publication date: 19 September 2016

A DNA hybridization detection sensor based on photo biased ZnO thin film FET devices

Mehdi Habibi and Maryam Fanaei

The purpose of this paper is to present a DNA hybridization detection sensor. An inexpensive fabrication procedure was used so that the sensors can be disposed…

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Abstract

Purpose

The purpose of this paper is to present a DNA hybridization detection sensor. An inexpensive fabrication procedure was used so that the sensors can be disposed economically after the measurement is completed.

Design/methodology/approach

Field effect transistor (FET) devices are used in the proposed structure. The FET device acts as a charge detection element and produces an amplified output current based on surface charge variations. As amplification is performed directly at the sensor frontend, noise sources have less effect on the detected signal, and thus, acceptably low DNA concentrations can be detected with simple external electronics. ZnO nano layers are used as the FET active semiconductor channel. Furthermore, a photobiasing approach is used to adjust the operating point of the proposed FET without the need for an additional gate terminal.

Findings

The proposed sensor is evaluated by applying matched and unmatched target DNA fragments on the fabricated sensors with capture probes assembled either directly on the ZnO surface or on a nano-platinum linker layer. It is observed that the presented approach can successfully detect DNA hybridization at the nano mole range with no need for complex laboratory measurement devices.

Originality/value

The presented photobiasing approach is effective in the adjustment of the sensor sensitivity and decreases the fabrication complexity of the achieved sensor compared with previous works.

Details

Sensor Review, vol. 36 no. 4
Type: Research Article
DOI: https://doi.org/10.1108/SR-04-2016-0074
ISSN: 0260-2288

Keywords

  • DNA sensor
  • Field effect transistor
  • Hybridization detection
  • Photo biased FET
  • ZnO nano layers

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Article
Publication date: 22 March 2011

Stress corrosion leads to detachment of diamond-like carbon (DLC) nano layer: Ionbond, EMPA and Synthes find a solution

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Abstract

Details

Anti-Corrosion Methods and Materials, vol. 58 no. 2
Type: Research Article
DOI: https://doi.org/10.1108/acmm.2011.12858bab.010
ISSN: 0003-5599

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Article
Publication date: 2 November 2012

Functional coatings from the plasma nozzle

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Abstract

Details

Anti-Corrosion Methods and Materials, vol. 59 no. 6
Type: Research Article
DOI: https://doi.org/10.1108/acmm.2012.12859faa.012
ISSN: 0003-5599

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Article
Publication date: 1 December 2005

Superior, whisker‐reduced immersion tin technology

Sabine Schroeder

To provide information about latest product developments to address and take away the fear of whisker formation on pure immersion tin surface finishes on PCBs.

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Abstract

Purpose

To provide information about latest product developments to address and take away the fear of whisker formation on pure immersion tin surface finishes on PCBs.

Design/methodology/approach

This paper summarises the latest findings on whisker formation of pure tin surface finishes and describes an effective methodology for whisker suppression in combination with other benefits for the use of this new immersion tin generation.

Findings

Whisker formation is a typical feature of pure tin when coated, e.g. on copper and is a threat to the PCB industry, because of the risks of shortcuts involved. The main driving force for whiskers is an accumulation of internal stress created by diffusion at the boundary of copper and tin. A nano layer deposited from an organic metal‐based pre‐dip significantly reduces the diffusion by creating a unique sandwich layer with smooth concentration gradients. A drastic reduction of diffusion and stress was found, eliminating the driving force for whisker formation and prolonging the layer's shelf life and temperature stability at the same time.

Practical implications

Whenever whisker formation on immersion tin is regarded as a potential risk, e.g. by OEMs, a whisker‐reduced process is available and should be chosen to meet the market's specifications.

Originality/value

This paper takes the edge off the whisker threat discussions, leading to a hesitant implementation of immersion tin surface finish technology for PCBs, which disregard its excellent features with respect to future lead‐free soldering. Whisker‐reduced immersion tin is a viable and preferable alternative solderable surface finish for the lead‐free era.

Details

Circuit World, vol. 31 no. 4
Type: Research Article
DOI: https://doi.org/10.1108/03056120510603134
ISSN: 0305-6120

Keywords

  • Printed‐circuit boards
  • Metals
  • Surface treatment

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Article
Publication date: 5 September 2016

Particle shape effects on Marangoni convection boundary layer flow of a nanofluid

R. Ellahi, A. Zeeshan and Mohsan Hassan

The purpose of this paper is to study the particle shape effects on Marangoni convection boundary layer flow of a nanofluid. The paper aims to discuss diverse issues…

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Abstract

Purpose

The purpose of this paper is to study the particle shape effects on Marangoni convection boundary layer flow of a nanofluid. The paper aims to discuss diverse issues befell for the said model.

Design/methodology/approach

The work undertaken is a blend of numerical and analytical studies. Analytical and numerical solutions of nonlinear coupled equations are developed by means of Mathematica package BVPh 2.0 based on the homotopy analysis method.

Findings

The velocity of nanofluid decreases by increasing particle volume friction and similarity parameters. With the increase in particle volume friction and similarity parameter, temperature profile is correspondingly enhanced and decline. The lowest velocity and highest temperature of nanofluid is cause by needle- and disc-shaped particle. Consequence for interface velocity and the surface temperature gradient are perceived by numeric set of results. It is found that the interface velocity is declined by increasing particle volume friction and volume concentration of ethylene glycol in the water. The minimum interface velocity is seen by needle-shaped particle and 30 percent concentrations of ethylene glycol. With increase in volume friction and size of particle, the behaviors of surface temperature gradient are found decreasing and increasing function, respectively. The maximum heat transfer rate at the surface is achieved when we chose sphere nanoparticles and 90 percent concentrations of ethylene glycol as compared to other shapes and concentrations.

Originality/value

This model is investigated for the first time, as the authors know.

Details

International Journal of Numerical Methods for Heat & Fluid Flow, vol. 26 no. 7
Type: Research Article
DOI: https://doi.org/10.1108/HFF-11-2014-0348
ISSN: 0961-5539

Keywords

  • Nanofluid
  • Analytical and numerical solutions
  • Interfacial layer
  • Marangoni convection
  • Shape effects

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