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The prime task of research in hot forging industry is to improve the service life of forging dies. The in-service microstructural changes that may occur in a die during hot forging is expected to significantly affect the service life. The purpose of this work is to analyse the microstructural evolution of double tempered hot forging dies in a real industrial environment, and the correlation of microstructural and microhardness evolution to the in-service wear and plastic deformation.

Specific hot forging tests were carried out on double tempered AISI H11 chromium tool steel for 100, 500 and 1,000 forging strokes. Macro analysis was conducted on die cross section to analyse the wear and plastic deformation at different stages of forging cycles. Microhardness and microstructural analyses were performed on the die surface after these forging tests.

The macro analysis on the transverse section of dies shows that wear is predominant during initial forging strokes, whereas plastic deformation is observed in later stages. Microstructural analyses demonstrate that during first 500 forging cycles, carbide population decreases at 63 per cent higher rate as compared to corresponding drop during 501 to 1,000 forging cycles. Additionally, the carbide size increases at all stages of forging cycle. Further, microstructural images from dies after 1,000 forging strokes show clustering and spherodisation of carbides by which the “blocky”-shaped carbides in pre-forging samples had spherodised to form “elongated spherical” structures.

The findings of this work can be used in hot forging industries to predict amount of wear and plastic deformation at different stages of service. From the results of this work, the service life of double tempered H11 hot forging dies used in forging without lubrication is within 501 to 1,000 forgings.

Most of the literatures are focussed on the cyclic softening of material at constant temperature. This work analyses the microstructural evolution of double tempered hot forging dies in a real industrial environment and correlates the microstructural and microhardness evolution to the in-service wear and plastic deformation.

To find properties of screen printed PZT (PbZr_0.53Ti_0.47O₃ with 6 per cent of PbO and 2 per cent of Pb₅Ge₃O₁₁) thick films layers on LTCC substrate.

The influence of PZT firing time and electrode materials on electrical characteristics and microstructure were examined. A scanning electron microscope (SEM) equipped with an energy‐dispersive X‐ray (EDS) analyser was used for the microstructural and compositional analysis.

Microstructural and compositional analyses have shown the diffusion of SiO₂ from LTCC into PZT layers and the diffusion of PbO in the opposite direction. SiO₂ presumably forms low permitivity lead based silicates in PZT layer. The new phase deteriorates the piezoelectric properties. The amount of diffused materials was dependent upon the electrode material and increased with increasing firing time. Better properties, i.e. higher remanent polarisation and dielectric constant were achieved for samples with PdAg electrodes and shorter firing time.

New information on electrical and microstructural properties of thick film PZT made on LTCC substrate.

This study aims to demonstrate a modified wire arc additive manufacturing (AM) named non-transferring arc and wire AM (NTA-WAM). Here, the build plate has no electrical arc attachment, and the system’s arc is ignited between tungsten electrode and filler wire.

The effect of various deposition conditions (welding voltage, travel speed and wire feed speed [WFS]) on bead characteristics is studied through response surface methodology (RSM). Under optimum deposition condition, a single-bead and thin-layered part is fabricated and subjected to microstructural, tensile testing and X-ray diffraction study. Moreover, bulk texture analysis has been carried out to illustrate the effect of thermal cycles and tensile-induced deformations on fibre texture evolutions.

RSM illustrates WFS as a crucial deposition parameter that suitably monitors bead width, height, penetration depth, dilution, contact angle and microhardness. The ferritic (acicular and polygonal) and lath bainitic microstructure is transformed into ferrite and pearlitic micrographs with increasing deposition layers. It is attributed to a reduced cooling rate with increased depositions. Mechanical testing exhibits high tensile strength and ductility, which is primarily due to compressive residual stress and lattice strain development. In deposits, ϒ-fibre evolution is more resilient due to the continuous recrystallisation process after each successive deposition. Tensile-induced deformation mostly favours ζ and ε-fibre development due to high strain accumulations.

This modified electrode arrangement in NTA-WAM suitably reduces spatter and bead height deviation. Low penetration depth and dilution denote a reduction in heat input that enhances the cooling rate.

The purpose of this paper is to develop an automated phase segmentation model from complex microstructure. The mechanical and physical properties of metals and alloys are influenced by their microstructure, and therefore the investigation of microstructure is essential. Coexistence of random or sometimes patterned distribution of different microstructural features such as phase, grains and defects makes microstructure highly complex, and accordingly identification or recognition of individual phase, grains and defects within a microstructure is difficult.

In this perspective, computer vision and image processing techniques are effective to help in understanding and proper interpretation of microscopic image. Microstructure-based image processing mainly focuses on image segmentation, boundary detection and grain size approximation. In this paper, a new approach is presented for automated phase segmentation from 2D microstructure images. The benefit of the proposed work is to identify dominated phase from complex microstructure images. The proposed model is trained and tested with 373 different ultra-high carbon steel (UHCS) microscopic images.

In this paper, Sobel and Watershed transformation algorithms are used for identification of dominating phases, and deep learning model has been used for identification of phase class from microstructural images.

For the first time, the authors have implemented edge detection followed by watershed segmentation and deep learning (convolutional neural network) to identify phases of UHCS microstructure.

Military and unmanned aerial vehicles (UAV) applications like rocket motor casings, missile covers and ship hulls use components that are made of maraging steel. Maraging steel has properties that are superior to other metals, making it more suitable for the fabrication of such components. A grey relational analysis (GRA) that is based on the Taguchi method has been utilised in the current study to optimise a laser beam welding (LBW) process. Further aspects such as GRA's optimum ranges and percentage contributions were also estimated.

A Taguchi L16 orthogonal array is utilised to design and conduct the experiments. Laser power (LP), welding speed (WS) and focal position (FP) are the three parameters are chosen for the process of welding. The output responses are the upper width of the heat-affected zone (HAZup), the upper width of the fusion zone (FZup) and the depth of penetration (DOP). The effect of the above key parameters on the responses was examined using an analysis of variance (ANOVA).

The results of ANOVA reveal that the parameter that has the most influence on the overall grey relational grade (GRG) is the FP. Finally, metallographic characterisation and a microstructural analysis are conducted on the weld bead geometry to demarcate the zone of HAZ and fusion zone (FZ).

As the most important criteria for LBW of maraging steels is the provision of higher DOP, higher FZ width and lower heat-affected zone, the study intended to prove the applicability of GRA technique in solving multi-objective optimisation problems in applications like defence and unmanned systems.

This study aims to present a direct repurposing activity of consumed high-speed steel (HSS) hacksaw blade into fine-looking handmade knives to increase the awareness about sustainability by evaluating the relationship between the quality of material alloys and heat treatment as well as cultural aspects such as the treatment on the HSS hacksaw blade that will affect the material hardness.

The quality of HSS hacksaw blade samples was analyzed by using scanning electron microscope/energy dispersive X-Ray spectroscopy (SEM/EDX) through the identification of material element’s properties. Besides, finite element structural analysis was performed by using SolidWorks Simulation to evaluate the material performance by determining the Von Mises stress to find the factor of safety of the knife designs. Then, the effect of tribology implementation toward mechanical properties of the handmade knives was determined by using a Rockwell C hardness test.

It is found that the material composition of carbon plays a vital role in increasing and improving the hardness and wear resistance of the HSS hacksaw blade. The Von Mises stress obtained is lower than the yield strength of 3,250 MPa by 71.44 per cent with the safety factor of 3.58,which means the design will not be subjected to failure. The mechanical properties of the HSS hacksaw blade such as hardness were determined averagely by 5 per cent of hardness increase.

It has been validated that the tribological effect toward the material characteristic leads to hardness changes which contributed to the enhancement of tool life of the HSS hacksaw blade, thus producing better quality knives.

This paper presents the outcomes of the international project “Protecting Landscape Heritage: a requalification project as an instrument for the re-birth of Quang Tri Old Citadel in Vietnam”, achieved with scientific cooperation between the Università Politecnica delle Marche (Italy) and Hue University of Sciences (Vietnam) funded by the Italian Ministry of Foreign Affairs and International Cooperation and Ministry of Science and Technology of Vietnam. The research focuses on the Quang Tri Citadel, founded in 1809 and now in an advanced state of degradation.

For the purpose of rehabilitation, the wide multidisciplinary project first examined the historical context of the military model, the architectural aspects of the structure, the characterization of the existing materials, the degradation levels of different parts, and, finally, a proposal of the suggested interventions.

The original structure and geometry were extrapolated and studied. Building materials were produced with nearby raw materials. Firing temperatures of bricks ranged from 800 to 1,000 °C, hydraulic lime was supposed the binder of the mortar with a calcination temperature lower than 1,000 °C. Damage assessment was provided and after these analyses a requalification project was proposed so the cultural heritage can play a role for the future in the dialog between different cultures.

The requalification project achieved by an integrated analytical approach defines aspects in relation to the restoration of the structures, enabling compliance with the geometry, techniques, building materials used in the original construction and allowing its guardianship and management to align with the historical context of the architectural heritage.

Additive manufacturing (AM) processes involve a layer-by-layer sintering of metallic powders to produce fully functional three-dimensional parts. This layer-by-layer building process provides a unique opportunity to enhance mechanical properties by applying treatments that previously were possible only on the surface in traditional manufacturing techniques. The purpose of the study is to examine the effect of ultrasonic peening (UP) applied during a layer-by-layer direct metal laser sintering (DMLS) fabrication of 316L stainless steel on its mechanical properties and microstructure.

Uniaxial tensile tests were performed at 1.27 mm/s to determine the effect of UP treatment on the average global behavior of a 316L part, whereas hardness measurements using nanoindentation were performed to determine the modification of local mechanical properties. Compressive buckling tests at a loading rate of 3 mm/min were performed on sample coupons with a large aspect ratio to evaluate the effect of UP on any potential delamination of DMLS layers. Techniques such as optical and scanning electron microscopy (SEM) imaging were utilized to determine the effect of UP on the microstructure.

Overall, significant modification in mechanical properties such as hardness and yield strength, along with microstructure, was observed. Large increases in both the average global and local mechanical properties, as well as a disruption in the columnar grain microstructure, was observed in DMLS parts treated with UP treatment.

Results indicate an opportunity for UP to be used as an in-situ process during AM processes for dynamically altering the mechanical behavior, microstructure, and distortion due to residual stress formation, in a tunable fashion.

In this work, with a goal to ultimately forward the advancement of additive manufacturing research, the author applies the Wheeler-Boettinger-McFadden model through a progressive series of increasingly complex solidification problems illustrating the evolution of both dendritic as well as columnar growth morphologies. For purposes of convenience, the author assumes idyllic solutions (i.e. the excess energies associated with mixing solid and liquid phases can be neglected).

In this work, the author applied the phase-field model through a progressive series of increasingly complex solidification problems, illustrating the evolution of both dendritic as well as columnar growth morphologies. Beginning with a non-isothermal treatment of pure Ni, the author further examined the isothermal and directional solidification of Cu–Ni binary alloys.

(1) Consistent with previous simulation results, solidification simulations from each of the three cases revealed the presence of parabolic, dendrite tips evolving along directions of maximum interface energy. (2) For pure Ni simulations, changes in the anisotropy and noise magnitudes resulted in an increase of secondary dendritic branches and changes in the direction of propagation. The overall shape of the primary structure tended also to elongate with increased anisotropy. (3) For simulations of isothermal solidification of Ni–Cu binary alloys, the development of primary and secondary dendrite arm formation followed similar patterns associated with a pure substance. Calculations of dendrite tip velocity tended to increase monotonically with increasing anisotropy in accordance with previous research. (4) Simulations of directional solidification of Ni–Cu binary alloys with a linear temperature profile demonstrated the presence of cellular dendrites with relatively weak side-branching. The occurrence of solute trapping was also apparent between the primary dendrite columns. Dendrite tip velocities increased with increasing cooling rate.

This research, particularly the section devoted to directional solidification of binary alloys, describes a novel numerical framework and platform for the parametric analysis of various microstructural related quantities, including the effects due to changes in temperature gradient and cooling rate. Both the evolution of the phase and concentration are resolved.

The purpose of this paper is to study the use of titanium as a protecting element for aluminum in alkaline conditions.

Aluminum coatings containing up to 20 weight per cent Ti6Al4V were produced using laser cladding and were investigated using light optical microscope, scanning electron microscope – energy-dispersive X-ray spectroscopy and X-Ray Diffraction, together with alkaline exposure tests and potentiodynamic measurements at pH 13.5.

Cladding resulted in a heterogeneous solidification microstructure containing an aluminum matrix with supersaturated titanium (<1 weight per cent), Al₃Ti intermetallics and large partially undissolved Ti6Al4V particles. Heat treatment lowered the titanium concentration in the aluminum matrix, changed the shape of the Al₃Ti precipitates and increased the degree of dissolution of the Ti6Al4V particles. Corrosion testing showed significant localized dissolution of the aluminum matrix.

Increased titanium concentration and heat treatment gave improved alkaline corrosion properties. At pH 13.5, the Al₃Ti phases were protected, while the aluminum matrix corroded.

For alkaline corrosion-protection of aluminum in the automobile industry, titanium might be useful at pH values below 13.5 or by using other coating techniques.

This is the first study testing the use of titanium as a protective element of aluminum in stringent alkaline conditions.