Search results

To investigate the effect of the metallization and solder mask materials on the solder joint reliability of low temperature co‐fired ceramic (LTCC) modules.

The fatigue performance of six LTCC/PCB assembly versions was investigated using temperature cycling tests in the −40‐125°C and 20‐80°C temperature ranges. In order to eliminate fatigue cracking in the LTCC module itself, large AgPt‐metallized solder (1 mm) lands with organic or co‐fired glaze solder masks, having 0.86‐0.89 mm openings, were used. The performance of these modules was compared to that of AgPd‐metallized modules with a similar solder land structure. The joint structures were analysed using resistance measurements, scanning acoustic microscopy, SEM/EDS investigation, and FEM simulations.

The results showed that failure distributions with Weibull shape factor (β) values from 8.4 to 14.2, and characteristic life time (θ) values between 860 and 1,165 cycles were achieved in AgPt assemblies in the −40‐125°C temperature range. The primary failure mechanism was solder joint cracking, whereas the AgPd‐metallized modules suffered from cracking in the ceramic. In the milder test conditions AgPd‐metallized modules showed better fatigue endurance than AgPt‐metallized modules.

This paper proves that the cracking in ceramic in the harsh test condition can be eliminated almost completely by using AgPt metallization instead of AgPd metallization in the present test module structure.

The purpose of this paper is to develop the device made of low temperature co-fired ceramics (LTCC) and lead zirconate titanate (PZT) by co-firing both materials. In the paper, the technology and properties of a miniature uniaxial ceramic accelerometer are presented.

Finite element method (FEM) is applied to predict properties of the sensor vs main dimensions of the sensor. The LTCC process is applied during manufacturing of the device. All the advantages of the technology are taken into account during designing three-dimensional structure of the sensor. The sensitivity and resonant frequency of the accelerometer are measured. Real material parameters of PZT are estimated according to measurement results and FEM simulations.

The ceramic sensor integrated with SMD package with outer dimensions of 5 × 5 × 5 mm3 is manufactured. The accelerometer exhibits sensitivity of 0.75 pC/g measured at 100 Hz. The resonant frequency is equal to about 2 kHz. Useful frequency range is limited by 3 dB sensitivity change at about 1 kHz.

Sensitivity of the device is limited by interaction between LTCC and PZT materials during co-firing process. The estimated d parameters are ten times worse comparing to bulk Pz27 material. Further research on materials compatibility should be carried out.

The sensor can be easily integrated into various devices made of standard electronic printed circuit boards (PCBs). Applied method of direct integration of piezoelectric transducers with LTCC material enables manufacturing of complex ceramic systems with built-in accelerometer in the substrate.

The accelerometer is a sensor and a package simultaneously. The miniature ceramic device is compatible with surface mounting technology; hence, it can be used directly on PCBs for vibration monitoring inside electronic devices and systems.

The purpose of this study is to design, fabricate and investigate low-temperature co-fired ceramic (LTCC) structures with integrated microfluidic elements. Special attention is paid to the study of fluid properties of micro-channels and microvalves, which are important constitutive parts of both, microfluidic systems and individual microfluidic devices.

Several test patterns of fluid channels with different geometry and different types of valves were designed and realized in LTCC technology. All test structures were tested under the flow of two fluids (liquids): water and isopropyl alcohol. Flow rates at different applied pressure were measured and hydrodynamic resistance and diode effect were calculated.

The investigation of the channels showed that viscosity of fluidic media has significant influence on the hydrodynamic resistance in channels with rectangular cross-section, while this effect is small on channels with square cross-section. The viscosity also has a decisive influence on the diode effect of different shape of valves, and therefore, it is important in the selection of the valve in practical applications.

In this work, the investigation of hydrodynamic resistance of channels and diode effect of passive valves is limited on selected geometry and only on two fluidic media and two applied pressures. All these and some other parameters have a significant influence on fluidic properties, but this will be the topic of the next research work, which will be supported by numerical modelling.

The presented results are useful in the future designing process of LTCC-based microfluidic devices and systems.

Microfluidic in the LTCC structures is an unconventional use of this technology. Therefore, the fluid properties are relatively unsearched. On the other hand, the global use of microfluidic devices and systems is growing rapidly in various applications. They are mostly made by polymer materials, however, in more demanding applications; ceramic is a useful alternative.

The purpose of this paper is to report on fabrication procedure and present microstructure and dielectric behavior of willemite ceramic material with addition of 5% Li₂CO₃ as a sintering aid.

The samples were fabricated by ball milling of the ceramic powders, preparation of granulate and pressing and co-firing using temperature profile based on heating microscope observation. The dielectric properties of the material were measured by impedance spectroscopy (Hz-MHz), transmission method (GHz) and time domain spectroscopy (THz). The composition and microstructure of the material were investigated using X-ray diffraction, scanning electron microscopy and energy-dispersive spectroscopy analysis. Ceramic powder was used to fabricate a green tape and low temperature co-fired ceramics (LTCC) multilayer structures, which in the next steps of the research were examined at the angle of cooperation with conductive pastes, strength and geometric repeatability.

The fabricated material showed low sintering temperature (920°C–960°C), low dielectric constant 6.2–6.34 and low dissipation factor at the level of 0.004–0.007. As LTCC material, willemite with 5% Li₂CO₃ addition showed good compatibility with AgPd conductive paste.

Search for new materials with low dielectric constant, applicable in LTCC technology, and development of their fabrication procedure are important tasks for the progress in modern microwave circuits.

The purpose of this paper is to investigate the thermal behaviors of high power LED packages to enhance the thermal performances of low temperature co‐fired ceramic chip on board (LTCC‐COB) package. Thermal analysis demonstrated an improved LTCC‐COB package design that is comparable to a metal lead frame package with low thermal resistance.

The LED device developed in this study is a LTCC package mounted directly on the metal PCB. A numerical simulation was performed to investigate the thermal characteristics of the LED module using the finite volume method, which is embedded in commercial software (Fluent V.6.3). Thermal resistance and temperature measurement validate the simulated results.

The effect of the thickness of the die attach material on the thermal resistance was dominant due to low thermal conductivity, and the junction temperature decreased significantly with slight increases in thermal conductivity, especially when the value was less than 5 W/mK. The results reveal that the thermal resistance of MCPCB is about 49 per cent‐58 per cent of the junction to board thermal resistance. The thermal model results showed good agreement with experimental results.

The developed model overcomes the large thermal resistance of a conventional LTCC package for high power LED module. The extensive results have demonstrated an improved thermal design, optimal dimensions of each component and boundary conditions for high power LTCC‐COB type package.

The purpose of this paper was to develop the methodology of thick-film/low temperature co-fired ceramic (LTCC) multilayer thermoelectric microgenerator fabrication including the procedure of silver-nickel thermocouples integration with LTCC.

To miniaturize the structures and to increase the output parameters (generated voltage, electrical power), the microgenerator was designed as multilayer systems. It allows to reduce size of the system and to increase the number of thermocouples integrated inside the structure. It also protects buried thermocouples against exposure to harmful external factors (e.g. moisture, oxidation and mechanical exposures). As a substrate, LTCC was used. For the thermocouples fabrication, thick-film pastes based on silver and nickel were chosen. Ag/Ni thermocouple has nearly three times higher Seebeck coefficient and 30 per cent lower electrical resistance than the combination of Ag/PdAg used in previous works of the author.

A multi-layer thick-film thermoelectric generator based on LTCC and Ag, Ni pastes was fabricated. Thirty Ag/Ni thermocouples were precisely screen-printed on few layers. Thermocouples’ arms are 15 mm long and about 150 μm wide. Interlayer connections (via-holes filled with conductive paste) provided the electrical contact between the layers. The biggest fabricated harvester consisted of 90 miniature thermocouples buried inside the LTCC.

The paper presents the results of research that provided to optimize the co-firing process of the LTCC/Ni set. In the result, the methodology of co-firing of silver-nickel thermocouples and LTCC ceramic was elaborated. Also, the methodology of fabrication of miniature thermoelectric energy harvesters was optimized.

The purpose of this paper is to investigate the effect of electroless NiAu (ENIG) deposition on the failure mechanisms and characteristic lifetimes of three different non‐collapsible lead‐free 2nd level interconnections in low‐temperature co‐fired ceramic (LTCC)/printed wiring board (PWB) assemblies.

Five LTCC module/PWB assemblies were fabricated and exposed to a temperature cycling test over a −40 to 125°C temperature range. The characteristic lifetimes of these assemblies were determined using direct current resistance measurements. The failure mechanisms of the test assemblies were verified using X‐ray and scanning acoustic microscopy, optical microscopy with polarized light, scanning electron microscope (SEM)/energy dispersive spectroscopy and field emission‐SEM investigation.

A stable intermetallic compound (IMC) layer is formed between the Ni deposit and solder matrix during reflow soldering. The layer thickness does not grow excessively and the interface between the layer and solder is practically free from Kirkendall voids after the thermal cycling test (TCT) over a temperature range of −40 to 125°C. The adhesion between the IMC layer and solder matrix is sufficient to prevent separation of this interface, resulting in intergranular (creep) or mixed transgranular/intergranular (fatigue/creep) failure within the solder matrix. However, the thermal fatigue endurance of the lead‐free solder has a major effect on the characteristic lifetime, not the deposit material of the solder land. Depending on the thickness of the LTCC substrate and the composition of the lead‐free solder alloy, characteristic lifetimes of over 2,000 cycles are achieved in the TCT.

The paper investigates in detail the advantages and disadvantages of ENIG deposition in LTCC/PWB assemblies with a large global thermal mismatch (ΔCTE≥10 ppm/°C), considering the design and manufacturing stages of the solder joint configuration and its performance under harsh accelerated test conditions.

The purpose of this paper is to describe the behavior of different lead-free solders (95.5Sn3.8Ag0.7Cu, i.e. SAC387 and Sn7In4.1Ag0.5Cu, i.e. SAC-In) in thermomechanically loaded non-collapsible ball grid array (BGA) joints of a low-temperature co-fired ceramic (LTCC) module. The validity of a modified Engelmaier’s model was tested to verify its capability to predict the characteristic lifetime of an LTCC module assembly implementable in field applications.

Five printed wiring board (PWB) assemblies, each carrying eight LTCC modules, were fabricated and exposed to a temperature cycling test over a −40 to 125°C temperature range to determine the characteristic lifetimes of interconnections in the LTCC module/PWB assemblies. The failure mechanisms of the test assemblies were verified using scanning acoustic microscopy, scanning electron microscopy (SEM) and field emission SEM investigation. A stress-dependent Engelmaier’s model, adjusted for plastic-core solder ball (PCSB) BGA structures, was used to predict the characteristic lifetimes of the assemblies.

Depending on the joint configuration, characteristic lifetimes of up to 1,920 cycles were achieved in the thermal cycling testing. The results showed that intergranular (creep) failures occurred primarily only in the joints containing Sn7In4.1Ag0.5Cu solder. Other primary failure mechanisms (mixed transgranular/intergranular, separation of the intermetallic compound/solder interface and cracking in the interface between the ceramic and metallization) were observed in the other joint configurations. The modified Engelmaier’s model was found to predict the lifetime of interconnections with good accuracy. The results confirmed the superiority of SAC-In solder over SAC in terms of reliability, and also proved that an air cavity structure of the module, which enhances its radio frequency (RF) performance, did not degrade the reliability of the second-level interconnections of the test assemblies.

This paper shows the superiority of SAC-In solder over SAC387 solder in terms of reliability and verifies the applicability of the modified Engelmaier’s model as an accurate lifetime prediction method for PCSB BGA structures for the presented LTCC packages for RF/microwave telecommunication applications.

The purpose of this paper is to present the research activity and results to research and development society on the field of ceramic microsystems.

The chemical reactor was developed as a non-conventional application of low temperature co-fired ceramic (LTCC) and thick-film technologies. In the ceramic reactor with a large-volume, buried cavity, filled with a catalyst, the reaction between water and methanol produces hydrogen and carbon dioxide (together with traces of carbon monoxide). The LTCC ceramic three-dimensional (3D) structure consists of a reaction chamber, two inlet channels, an inlet mixing channel, an inlet distributor, an outlet collector and an outlet channel. The inlet and outlet fluidic barriers for the catalyst of the reaction chamber are made with two “grid lines”.

A 3D ceramic structure made by LTCC technology was successfully designed and developed for chemical reactor – methanol decomposition.

Research activity includes the design and the capability of materials and technology (LTCC) to fabricate chemical reactor with large cavity. But further dimensions-scale-up is limited.

The technology for the fabrication of LTCC-based chemical reactor was developed and implemented in system for methanol decomposition.

The approach (large-volume cavity in ceramic structure), which has been developed, can be used for other type of reactors also.

In microfluidic channel fabrication in low temperature co‐fired ceramics (LTCC), one of the biggest challenges is the elimination of channel deformation during lamination. The purpose of this paper is to describe the expected deformation of the substrate and the sacrificial layer (starch powder and 3D printed UV polymerized material) during the lamination process of microfluidic structure fabrication.

Uniaxial compression and Jenike shear test were used to obtain the mechanical parameters of starch sacrificial volume material (SVM). To determine the stress‐strain characteristics of LTCC a uniaxial compression experiment was conducted. The shape of the laminated LTCC containing embedded channel was modeled by finite element method using the mechanical parameters obtained by the measurements.

It was found that the choice of SVM plays an important role in channel deformation. A design rule is given considering the channel width and the choice of SVM based on the simulation results.

Until now the lamination step of LTCC technology was only optimized in an empirical way.