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This paper aims to establish a method to verify in real time the quality of a part being built using Selective Laser Sintering (SLS).

A SLS build of 30 Nylon 12 tensile bars was done while using an infrared camera to record the thermal history of each bar. The thermal history was then compared to the ultimate tensile strength (UTS) of each bar. In addition, an attempt was made to identify where the fracture of each bar occurred based on its thermal history.

Several analysis techniques were used to compare the thermal history of each bar to its UTS. The strongest correlation found was 0.746. In addition, multiple strategies for predicting the break location where used, with the most successful making a correct prediction on 46 per cent of the bars.

This paper studies the feasibility of in-situ build verification, a technique that if successful would greatly help the further adoption of SLS as a method of manufacturing.

Recent work has demonstrated the possibility of selectively sintering polymer powders with radio frequency (RF) radiation as a means of rapid, volumetric additive manufacturing. Although RF radiation can be used as a volumetric energy source, non-uniform heating resulting from the sample geometry and electrode configuration can lead to adverse effects in RF-treated samples. This paper aims to address these heating uniformity issues by implementing a computational design strategy for doped polymer powder beds to improve the RF heating uniformity.

Two approaches for improving the RF heating uniformity are presented with the goal of developing an RF-assisted additive manufacturing process. Both techniques use COMSOL Multiphysics® to predict the temperature rise during simulated RF exposure for different geometries. The effectiveness of each approach is evaluated by calculating the uniformity index, which provides an objective metric for comparing the heating uniformity between simulations. The first method implements an iterative heuristic tuning strategy to functionally grade the electrical conductivity within the sample. The second method involves reorienting the electrodes during the heating stage such that the electric field is applied in two directions.

Both approaches are shown to improve the heating uniformity and predicted part geometry for several test cases when applied independently. However, the greatest improvement in heating uniformity is demonstrated by combining the approaches and using multiple electrode orientations while functionally grading the samples.

This work presents an innovative approach for overcoming RF heating uniformity issues to improve the resulting part geometry in an RF-assisted, volumetric additive manufacturing method.

Additive manufacturing (AM) of thermoplastic polymers for powder bed fusion processes typically requires each layer to be fused before the next can be deposited. The purpose of this paper is to present a volumetric AM method in the form of deeply penetrating radio frequency (RF) radiation to improve the speed of the process and the mechanical properties of the polymer parts.

The focus of this study was to demonstrate the volumetric fusion of composite mixtures containing polyamide (nylon) 12 and graphite powders using RF radiation as the sole energy source to establish the feasibility of a volumetric AM process for thermoplastic polymers. Impedance spectroscopy was used to measure the dielectric properties of the mixtures as a function of increasing graphite content and identify the percolation limit. The mixtures were then tested in a parallel plate electrode chamber connected to an RF generator to measure the heating effectiveness of different graphite concentrations. During the experiments, the surface temperature of the doped mixtures was monitored.

Nylon 12 mixtures containing between 10% and 60% graphite by weight were created, and the loss tangent reached a maximum of 35%. Selective RF heating was shown through the formation of fused composite parts within the powder beds.

The feasibility of a novel volumetric AM process for thermoplastic polymers was demonstrated in this study, in which RF radiation was used to achieve fusion in graphite-doped nylon powders.

Considers efforts to date to produce parts by direct selective laser sintering (SLS) of metals, including post processing to improve structural integrity and/or to induce a transformation. Provides a brief overview of the basic principles of SLS machine operation, and discusses materials issues affecting direct SLS of metals and the resultant properties and microstructures of the parts. Reviews results of past efforts on SLS of metal systems such as Cu‐Sn, Cu‐Solder (Pb‐Sn), Ni‐Sn, pre‐alloyed bronze (Cu‐Sn). Finally discusses more recent efforts on SLS of bronze‐nickel powder mixtures in greater detail.

Functional testing of rapid prototypes (RP) represents an exciting area of research in solid freeform fabrication. One approach to functional testing is to use similitude techniques to correlate the behavior of an RP model and a product. Previous research at UT, Austin has resulted in the development of an empirical similitude technique for correlating the behavior of parts with different material properties. Advances in the empirical similitude technique are presented in this paper. Sources of coupling between material properties and geometric shape that produce distortions in the current empirical similitude technique are outlined. A modified approach that corrects such distortions is presented. Numerical examples are used to illustrate both the current and the advanced empirical similitude methods.

Gives a brief overview of post‐processing of selective laser sintered (SLS) metal parts to improve structural integrity and/or to induce a material transformation. Presents results which show the effect of post‐processing liquid phase sintering temperature and time on material properties. Describes the hot isostatic pressing process, and discusses its application to SLS metal parts. Results gained from using this process show that it is suitable for achieving almost full‐density parts.

The purpose of this paper is to acquire thermal conductivities of both fresh and preheated polyamide 12 powder under various conditions to provide a basis for effective and accurate control during the laser sintering (LS) process.

A Hot Disk® TPS 500 thermal measurement system using a transient plane source (TPS) technology was employed for thermal conductivity measurements. Polyamide 12 powder was packed at different densities, and different carrier gases were used. Tests were also performed on fully dense laser sintered polyamide 12 to establish a baseline.

Polyamide 12 powder thermal conductivity varies with packing density and temperature, which is approximately one-third bulk form thermal conductivity. Inter-particle bonding is the primary factor influencing polyamide 12 thermal conductivity.

Limited ranges of density were tested, and the carrier gas needed carefully control to prevent powder oxidation. Thermal properties obtained were not tested in the LS process.

This experimental result could be used to enhance thermal control during the LS process.

Presents the mechanical properties of a new mould‐making material, proposed for producing rapidly prototyped injection mould inserts for plastics by selective laser sintering. Explains that although the strength of this material is far below that of the tool steel usually used to fabricate moulds, design calculations indicate that it can still be used for mould insert production. Points out that the thermal conductivity of this material is lower than that for steel but higher than that for plastic melts. Indicates from the calculations that proper choices of conduction length and cycle time can minimize differences, relative to steel moulds, in the operational behaviour of moulds made of the new material. Discusses the longevity of example moulds.

The purpose of this paper is to analyze the bulk energy transport processes in the build chamber environment before and during laser sintering (LS) to provide a basis for effective and accurate thermal control for the LS process. This leads to improved mechanical properties and geometrical tolerances for LS products and may be applied to optimize operation cycle times for the LS process.

Computational models with two levels of complexity were built to explore the heat transfer mechanisms in the LS process. In a one-dimensional model (1D), the powder performed as a semi-infinite solid and heater flux to the powder surface was modeled with a heater control law. A two-dimensional (2D) fluid/solid finite element model of the build chamber and powder bins provided insight into the thermal processes in the build chamber.

Numerical 1D simulations were verified with measurements from sensors embedded in the build chamber powder bed. Using a 2D model, computed powder surface temperatures during the warm up and build phases were verified with an infrared camera. Convective currents in the build chamber and non-uniformities in the distribution of temperature over the radiant heater surface were found to be substantial contributors to non-uniformities in the powder bed surface temperature.

Limited heat sources were analyzed. No three-dimensional model was built. Assumptions to decrease the part bed temperature difference were not tested.

These simulation and experimental results may be used to enhance thermal control and operation efficiency during the LS process and to improve LS product mechanical properties.

This paper aims to study the effects of solid additives and compounding processes on the selective laser sintering (SLS) behavior of composite powders.

Composite powders were prepared from TrueForm™ acrylic‐styrene co‐polymer and SiO₂ powder. Dry mixing and melt extrusion were used as the blending processes to produce the composite powders. Some SiO₂ powder was ground and treated with silane coupling agent before blending to study the effects of particle size and surface treatment of the filler, respectively. The temperature of the powder bed was monitored using an infrared thermometer. The fusion behaviors of the powders were investigated in situ using an optical microscope and the sintered specimens were examined by scanning electron microscopy.

For a given volume fraction of the filler, reducing its particle size will hinder fusion between the polymer particles and weaken the sintered specimens. Surface treatment of the filler by silane coupling agent had little effect on the morphology of the sintered specimens; however, it slightly improved their strength. The blending method plays an important role in the sintering behavior of the composite powders. Although melt blending improved the polymer‐to‐polymer contact between the composite powder particles, the high‐resultant viscosity of the material adversely affected the densification of the powder bed, leading to a highly porous structure of the sintered specimens.

The sintering experiments were conducted in ambient conditions using a laser engraving machine instead of a commercial SLS machine with atmospheric control. The temperature gradient within the powder bed was expected to be higher than that in normal SLS processes.

The SLS behavior of a composite powder not only depends on its composition but also on the powder preparation method or powder morphology.

This paper provides some useful information for future development of composite powders for SLS applications.