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This work proposes the utilization of electromechanical impedance measurements as a means of non-destructive evaluation (NDE) for additive manufacturing (AM). The effectiveness and sensitivity of the technique for a variety of defect types commonly encountered in AM are investigated.

To evaluate the feasibility of impedance-based NDE for AM, the authors first designed and fabricated a suite of test specimens with build errors typical of AM processes, including dimensional inaccuracies, positional inaccuracies and internal porosity. Two polymer AM processes were investigated in this work: material jetting and extrusion. An impedance-based analysis was then conducted on all parts and utilized, in a supervised learning context, for identifying defective parts.

The newly proposed impedance-based NDE technique has been proven to be an effective solution for detecting several types of print defects. Specifically, it was shown that the technique is capable of detecting print defects resulting in mass change (as small as 1 per cent) and in feature displacement (as small as 1 mm) in both extruded nylon parts and jetted VeroWhitePlus parts. Internal porosity defects were also found to be detectable; however, the impact of this defect type on the measured impedance was not as profound as that of dimensional and positional inaccuracies.

Compared to currently available NDE techniques, the newly proposed impedance-based NDE is a functional-based technique with the advantages of being cost-effective, sensitive and suitable for inspecting AM parts of complex geometry and deeply embedded flaws. This technique has the potential to bridge the existing gaps in current NDE practices, hence paving the road for a wider adoption of AM to produce mission-critical parts.

The purpose of this paper is to propose a fast, accurate and efficient algorithm for assessment of input impedance and consequently the evaluation of transient impedance of the grounding electrode.

The mathematical model is based on the thin wire antenna theory and related Pocklington integro-differential equation in the frequency domain, which is numerically treated via Galerkin-Bubnov variant of the indirect boundary element method (GB-IBEM). Two different approaches, scattered voltage method (ScVM) and induced electromotive force – boundary element method (IEMF-BEM), for input and transient impedance are discussed in detail. Extensive numerical experiments have been undertaken to analyze numerical sensitivity of the methods.

Although it was widely used so far, the ScVM, was shown to be unsuitable for the grounding impedance assessment because results are dependent on the number of elements used in the numerical solution. On the other hand, the other method, IEMF-BEM is rather stable, with the respect to the number of elements used and with excellent convergence rate. In addition, IEMF-BEM is much simpler to implement as it requires only multiplication of matrices already assembled within the procedure of current distribution calculation, as opposed to the ScVM which requires numerical integration of quasi-singular integrals which, by it self, can be very demanding.

The IEMF-BEM is originally developed by the authors and used for the first time for grounding impedance assessment. It is simple and very efficient and can easily be extended to arbitrary grounding configurations.

This paper aims to better design the resonant tank parameters for LLC resonant converter. And, it is found that under heavy load, the voltage gain is affected by junction capacitors of the primary side switching and the parasitic parameters of the secondary side diodes converted to the primary side, which will cause the voltage gain decreased when the switching frequency decreased.

This paper proposes an optimization parameters design method to solve this problem, which was based on impedance model considering the parasitic parameters of switching devices and diodes.

The effectiveness of the proposed method is verified by impedance Bode plots and experimental results.

From the perspective of impedance modeling, this paper finds the reasons for the insufficient voltage regulation capability of LLC resonant converters under heavy load and finds solutions through analysis.

The purpose of this paper is to examine the passive layer on 1050A aluminium alloy in non‐stationary conditions of linearly raised and lowered temperatures by means of dynamic electrochemistry impedance spectroscopy (DEIS).

The oxide passive layer on aluminium was examined using DEIS under non‐stationary conditions of linearly raised and lowered temperatures. In total, five heating‐cooling cycles were performed.

A significant change of impedance was observed only during the first cycle, which was called the forming one. During the subsequent cycles, the impedance of the system changed in a reversible manner.

The analysis using a equivalent circuit allowed us to determine a change of electric parameters of the circuit in the temperature function. Obtained changes of the electric parameters were correlated with layer structure.

The purpose of this paper is to present the investigation of aluminum alloy by means of dynamic electrochemical impedance spectroscopy (DEIS), which is simultaneous method of AC impedance and DC polarization measurements.

A method of DEIS has been applied. Changes in equivalent circuit (EC) parameters versus potential for both investigated aluminium alloys are evaluated.

On the basis of obtained results, it is unambiguously demonstrated that the addition of 4.5 percent magnesium degraded the anticorrosive properties of the test alloys. It is difficult to define unequivocally the range of passive state and a moment of passive layer breakdown on the basis of current/voltage dependencies. However, application of the DEIS method and analysis of the evolution of particular elements of an electrical EC allowed identification of the instant of corrosion process initiation.

The presented method is only suitable for laboratory evaluation of metal alloys because it requires sophisticated measuring equipment and is a difficult and time‐consuming way to obtain final results.

In one experiment, both polarization (DC) data and impedance (AC) measurements can be obtained. This allows the electrochemical properties of very similar aluminum alloys to be compared precisely with one other.

Impedance data obtained by electrochemical impedance spectroscopy (EIS) are fitted to a relevant electrical equivalent circuit to evaluate parameters directly related to the resistance and the durability of metal–coating systems. The purpose of this study is to present a novel and more efficient computational strategy for the modelling of EIS measurements using the Differential Evolution paradigm.

An alternative method to non-linear regression algorithms for the analysis of measured data in terms of equivalent circuit parameters is provided by evolutionary algorithms, particularly the Differential Evolution (DE) algorithms (standard DE and a representative of the self-adaptive DE paradigm were used).

The results obtained with DE algorithms were compared with those yielding from commercial fitting software, achieving a more accurate solution, and a better parameter identification, in all the cases treated. Further, an enhanced fitting power for the modelling of metal–coating systems was obtained.

The great potential of the developed tool has been demonstrated in the analysis of the evolution of EIS spectra due to progressive degradation of metal–coating systems. Open codes of the different differential algorithms used are included, and also, examples tackled in the document are open. It allows the complete use, or improvement, of the developed tool by researchers.

The purpose of this paper is to investigate the electrical transport mechanism of the Al‐doped ZnO nanorods at different temperatures by employing impedance spectroscopy.

Al‐doped ZnO nanorods were grown on silicon substrate using step sol‐gel method. For the seed solution preparation Zinc acetate dihydrate, 2‐methoxyethanol, monoethanolamine and aluminum nitrite nano‐hydrate were used as a solute, solvent, stabilizer and dopant, respectively. Prior to the deposition, P‐type Si (100) wafer was cut into pieces of 1 cm×2 cm. The samples were then cleaned in an ultrasonic bath with acetone, ethanol, and de‐ionized (DI) water for 5 min. The prepared seed solution was coated on silicon substrate using spin coater at spinning speed of 3000 rpm for 30 s and then dried at 250°C for 10 min followed by annealing at 550°C for 1 h. The hydrothermal growth was carried out in a solution of zinc nitrate hexahydrate (0.025M), Hexamethyltetramine (0.025M) in DI water.

Al‐doped ZnO nanorods were characterized using scanning electron microscope (SEM), X‐ray diffraction (XRD) and impedance spectroscopy. The impedance measurements were carried out at various temperatures (100°C‐325°C). The impedance results showed that temperature has great influence on the impedance; the impedance value decreased as the temperature increased. This decrement is attributed to the increase of the mobility of the defects, especially the oxygen vacancies. The surface morphology of the samples was measured by SEM and X‐ray diffraction. The SEM images show that the high density of Al‐doped ZnO nanorods covers the silicon substrate, whereas the XRD pattern shows the (002) crystal orientation.

This paper demonstrates the electron transport mechanism of Al‐doped ZnO nanorods, at different temperatures, to understand the charge transport model.

An electrochemical impedance spectroscopy technique based on an equivalent circuit used for the evaluation of metallic substratum/organic coating/electrolyte systems as well as the importance of each parameter and the way to calculate it is analysed. It is emphasised that the classical semi circumference in the complex plot, which describes the response of a parallel RC circuit, is not real axis centred. This fact makes it necessary to consider the organic film and electrochemical double layer capacitance as pseudo‐capacitances which depend on a fractional power of the frequency. Starting from mathematical relationships over the total impedance algorithms based on the least squares methods are proposed to fit experimental data requiring less processing time than iterative techniques. The methodology is described analysing the charge transfer resistance, ionic resistance and dielectric capacitance variation at increasing immersion times for naval steel/chlorinated rubber (with different PVC)/artificial sea water systems. Parameters thus obtained correlate well with the naval steel/organic coating deterioration with time, also determined by using corrosion potential measurements and visual assessment.

The purpose of this research was to verify the changes in the body weight of breastfeeding women, using the anthropometric and the bioelectrical impedance (BIA) methods. The sample was formed by 30 women who were exclusively breastfeeding their children, with an average age of 27.9±4.4 years old, followed up during four appointments in a public hospital of Rio de Janeiro, Brazil. The anthropometric data showed a significant reduction of body weight during the studied period. Regarding skinfolds, we observed a greater loss in the lower part of the abdominal region, in the suprailiac region and in the thigh. The same occurred to the body circumferences. Resistance values remained unaltered, thus indicating that the total body water content was preserved. We concluded that the significant reduction of body weight was mainly due to the mobilization of the fat tissue, being unrelated to changes in the body water content. In addition, we verified how important it is to associate different methods to assess the change of body weight during breastfeeding.

This paper aims to enhance the barrier properties and active protection of a water-based silane coating on mild steel through nanoclay and zinc acetylacetonate simultaneously included into the formulation.

The corrosion protection performance of the silane sol-gel coatings with no additive, zinc acetylacetonate, nanoclay and nanoclay + zinc acetylacetonate was monitored using electrochemical impedance spectroscopy during 5 h of immersion in a sodium chloride solution. Moreover, the surface of coatings was analyzed using a field emission scanning electron microscopy equipped with an energy dispersive X-ray spectrometer (FESEM-EDX) and water contact angle measurements.

In electrochemical impedance spectroscopy analysis, the impedance at low frequencies, coating resistance and charge transfer resistance were the parameters considered which indicated the superiority of silane coating formulated with both nanoclay and zinc acetylacetonate. According to the results of FESEM/EDX and water contact angle measurements, the superiority was linked with the enhancement in the barrier properties in the presence of nanoclay, as well as function of the corrosion inhibitor at coating–substrate interface.

According to the literature, there is no research conducted to study the impact of the simultaneous use of nanoclay and zinc acetylacetonate on the barrier properties and active protection of an eco-friendly silane sol-gel coating including glycidyloxypropyltrimethoxysilane, tetraethoxysilane and methyltriethoxysilane on mild steel in a sodium chloride solution.