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The purpose of this study was to examine the impact of five key build parameters – layer thickness, deposition angle, infill, extrusion speed and extrusion temperature, and their interactions – on the maximum flexural force in specimens which are made of polylactic acid (PLA).

Through a previous study on the flexural properties of PLA specimens, a statistically significant effect of layer thickness was indicated, requiring further experimentation to establish the values of quadratic term in the model, as well as to perform optimization. Instead of performing a conventional Central Composite Design, a novel, definitive screening design (DSD) was used as statistical method. DSD allowed the reduction of the number of runs required for optimization while minimizing aliasing.

Significance of deposition angle and infill as main effects was established. Moreover, significant two-way interactions between infill/layer thickness and infill/extrusion speed were detected and discussed. The optimization procedure showed that minimum level of deposition angle, maximum levels of extrusion speed and infill and near mid-level of layer thickness yield maximum flexural force.

In this study, the three levels of infill were 0.1, 0.2 and 0.3, which corresponds to 10, 20 and 30 per cent of infill, respectively. In everyday practice, infill is usually kept within this range since it allows time-efficiency, i.e. significant reduction of build time. Though, unsurprisingly, higher infill is positively correlated with flexural strength, this study provides practical directions for optimal selection of other key parameters when working with low infill values.

Optimal 3D printing with low infill can contribute to lower material waste and pollution, while PLA plastic’s biodegradability remains high on the environment protection agenda.

According to available literature, no previous studies have investigated the FDM extrusion of PLA material using a combination of low infill, deposition angle, layer thickness, extrusion speed and extrusion temperature.

The purpose of this paper is to investigate the effect of process parameters of fused deposition modelling (FDM) 3D printing process on viscoelastic responses (creep compliance and recoverable compliance) of FDM built parts using a novel experimental design technique.

As part of the process characterization, a recently developed class of three-level design methodology – definitive screening design (DSD) – was used in this study to fit a second-order polynomial regression model. Artificial neural network (ANN) was also used to determine the optimal process parameters to improve creep compliance and recoverable compliance. The relationship between layer thickness, air gap, raster angle, build orientation, road width, number of contours and creep performance of FDM fabricated part was thereafter established empirically. Scanning electron microscope (SEM) is used to examine and characterize the morphology of the structures for some samples.

This study found that the creep resistance of FDM-manufactured part is significantly influenced by layer thickness, air gap, raster angle and number of contours and it can be improved by optimizing the settings of the selected parameters. The relationship between FDM process parameters and creep properties was determined, with the best creep performance observed by using 0.127 mm of layer thickness, zero air gap, zero raster angle, build orientation of 17.188°, road width of 0.4572 mm and 10 contours. Finally, the result is verified by confirmation experiments. The results prove that a DSD is a very effective design in characterizing the influence of process parameters on creep properties of FDM-built part at the lowest cost.

The originality of this paper lies in characterizing and optimizing the effect of process parameters on creep performance of FDM manufactured part that has not been studied in all previous studies. The paper highlights, for the first time, how the application of DSD can overcome most of the limitations encountered in the conventional techniques. This study can be used as a guide to the different additive manufacturing users of various industries and the results provide a good technical database on how FDM process parameters influence the creep performance of manufactured parts.

This paper aims to propose a vacuum-assisted post-processing method for use in binder jetted technology. The method is based on six key technological parameters and uses standard, commercially available consumables to achieve improvement in tensile strength, as well as the microstructure and porosity of the infiltrated matrix.

Six key technological parameters were systematically varied as factors on three levels, using design of experiment, i.e. definitive screening design. Surface response methodology was used to optimize the process and yield optimal tensile strength for the given range of input factors. Thus obtained, the optimized factor settings were used in a set of confirmation runs, where the result of optimization was experimentally confirmed. To confirm improvement in microstructure of the infiltrated matrix, SEM analysis was performed, while the reduction of porosity was analyzed using mercury porosimetry.

The obtained results indicate that, compared to its conventional counterpart, the proposed, optimized infiltration method yields improvement in tensile strength which is significant from both the statistical and engineering point of view, while reducing porosity by 3.5 times, using only standard consumables. Scanning electron microscopy examination of fractured specimens’ micrographs also revealed significant morphological differences between the conventional and proposed method of post-processing. This primarily reflects in higher surface area under hardened epoxy infiltrate, which contributes to increased load capacity of specimen cross-section.

At the present stage of development, the most important limitation of the proposed method is the overall size of models which can be accommodated in standard vacuum impregnation units. Although, in this study, the infiltration method did not prove statistically significant, further investigation is required with models of complex geometry, various sizes and mass arrangements, where infiltration would be more challenging and could possibly result in different findings.

The most important practical implication of this study is the experimentally verified result of optimization, which showed that tensile strength and matrix microstructure can be significantly improved, using just standard consumables.

Improved strength contributes to reduction of material consumption, which, in a longer run, can be beneficial for environment protection and sustainable development.

Based on literature review, there have been no previous investigations which studied the tensile strength of infiltrated specimens through design of experiment, which involved specimen preheating temperature, level and duration of vacuum treatment of infiltrate mixture and infiltrated specimens and infiltration method.

This study aims to investigate the impact of layer thickness, extrusion temperature, extrusion speed and build plate temperature on the tensile strength, crystallinity achieved during fabrication (herein, in-process crystallinity) and mesostructure of Poly(lactic acid) specimens. Both tensile strength and in-process crystallinity were optimized and verified as the function of processing parameters, and their relationship was thoroughly examined.

The four key technological parameters were systematically varied as factors on three levels, using the statistically designed experiment. Surface response methodology was used to optimize tensile strength and crystallinity for the given ranges of input factors. Optimized factor settings were used in a set of confirmation runs, where the result of optimization was experimentally confirmed. Material characterization was performed using differential scanning calorimetry and X-ray diffraction analysis, while the effect of processing parameters on mesostructure was examined by scanning electron microscopy.

Layer thickness and its quadratic effect are dominant contributors to tensile strength. Significant interaction between layer thickness and extrusion speed implies that these parameters should always be varied simultaneously within designed experiment to obtain adequate process model. As regards, the in-process crystallinity, extrusion speed is part of two significant interactions with plate temperature and layer thickness, respectively. Quality of mesostructure is vital contributor to tensile strength during FDM process, while the in-process crystallinity exhibited no impact, remaining below the 20 per cent margin regardless of process parameter settings.

According to available literature, there have been no previously published investigations which studied the effect of process parameters on tensile strength, mesostructure and in-process crystallinity through systematic variation of four critical processing parameters.