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Article
Publication date: 21 October 2019

Khaled Mostafa and Azza El-Sanabary

This study aims to explore the incorporation of the authors previously prepared chitosan nanoparticles (CNPs) of size around 60-100 nm in the cross-linking formulation of viscose…

Abstract

Purpose

This study aims to explore the incorporation of the authors previously prepared chitosan nanoparticles (CNPs) of size around 60-100 nm in the cross-linking formulation of viscose fabrics to see CNPs impact in terms of imparting multi-functional characteristics such as tensile strength, dry wrinkle recovery angles and antibacterial properties.

Design/methodology/approach

CNPs of size around 60-100 nm were incorporated in cross-linking formulations for viscose fabrics, including different concentrations of glutaraldehyde as a non-formaldehyde cross-linking agent and magnesium chloride hexahydrate as a catalyst. The formulations were applied at different curing times and temperatures in 100 mL distilled water, giving rise to a wet pickup of ca. 85 per cent. The fabrics were dried for 3 min at 85°C and cured at specified temperatures for fixed time intervals in thermo fixing oven according to the traditional pad-dry-cure method.

Findings

The above eco-friendly method for finished viscose fabrics was found to obtain high dry wrinkle recovery angle and maintain the tensile strength of the finished fabric within the acceptable range, as well as antibacterial properties against Escherichia coli and Staphylococcus aureus as a gram-negative and gram-positive bacteria, respectively. Both, scanning electron microscope and nitrogen percent on the finished fabric confirm the penetration of CNPs inside the fabric structure. Finally, viscose fabrics pageant antibacterial activity against gram-positive and gram-negative bacteria assessed even after 20 washing cycle.

Research limitations/implications

CNPs with its flourishing effect with respect to cationic nature, biodegradability, reactivity, higher surface area and antimicrobial activity; in addition to glutaraldehyde as non-formaldehyde finishing agent can be used as multi-functional agents for viscose fabrics instead of DMDHEU, polyacrylate and monomeric composites as hazardous materials.

Practical implications

CNPs as cationic biopolymers were expected to impart multi-functional properties to viscose fabrics especially with obtaining reasonable dry wrinkle recovery angle and tensile strength in addition to antibacterial properties.

Originality/value

The novelty addressed here is undertaken with a view to impart easy care characteristics and antibacterial activities onto viscose fabrics using CNPs as antimicrobial agent and glutaraldehyde as non-formaldehyde durable press finishes to-replace the traditional formaldehyde-based resins. Besides, to the authors’ knowledge, there is no published work so far using the above cross-linking formulation written above.

Details

Pigment & Resin Technology, vol. 49 no. 1
Type: Research Article
ISSN: 0369-9420

Keywords

Article
Publication date: 16 October 2023

Nonsikelelo Sheron Mpofu, Josphat Igadwa Mwasiagi, Cleophas Achisa Mecha and Eric Oyondi Nganyi

This study aims to investigate the potential use of potato peel extracts as antibacterial finishes for cotton fabrics against Staphylococcus aureus and Escherichia coli. Potato…

Abstract

Purpose

This study aims to investigate the potential use of potato peel extracts as antibacterial finishes for cotton fabrics against Staphylococcus aureus and Escherichia coli. Potato peels are abundant as waste and provide a natural, cheaper and sustainable alternative means of preventing the spread of bacterial infections on cotton fabric.

Design/methodology/approach

This research included the characterization of potato peel extracts, application of the extract onto cotton fabric and efficacy testing of the treated cotton fabric against bacteria. Phytochemical screening, agar well diffusion antibacterial test, minimum inhibitory concentration and Fourier transform infrared (FTIR) tests were used to characterize the extract. Antibacterial efficacy of the treated fabric was determined qualitatively using the disc diffusion assay and quantitatively using the bacteria reduction test.

Findings

Phytochemical screening confirmed the presence of several secondary metabolites including phenols and flavonoids. Antibacterial tests revealed a positive response in Escherichia coli and Staphylococcus aureus with a zone of inhibition of 6.50 mm and 5.60 mm, respectively. Additional peaks on the FTIR spectroscopy confirmed the presence of potato peel extract on the treated cotton fabric. The treated cotton fabrics showed efficacy against Staphylococcus aureus and Escherichia coli up to 20 washes.

Originality/value

This study introduced the application of potato peel extracts onto cotton fabrics and assessment of the antibacterial properties before and after washing. Results of this study suggest that potato peel extracts can be used as an organic eco-friendly antibacterial finish for cotton fabrics.

Details

Research Journal of Textile and Apparel, vol. ahead-of-print no. ahead-of-print
Type: Research Article
ISSN: 1560-6074

Keywords

Article
Publication date: 15 September 2022

Saima Habib, Farzana Kishwar and Zulfiqar Ali Raza

The purpose of this study is to apply silver nanoparticles on the cellulosic fabric via a green cross-linking approach to obtain antibacterial textiles. The cellulosic fabrics may…

Abstract

Purpose

The purpose of this study is to apply silver nanoparticles on the cellulosic fabric via a green cross-linking approach to obtain antibacterial textiles. The cellulosic fabrics may provide an ideal enclave for microbial growth due to their biodegradable nature and retention of certain nutrients and moisture usually required for microbial colonization. The application of antibacterial finish on the textile surfaces is usually done via synthetic cross-linkers, which, however, may cause toxic effects and halt the biodegradation process.

Design/methodology/approach

Herein, we incorporated citrate moieties on the cellulosic fabric as eco-friendly crosslinkers for the durable and effective application of nanosilver finish. The nanosilver finish was then applied on the citrate-treated cellulosic fabric under the pad-dry-cure method and characterized the specimens for physicochemical, textile and antibacterial properties.

Findings

The results expressed that the as-prepared silver particles possessed spherical morphology with their average size in the nano range and zeta potential being −40 ± 5 mV. The results of advanced analytical characterization demonstrated the successful application of nanosilver on the cellulosic surface with appropriate dispersibility.

Practical implications

The nanosilver-treated fabric exhibited appropriate textile and comfort and durable broad-spectrum antibacterial activity.

Originality/value

The treated cellulosic fabric expressed that the cross-linking, crystalline behavior, surface chemistry, roughness and amphiphilicity could affect some of its comfort and textile properties yet be in the acceptable range for potential applications in medical textiles and environmental sectors.

Details

Pigment & Resin Technology, vol. 53 no. 2
Type: Research Article
ISSN: 0369-9420

Keywords

Article
Publication date: 18 May 2021

Jemal Endris and Nalankilli Govindan

The purpose of this study is to establish a suitable procedure for dyeing and multifunctional finishing on 100% cotton using extracts of eucalyptus leaves in an eco-friendly…

Abstract

Purpose

The purpose of this study is to establish a suitable procedure for dyeing and multifunctional finishing on 100% cotton using extracts of eucalyptus leaves in an eco-friendly manner.

Design/methodology/approach

Box–Behnken design of experiments and analysis of variance (ANOVA) were used to optimise the conditions of extraction, dyeing and finishing. Phytochemical analysis was performed to determine the chemical constituents of the extracts. Colour strength, fastness properties were evaluated for dyed fabric samples. The effectiveness of eucalyptus leaves extract as an insect repellent, aroma, antibacterial finishing agent, was assessed. Pre-soaking and padding method was used for the application of active essential oil on the fabric.

Findings

Essential oil extracted from Eucalyptus globulus leaves have great repellent rate for insects to the extent of 90% and aroma intensity of 72% and antibacterial effect of 100% bacterial reduction up to five washings. The use of citric acid as cross-linking agent helps increase the durability of the finish. Natural dyeing to get light yellow shade is possible with extracts made with water, possessing good fastness properties.

Research limitations/implications

Scaling up the extraction process and soaking larger quantities of fabrics in extracted essential oil solution before the pad applications are considered limitations of this study. However, smaller pieces of fabrics can conveniently be handled in this process. It has tremendous potential for practising industrially, to get yellow-shaded multifunctional finished cotton textiles.

Practical implications

Protection against insects, including mosquitoes, bacteria with additional aroma on cotton will be of great use in day-to-day life for the wearer.

Social implications

Eco-friendly, renewable sources of ingredients from the plant were used to obtain protection against pathogenic or odour-causing microorganisms using this hygiene finish with multiple end uses.

Originality/value

This original work enables conducting dyeing and multifunctional finishing together in a single stage, which otherwise takes a number of steps, consuming large quantities of water, chemicals and energy to impart similar effects on cotton.

Details

Research Journal of Textile and Apparel, vol. 25 no. 3
Type: Research Article
ISSN: 1560-6074

Keywords

Article
Publication date: 6 April 2021

Gemeda Gebino, Gezu Ketema, Adina Fenta, Gideon Kipchirchir Rotich and Ayalew Debebe

The purpose of this study was to evaluate the extract of Moringa stenopetala seed oil, by organic solvents (methanol and hexane), for its efficacy against microbial activity on…

Abstract

Purpose

The purpose of this study was to evaluate the extract of Moringa stenopetala seed oil, by organic solvents (methanol and hexane), for its efficacy against microbial activity on cotton fabrics. The selected microbes for the study were two types of bacteria which are Gram-positive (S. aureus) and Gram-negative (E. coli).

Design/methodology/approach

Two types of bacteria, Gram-positive (S. aureus) and Gram-negative (E. coli) were used. The extract was applied on fabrics at a concentration of 5, 10 and 15 g/L using the pad-dry-cure method and antibacterial activities verified by the bacterial-growth reduction method. The treated fabrics were evaluated for antimicrobial activity against the bacteria before and after 15 washing cycles. The extract was examined for molecular structural change using fourier transform infrared spectroscopy (FTIR) and physical properties of the fabric; tensile strength, elongation, air permeability, stiffness and wettability were evaluated.

Findings

Results showed treated fabrics reduces the growth of Gram-positive (S. aureus) and Gram-negative (E. coli) bacteria from 77.6%–100% before wash and 45.8%–85.2% after wash for both extract concentrations. Comparing extracts, hexane extract reduces all bacteria growth than methanol extract for both extract concentrations while S. aureus was more susceptible to antimicrobial agents than E. coli at a lower concentration. As result, the tensile strength and air permeability were relatively lower than untreated ones without affecting the comfort properties of the fabric.

Originality/value

This study indicates that the Moringa stenopetala seed oil extract has a strong antimicrobial activity.

Details

Research Journal of Textile and Apparel, vol. 25 no. 3
Type: Research Article
ISSN: 1560-6074

Keywords

Article
Publication date: 15 December 2020

Kh M. Mostafa and A.A. El-Sanabary

This study aims to use multi-functional viscose fabric that was facilely developed with with respect to ease and care characteristics, reinforcement effect and antibacterial

Abstract

Purpose

This study aims to use multi-functional viscose fabric that was facilely developed with with respect to ease and care characteristics, reinforcement effect and antibacterial activity by using novel echo friendly antibacterial finish based on citric acid/sodium hypophosphite and the authors’ previously tailor-made poly meth acrylic acid (MAA)-chitosan graft copolymer via alternative microwave curing approach instead of traditional high-temperature cure one.

Design/methodology/approach

Viscose fabric was paddled twice in the cross-linking formulations containing different concentrations of citric acid, poly (MAA)-chitosan graft copolymer and sodium hypophosphite to 90 % wet pick up and dried at 100°C for 3 min in an electric oven. Then, the treated fabrics were placed on the disk spinner of the microwave oven and cured at different power (100–800 Watt) for various durations (60–180 s). The fabric was then water-rinsed and dried at ambient condition before use.

Findings

Results revealed that the above echo friendly method for finished viscose fabrics was found to achieve relatively high dry wrinkle recovery angle and maintain the loss in tensile strength within the acceptable range, as well as antibacterial activity against Escherichia coli and Staphylococcus aureus as a gram-negative and gram-positive bacteria, respectively; in addition to durability up to ten washing cycles. Furthermore, scanning electron microscope images, nitrogen content and add on % of the finished fabric confirmed the penetration of grafted chitosan inside the fabric structure. The tentative mechanism for these reactions is advocated.

Originality/value

The novelty addressed here is undertaken with the advantages of using citric acid as a nonformaldehyde, safe and cheap poly carboxylic acid as a crosslinking agent and sodium hypophosphite as a potential catalyst, in addition to the authors’ noncitable multifunctional echo friendly tailor-made poly (MAA)-chitosan graft copolymer for imparting reinforcement and antibacterial characteristics to viscose fabric that uses the pad-dry/cure microwave fixation for progressively persuaded heat within the fabric during curing.

Research limitations/implications

This was done to see the impact of microwave as green and efficient tool with respect to reduction in organic solvents, chemicals and exposer time as well as fixation temperature on the finishing reaction in comparison with traditional pad-dry-cure method.

Practical implications

Poly (MAA)-chitosan graft copolymer as amphoteric biopolymer was expected to impart multifunctional properties to viscose fabrics especially with comparable dry wrinkle recovery angle and minimize the loss in tensile strength in addition to antibacterial properties in comparison with untreated one.

Details

Pigment & Resin Technology, vol. 50 no. 4
Type: Research Article
ISSN: 0369-9420

Keywords

Article
Publication date: 1 November 2013

Chang-E Zhou and Chi-wai Kan

Textiles are a suitable substrate for the growth of micro-organisms, especially at appropriate humidities and temperatures, when in contact with the human body. Due to the…

Abstract

Textiles are a suitable substrate for the growth of micro-organisms, especially at appropriate humidities and temperatures, when in contact with the human body. Due to the awareness that healthcare textiles enhance the quality of life, antimicrobials and antibacterial textiles have received, and continue to receive, considerable attention from researchers due to their potential to provide quality and safety benefits to many products. However, antimicrobial agents and antibacterial finishing processes have not grown in number because of possible harmful or toxic effects on humans and the environment. The application of rechargeable, safe antimicrobial agents and eco-friendly antibacterial finishing processes are being studied. This paper analyzes the disadvantages and advantages of antimicrobials and antibacterial finishing processes and finds suitable antimicrobials and antibacterial finishing processes for cotton. It is anticipated that the review will be a good resource for those who are interested in antimicrobials and biocidal textile materials, and will help to stimulate further interest in this area.

Details

Research Journal of Textile and Apparel, vol. 17 no. 4
Type: Research Article
ISSN: 1560-6074

Keywords

Article
Publication date: 12 May 2023

Saima Habib, Zulfiqar Ali Raza, Farzana Kishwar and Sharjeel Abid

Present study aimed to nanosilver-treat some commercially dyed denim fabric using an eco-friendly cross-linker of citric acid for possible application in the fabrication of…

Abstract

Purpose

Present study aimed to nanosilver-treat some commercially dyed denim fabric using an eco-friendly cross-linker of citric acid for possible application in the fabrication of sustainable antibacterial and nontoxic surgical gowns.

Design/methodology/approach

The conventional untreated surgical gowns are prone to bacterial attack making them unprotective and infection carriers. Thereby, nanosilver finishing of the surgical-grade dyed denim fabric was achieved via citrate cross-linking under the pad-dry-cure method. The hence treated denim fabrics were characterized for surface chemical, crystalline, textile, color and antibacterial attributes using both conventional and advanced analytical approaches.

Findings

The results expressed that the prepared denim specimens contained surface roughness at the nanoscale besides some alterations in their textile and color parameters. Both textile and comfort properties of the finished fabric remained in the acceptable range with effective antibacterial activity.

Practical implications

The silver nano-finished dyed denim expressed broad-spectrum antibacterial activity and qualified as a potential substrate in the fabrication of surgical gowns. Such sustainable application of nanosilver finishing could be perused for industrial implications.

Originality/value

This study presents citric acid as a crosslinking agent to impregnate the commercially dyed denim fabric for potential application in the fabrication of surgical gowns. The application of nanosilver on prior citrated dyed-grown fabrics could be a novel approach. This study used approximately all the reagents and auxiliaries as bio-based to ensure the nontoxicity and sustainability of the resultant fabric.

Details

Pigment & Resin Technology, vol. ahead-of-print no. ahead-of-print
Type: Research Article
ISSN: 0369-9420

Keywords

Article
Publication date: 11 April 2023

Saima Habib, Farzana Kishwar, Zulfiqar Ali Raza and Sharjeel Abid

This study aims to present a sustainable approach in the natural dyeing of cellulose fabric followed by nanosilver finishing through a green crosslinker of citric acid for…

Abstract

Purpose

This study aims to present a sustainable approach in the natural dyeing of cellulose fabric followed by nanosilver finishing through a green crosslinker of citric acid for potential antibacterial surgical gown fabrication.

Design/methodology/approach

The nanosilver finish was reproduced using the chemical reduction method. The fabric dyeing was performed on a lab-scale dyeing machine, whereas silver nano-finishing through a pad-dry-cure approach. Citric acid was used as an eco-friendly crosslinker. The specimens were characterized for antibacterial activity, surface chemical, textile, color properties and finish release trend.

Findings

The results demonstrated the successful application of curcumin dye followed by silver nano-finishing. The resultant fabric exhibited appropriate textile, dyeing performance indicators, hydrophobic behavior and sustainable broad-spectrum antibacterial activity.

Practical implications

The prepared nanosilver-finished/curcumin-treated fabric expressed desirable properties for potential applications in the fabrication of surgical gowns.

Originality/value

The authors found no reports on an extensive examination of nanosilver finishing on the color parameters of curcumin-dyed cellulose fabric while retaining its textile and comfort properties for possible surgical gown fabrication.

Details

Pigment & Resin Technology, vol. ahead-of-print no. ahead-of-print
Type: Research Article
ISSN: 0369-9420

Keywords

Article
Publication date: 22 September 2021

Neha Mulchandani and Vishaka Karnad

The durability of antimicrobial agents and its effectiveness is the most important factor for consumer usage. One important class of antimicrobial agents are inorganic metals and…

145

Abstract

Purpose

The durability of antimicrobial agents and its effectiveness is the most important factor for consumer usage. One important class of antimicrobial agents are inorganic metals and their metal oxides which can be prepared into nanoparticles and can be imparted to enhance the antimicrobial properties. The purpose of this paper is to investigate the effect of three different polymeric binders during the application of zinc oxide (ZnO) nanoparticles on the antimicrobial and performance properties of the finished fabric.

Design/methodology/approach

In this study, ZnO nanoparticles were prepared by a wet chemical method. The nano-particles size distributions was determined using Nanoplus Dynamic Light Scattering particle size distribution analyzer and concentration of nano ZnO 0.1% (w/v) was applied with 2% (w/v) polymeric binders, namely, polyvinyl alcohol (PVA), polyurethane (PU) and butyl acrylic (BA) on cotton fabric by pad dry cure method. The treated samples were tested for physical properties such as tearing strength, tensile strength, crease recovery and air permeability and antimicrobial properties using test method American Association of Textile Chemists and Colorists (AATCC) 100. Further, the content of zinc in the treated samples was determined by the atomic absorption method. The treated fabric was analyzed using fourier transform infrared spectroscopy and scanning electron microscopic and also tested for cytotoxicity as per International Organization for Standardization 10993.

Findings

The results indicated that the type of polymeric binders did not show any influence on the uptake of the zinc content. All treated samples showed positive results >99% with regard to antibacterial property. However, the polymeric treated samples showed a difference in physical properties. The ZnO nano-finish reduced the tensile strength and tearing strength of the fabrics. The difference in crease recovery for samples ZnO/PVA and ZnO/PU was not much except for ZnO/BA where it increased by 38%. The air permeability decreased after application for all treated samples, the lowest among treated samples was in ZnO/PU fabric. Further, ZnO/PVA finished fabric was found to retain antibacterial property up to 50 washes and was effective against MS2 Bacteriophage as a surrogate virus when analyzed as per AATCC 100–2012 test method, and therefore can be potentially used as health-care apparel such as doctors coat and scrub suits.

Originality/value

The outcome of this research is in its contribution to the field of reusable textiles. It highlights the use of nanotechnology to design and develop cotton fabrics for antimicrobial properties which has the potential of preventing the growth of harmful bacteria. The study brings forth the use of ZnO nanoparticles mixed with PVA binder on 100% cotton fabrics which exhibits antibacterial and antiviral properties with adequate wash durability. Currently, there is a high demand of effective durable textiles with barrier properties and the present study provides a promising solution to provide reusable textiles with a greater level of protection.

Details

Research Journal of Textile and Apparel, vol. 26 no. 4
Type: Research Article
ISSN: 1560-6074

Keywords

1 – 10 of 261