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This study aims to present the optimization of parameters and effects of annealing and vapor smoothing post-processing treatments on the surface roughness and tensile mechanical properties of fused deposition modeling (FDM) printed acrylonitrile butadiene styrene (ABS).

Full-factorial test matrices were designed to determine the most effective treatment parameters for post-processing. The parameters for annealing were temperature and time, whereas the parameters for the vapor smoothing were volume of acetone and time. Analysis of surface roughness and tensile test results determined influences of the levels of parameters to find an ideal balance between mechanical properties and roughness.

Optimal parameters for vapor smoothing and annealing were determined. Vapor smoothing resulted in significantly higher improvements to surface roughness than annealing. Both treatments generally resulted in decreased mechanical properties. Of all treatments tested, annealing at 100 °C for 60 min provided the greatest benefit to tensile properties and vapor smoothing with 20 mL of acetone for 15 min provided the greatest benefit to surface roughness while balancing effects on properties.

Vapor smoothing and annealing of FDM ABS have typically been studied independently for their effects on surface roughness and material properties, respectively, with varying materials and manufacturing methods. This study objectively compares the effects of each treatment on both characteristics simultaneously to recommend ideal treatments for maximizing the balance between the final quality and performance of FDM components. The significance of the input variables for each treatment have also been analyzed. These findings should provide value to end-users of 3D printed components seeking to balance these critical aspects of manufacturing.

A new method of studying the accelerated ageing of interconnection materials is applied to a high‐stability thick film resistor system (the Du Pont HS‐80 system). The new method, referred to hereafter as the in‐situ method, allows measurement of the electrical resistance of a thick film resistor to a resolution of a few ppm during accelerated ageing. With the in‐situ technique, the electrical resistance measurements are performed at the elevated ageing temperature during the ageing treatment, whereas with the conventional ageing method the resistance measurements are carried out at room temperature, between subsequent annealing steps. The measuring resolution obtainable with the in‐situ method is orders of magnitude better than with the conventional method. The ageing kinetics can therefore be studied on a shorter time scale and in greater detail than with the conventional method. In this paper, the authors use the in‐situ method to study the accelerated ageing of the Du Pont HS‐80 thick film resistor system, encapsulated with a proper glaze. It will be shown that kinetics of the resistance drift observed in this system cannot be described by an Arrhenius‐type equation. The ageing data can only be interpreted in terms of a kinetic model incorporating a spectrum of activation energies for the ageing process. Such a model is given, and is shown to provide a good explanation of the observed ageing behaviour. The physical process that causes the observed ageing is most probably diffusion of silver from the contacting terminals into the amorphous matrix of the thick film resistor.

The purpose of this paper is to investigate the post-treatment processes on lattice structures of selective laser melting. Moreover, the effect of pressure during hot isostatic pressing (HIP) is determined.

Three post-treatment processes, annealing at 650°C, 920°C and HIP were adopted. The microstructure evolution and mechanical properties of selective lasering melted Ti6Al4V lattice structures after post-treatment were systematically investigated by optical microscope, scanning electron microscope, electron backscattered diffraction, differential scanning calorimetry and quasi-static mechanics tests.

The main findings in this paper are as below: first, the pores existing in the samples as-fabricated, annealed at 650°C and 920°C are disappeared after HIP. Second, the microstructure and compressive properties after HIP are similar to that after pure annealing at the same temperature. However, the HIPed sample had the highest number of cycles to failure. Third, the fracture mechanism of as-fabricated samples changes from mixed fracture to the micro-voids accumulation fracture after post-treatment processes.

HIP post-treatment can be replaced by annealing at the same temperature when the requirement for porosity and fatigue life is not very high.

The purpose of this study was to conduct various heat treatments (HT) such as stress relief annealing, mill annealing, recrystallization (α + β) annealing and β annealing followed by furnace cooling (FC) that were implemented to determine the effect of these on mechanical properties and the microstructure of selective laser melted and wrought samples. The mentioned annealings have been carried out to achieve the related standards in the fabrication of surgery implants.

In this paper, based on F2924-14 ASTM standard SLM and conventionally wrought parts were prepared. Then HT was performed and different characteristics such as microstructure, mechanical properties, macro-hardness and fracture surface for selective laser melted and wrought parts were analysed.

The results show that the high cooling rate in selective laser melting (SLM) generates finer grains. Therefore, tensile strength and hardness increase along with a reduction in ductility was noticed. Recrystallization annealing appears to give the best combination of ductility, strength and hardness for selective laser melted parts, whilst for equivalent wrought samples, increasing HT temperature results in reduction of mechanical properties.

The contributions of this paper are discussing the effect of different annealing on mechanical properties and microstructural evolution based on new ASTM standards for selective laser melted samples and comparing them with wrought parts.

The purpose of this study is to evaluate and compare the mechanical performance of FFF parts when subjected to post processing thermal treatment. Therefore, a study of the annealing treatment influence on the mechanical properties was performed. For this, two different types of Nylon (PA12) were used, FX256 and CF15, being the second a short fibre reinforcement version of the first one.

In this study, tensile and flexural properties of specimens produced via FFF were determined after being annealed at temperatures of 135°C, 150°C or 165°C during 3, 6, 12 or 18 h and compared with the non-treated conditions. Differential scanning calorimetry (DSC) was performed to determine the degree of crystallinity. To evaluate the annealing parameters’ influence on the mechanical properties, a full factorial design of experiments was developed, followed by an analysis of variance, as well as post hoc comparisons, to determine the most significative intervening factors and their effect on the results.

The results indicate that CF15 increased its tensile modulus, strength, flexural modulus and flexural strength around 11%, while FX256 presented similar values for tensile properties, doubling for flexural results. Flexural strain presented an improvement, indicating an increased interlayer behaviour. Concerning to the DSC analysis, an increase in the degree of crystallinity for all the annealed parts.

Overall, the annealing treatment process cause a significant improvement in the mechanical performance of the material, with the exception of 165°C annealed specimens, in which a decrease of the mechanical properties was observed, resultant of material degradation.

AN alloy for which many uses are predicted in the aircraft industry is beryllium copper. The best known applications so far are found in instrument parts, beryllium copper being non‐magnetic, and in adjustable‐pitch propeller hub cones and retractable landing gear parts, where good wear resistance is required. The alloy also has possibilities in the working of magnesium. In magnesium working machines must be kept free from chips, tools must be kept sharp, and plenty of lubrication must be provided to avoid fire. Special tools have been designed to keep down friction heat, and they should be used in working with magnesium. These tools have wider clearance angles and their surfaces are smaller than tools used with other materials. The comparatively high hardness and shock resistance of beryllium copper permits it to be used for non‐sparking hand tools such as hammers, chisels, wrenches, wrecking bars, drift pins and scrapers.

This paper aims to investigate the corrosion behaviour of heat-treated and cryorolled Al 5052 alloys in different Cl⁻ ion concentrations.

NaCl solutions with concentrations of 0, 0.5, 3.5 and 5.5 per cent were selected. Samples were subjected to pre-heat treatment (annealing at 300 °C and solution treatment at 540 °C) and cryorolling up to 30 per cent reduction before undergoing corrosion tests. The corrosion behaviour of the samples was then investigated by potentiodynamic polarization. The microstructure of the corroded samples was evaluated under an optical microscope, and the percentages of pits on their surfaces were calculated.

The cryorolled samples had a lower corrosion rate than the samples that were not cryorolled. The cryorolled sample that underwent solution treatment showed the highest corrosion resistance among all the samples tested.

The commercial impact of the study is the possibility of using the cryorolled Al alloy in various ion chloride environment.

The obtained results help in understanding the corrosion behaviour of cryorolled samples under different heat treatment conditions.

The purpose of this paper is to report on the developments in manufacturing soft magnetic materials using laser powder bed fusion (L-PBF).

Ternary soft magnetic Fe-49Co-2V powder was produced by gas atomization and used in an L-PBF machine to produce samples for material characterization. The L-PBF process parameters were optimized for the material, using a design of experiments approach. The printed samples were exposed to different heat treatment cycles to improve the magnetic properties. The magnetic properties were measured with quasi-static direct current and alternating current measurements at different frequencies and magnetic flux densities. The mechanical properties were characterized with tensile tests. Electrical resistivity of the material was measured.

The optimized L-PBF process parameters resulted in very low porosity. The magnetic properties improved greatly after the heat treatments because of changes in microstructure. Based on the quasi-static DC measurement results, one of the heat treatment cycles led to magnetic saturation, permeability and coercivity values comparable to a commercial Fe-Co-V alloy. The other heat treatments resulted in abnormal grain growth and poor magnetic performance. The AC measurement results showed that the magnetic losses were relatively high in the samples owing to formation of eddy currents.

The influence of L-PBF process parameters on the microstructure was not investigated; hence, understanding the relationship between process parameters, heat treatments and magnetic properties would require more research.

The relationship between microstructure, chemical composition, heat treatments, resistivity and magnetic/mechanical properties of L-PBF processed Fe-Co-V alloy has not been reported previously.

Materials have been developed in recent years which are particularly well‐suited for use in fabricated gas turbine hot section components. Among these are HAYNES® alloy No. 230 and HASTELLOY® alloy S. These alloys combine very good performance characteristics with capability for fabrication into such complex components as combustion chambers, afterburner flame‐holders, seal rings, and thermocouple/probe assemblies. The properties and fabrication characteristics of these two materials are reviewed and compared with other well‐known gas turbine alloys.

This study aims to review the recent advancements in high entropy alloys (HEAs) called high entropy materials, including high entropy superalloys which are current potential alternatives to nickel superalloys for gas turbine applications. Understandings of the laser surface modification techniques of the HEA are discussed whilst future recommendations and remedies to manufacturing challenges via laser are outlined.

Materials used for high-pressure gas turbine engine applications must be able to withstand severe environmentally induced degradation, mechanical, thermal loads and general extreme conditions caused by hot corrosive gases, high-temperature oxidation and stress. Over the years, Nickel-based superalloys with elevated temperature rupture and creep resistance, excellent lifetime expectancy and solution strengthening L12 and γ´ precipitate used for turbine engine applications. However, the superalloy’s density, low creep strength, poor thermal conductivity, difficulty in machining and low fatigue resistance demands the innovation of new advanced materials.

HEAs is one of the most frequently investigated advanced materials, attributed to their configurational complexity and properties reported to exceed conventional materials. Thus, owing to their characteristic feature of the high entropy effect, several other materials have emerged to become potential solutions for several functional and structural applications in the aerospace industry. In a previous study, research contributions show that defects are associated with conventional manufacturing processes of HEAs; therefore, this study investigates new advances in the laser-based manufacturing and surface modification techniques of HEA.

The AlxCoCrCuFeNi HEA system, particularly the Al0.5CoCrCuFeNi HEA has been extensively studied, attributed to its mechanical and physical properties exceeding that of pure metals for aerospace turbine engine applications and the advances in the fabrication and surface modification processes of the alloy was outlined to show the latest developments focusing only on laser-based manufacturing processing due to its many advantages.

It is evident that high entropy materials are a potential innovative alternative to conventional superalloys for turbine engine applications via laser additive manufacturing.