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Synthetic textile materials are noted as one of the major contributors to microfiber pollution through laundry. Though many research works evaluated microfiber pollution, the solutions provided to control microfiber shedding are meager. The existing products collect or filter the microfiber from laundry effluent and restrict the direct leaching. However, no methods were proposed to effectively reduce the shedding from the textile itself.

This research is aimed to analyze the influence of surface modification of polyester knitted textiles by sodium hydroxide, on microfiber shedding. Response surface methodology was adapted to optimize different treatment parameters (alkali concentration, treatment time and temperature).

The results show that the sodium hydroxide concentration and treatment time had a negative correlation with microfiber shedding reduction. Whereas, treatment temperature had a positive correlation with microfiber shedding reduction. The statistical analysis revealed that 0.4 M concentration, 90°C temperature and 24 min of treatment time was the best process condition for minimum microfiber release. The same was confirmed with a practical experiment and a significant reduction of 80.63% in microfiber shedding after alkali treatment was found.

Alkali treatment of different knitted polyester fabrics with various knit structures and mass per square meter showed a significant reduction in microfiber shedding. The repeated laundry performed for 20 washes with surface-modified samples showed a significant reduction in microfiber release at every wash cycle and ensured the longevity of the effect.

Gourd fibres (GF) are a natural biodegradable fibre material with excellent mechanical properties and high tensile strength. The use of natural fibres in composite materials has gained popularity in recent years due to their various advantages, including renewability, low cost, low density and biodegradability. Gourd fibre is one such natural fibre that has been identified as a potential reinforcement material for composites. However, it has low surface energy and hydrophobic nature, which makes it difficult to bond with matrix materials such as polyester. To overcome this problem, chemically adapted gourd fibre has been proposed as a solution. Chemical treatment is one of the most widely used methods to improve the properties of natural fibres. This research evaluates the feasibility and effectiveness of incorporating chemically adapted gourd fibre into polyester composites for industrial fabrication. The purpose of this study is to examine the application of chemically modified GF in the production of polyester composite engineering materials.

This work aims to evaluate the effectiveness of chemically adapted gourd fibre in improving the adhesion of gourd fibre with polyester resin in composite fabrication by varying the GF from 5 to 20 wt.%. The study involves the preparation of chemically treated gourd fibre through surface modification using sodium hydroxide (NaOH), permanganate (KMnO₄) and acetic acid (CH₃COOH) coupling agents. The mechanical properties of the modified fibre and composites were investigated. It was then characterized using scanning electron microscopy (SEM) and Fourier transform infrared spectroscopy (FTIR) to determine the changes in surface morphology and functional groups.

FTIR characterization showed that NaOH treatment caused cellulose depolymerization and caused a significant increase in the hydroxyl and carboxyl groups, showing improved surface functional groups; KMnO₄ treatment oxidized the fibre surface and caused the formation of surface oxide groups; and acetic acid treatment induced changes that primarily affected the ester and hydroxyl groups. SEM study showed that NaOH treatment changed the surface morphology of the gourd fibre, introduced voids and reduced hydrophilic tendencies. The tensile strength of the modified gourd fibres increased progressively as the concentration of the modification chemicals increased compared to the untreated fibres.

This work presents the designed composite with density, mechanical properties and microstructure, showing remarkable improvements in the engineering properties. An 181.5% improvement in tensile strength and a 56.63% increase in flexural strength were got over that of the unreinforced polyester. The findings from this work will contribute to the understanding of the potential of chemically adapted gourd fibre as a reinforcement material for composites and provide insights into the development of sustainable composite materials.

Odour formation in textile material is mainly based on the fibre content and also the constituent fibres’ chemical and physical structures. Polyester fibre materials are very profound to form odour after being worn due to their highly oleophilic nature. The purpose of this paper is to analyse the odour formation characteristics of polyester fabric after surface modification through alkali treatment.

Five male participants were allowed to use the alkali-treated and untreated polyester fabrics, which were fixed in the axilla region of their vest. Subjective and objective odour analyses were performed for the worn samples. The odour was evaluated in terms of intensity rating, bacterial population (CFU/ml) and bacterial isolation.

The results showed that alkali treatment was effective in odour reduction in polyester fabric (p<0.005). The bacterial population density was also reduced significantly (p<0.005) in the alkali-treated polyester fabric compared to the untreated polyester fabric after the wear trial. The alkali treatment affected the surface structure of the polyester fabric and thus changed it from hydrophilic to hydrophobic. This was confirmed by the moisture management test results.

The odour formation in the polyester fabric can be controlled by simple surface modification process like alkali treatment, and thus the value of the product can be increased in the apparel sector.

–Prosopis juliflora is a raw material for long-term sustainable production of bioethanol. The purpose of this paper is to identify the best combination of pre-treatment strategy implemented on the lignocellulosic biomass Prosopis juliflora for bioethanol production.

Pre-treatment of lignocellulosic material was carried out using acid, alkali and sonication in order to characterize the biomass for bioethanol production. Prosopis juliflora stem was subjected to steam at reduce temperature (121°C) for one hour residence time initially. Further acid and alkali treatment was carried out individually followed by combinations of acid and sonication, alkali and sonication. Sodium hydroxide, potassium hydroxide, hydrochloric acid, sulphuric acid and nitric acid were used with 3 per cent (w/v) and 3 per cent (v/v) concentration under temperature range of 60-90°C for 60 min incubation time. Sonication under 60°C for 5 min and 40 KHz frequency was carried out. Pre-treated sample were further characterised using field emission scanning electron microscope and Fourier transform infrared spectroscopy to understand the changes in surface morphology and functional characteristics.

In sono assisted acid treatment-based method, nitric acid yields better cellulose content at 70°C and removes lignin that even at increased temperatures no burning was observed.

The paper adds to the scarce research available on the combination of auto hydrolysis coupled with sono assisted acid/alkali hydrolysis which is yet to be practiced.

The purpose of this study is to investigate surface treatments and fiber types on adhesion properties polylactic acid (PLA) three-dimensional (3D) parts printed on woven fabrics.

The cotton, flax and jute fabrics were exposed to alkali, hydrogen peroxide, stearic acid and ionic liquid treatments to modify surface characteristics before PLA 3D printing. The modification efficiency was assessed with Fourier transform infrared spectroscopy (FTIR) and scanning electron microscope (SEM) analyses. Then, fused deposition modeling (FDM) printer and PLA filament were used for 3D printing onto the untreated and treated fabrics. The adhesion strength between the fabrics and PLA 3D parts were tested according to DIN 53530 via universal tensile tester.

The fabric structure is effective on adhesion force and greater values were observed for plain weave fabrics. Maximum separation forces were obtained for alkali pretreated fabrics among jute and cotton. Hydrogen peroxide treatment also increased adhesion forces for jute and cotton fabrics while decreasing for flax fabrics. Stearic acid and ionic liquid treatments reduced adhesion forces compared to untreated fabrics. Treatments are effective to alter adhesion via changing surface chemistry, surface morphology and fabric physical properties but display different effects related to fabric material.

This study provides experimental information about effects of different fiber types and surface treatments on adhesion strength of PLA 3D parts. There is limited research about comprehensive observation on 3D printing on cellulosic-woven fabrics.

This paper aims to investigate the resultant optimal ultimate tensile strength, elongation, flexural strength and modulus, compression strength and impact strength of fabricated alkali-treated Lagenaria siceraria fiber (LSF)-reinforced polymer matrix composite by optimizing input factors and microstructural characterization by influencing fiber length, fiber concentration and treatment condition of LSF.

The fabrication of LSF-reinforced composite specimens involved surface treatment followed by custom experimental design using a simple hand layup process. The wear analysis was performed by a multi-tribotester TR25 machine, and the developed model was validated by using statistical software Design Expert V.8 and analysis of variance (ANOVA). The surface morphology of the sample was also analyzed by field emission scanning electron microscopy.

The alkali treatment for LSFs had reduced the hemicellulose, and enhanced mechanical performance was observed for 30 wt.% concentration of L. siceraria in epoxy resin. Thermogravimetric analysis revealed thermal stability up to 245°C; microstructure revealed fiber entanglements in case of longer fiber length and compression strength reduction; and the surface-treated fiber composites exhibited reduced occurrences of defects and enhanced matrix–fiber bonding. Enhanced mechanical performances were observed, namely, ultimate tensile strength of 17.072 MPa, elongation of 1.847%, flexural strength of 50.4 MPa, flexural modulus of 3,376.31 GPa, compression strength of 52.154 MPa and impact strength of 0.53 joules.

The novel approach of optimizing and characterizing alkali surface-treated LSF-reinforced epoxy matrix composite was explored, varying fiber length and concentrations for specimens by empirical relations and experimental design to obtain optimal performance validated by ANOVA. Enhanced properties were obtained for: 7 mm fiber length and 30 wt.% concentration of fiber in the composite for alkali-treated fiber.

Stereolithography is a well-established technique for producing complex part for rapid prototyping purpose by using UV or laser as a source for curing process. This technique has been implemented in a lot of industrial sectors. However, the parts fabricated by this technique exhibit low mechanical and thermal properties hindering a fast-growing application. The purpose of this paper is to propose a new method of digital light rapid prototyping (DLRP) system and investigate the effect of the addition of bamboo fiber with surface modification on improvement of mechanical properties of urethane diacrylate/bamboo composite.

Test specimens were fabricated using aliphatic urethane diacrylate photopolymer as matrix material and bamboo fiber as reinforce material. Adhesion between matrix and reinforce materials is a big issue in compositing, especially when handling bamboo as hydrophilic material and urethane diacrylate as hydrophobic material. To overcome this problem, two surface modifications of bamboo fiber, alkali treatment and silane treatment, were implemented.

As a result, bamboo fiber can increase mechanical properties of urethane diacrylate photopolymer fabricated by rapid prototyping system.

In this paper, the authors investigate the effect of the addition of bamboo powder with surface modification on mechanical properties. Test specimens were fabricated using aliphatic urethane diacrylate photopolymer as matrix material and bamboo powder as reinforce material.

The impact of potassium permanganate (KMnO₄) treatment on the tensile strength of an alkali-treated pineapple leaf fiber (PALF) reinforced with tapioca-based bio resin (cassava starch) was studied.

The PALF was exposed to sodium hydroxide (NaOH) treatment in varying concentrations of 2.0, 3.7, 4.5 and 5.5g prior to the fiber treatment with KMnO₄. The treated and untreated PALFs were reinforced with tapioca-based bio resin. Subsequently, they were subjected to Fourier transform infrared (FTIR) and tensile test analysis.

The FTIR analysis of untreated PALF revealed the presence of O-H stretch, N-H stretch, C=O stretch, C=O stretch and H-C-H bond. The tensile test result confirmed the highest tensile strength of 35N from fiber that was reinforced with 32.5g of cassava starch and treated with 1.1g of KMnO₄. In comparison, the lowest tensile strength of 15N was recorded for fiber reinforced with 32.5g of cassava starch without KMnO₄ treatment.

Based on the results, it could be deduced that despite the enhancement of bioresin (cassava starch) towards strength-impacting on the fibers, KMnO₄ treatment on PALF is very vital for improved tensile strength of the fiber when compared to untreated fibers. Hence, KMnO₄ treatment on alkali-treated natural fibers preceding reinforcement is imperative for bio-based fibers.

The purpose of this paper is to develop a high-performance composite emulsion cement waterproof coating. The coating has excellent durability and is effective in protecting cement mortar substrates from harmful ions.

The polymer cement waterproof coatings with different emulsion compounding ratios were tested for mechanical properties and water resistance after alkali immersion, water immersion, thermal aging and UV aging, and the coatings were analyzed by infrared spectroscopy after aging to evaluate its durability. Meanwhile, the coating that presents favorable durability was applied to cement mortar test blocks. The protective effect of the coating on the test blocks was tested by immersion method, and X-ray diffraction analysis was performed on the eroded test blocks.

The coating with neoprene latex/acrylate latex weight ratio of 90/10 presents favorable durability and has superior overall performance. Besides, when it is applied to cement mortar blocks, the coatings effectively reduced the erosive effect of harmful ions on cement mortar blocks, resulting in much lower mass change ratios and less internal structural damage of the blocks significantly.

The obtained coating will be of great application potential for use in building waterproofing construction. Moreover, the coating can practically prevent chloride ions and sulfate ions from penetrating cement-based materials.

The purpose of this study is to understand the behavior of hybrid bio-composites under varied applications.

Fabrication methods and material characterization of various hybrid bio-composites are analyzed by studying the tensile, impact, flexural and hardness of the same. The natural fiber is a manufactured group of assembly of big or short bundles of fiber to produce one or more layers of flat sheets. The natural fiber-reinforced composite materials offer a wide range of properties that are suitable for many engineering-related fields like aerospace, automotive areas. The main characteristics of natural fiber composites are durability, low cost, low weight, high specific strength and equally good mechanical properties.

The tensile properties like tensile strength and tensile modulus of flax/hemp/sisal/Coir/Palmyra fiber-reinforced composites are majorly dependent on the chemical treatment and catalyst usage with fiber. The flexural properties of flax/hemp/sisal/coir/Palmyra are greatly dependent on fiber orientation and fiber length. Impact properties of flax/hemp/sisal/coir/Palmyra are depended on the fiber content, composition and orientation of various fibers.

This study is a review of various research work done on the natural fiber bio-composites exhibiting the factors to be considered for specific load conditions.