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This paper aims to provide a comparison between the mechanical performance and microstructural aspects of stainless steel 17-4 PH processed using, respectively, two technologies: atomic diffusion additive manufacturing (ADAM) and metal fused filament fabrication (MFFF).

Different tensile specimens have been printed using an industrial system and a consumer three-dimensional (3D) printer, varying two main 3D printing parameters. Mechanical and microstructural tests are executed to make a comparison between these two technologies and two different feedstock material, to identify the main differences.

These 3D printing processes make parts with different surface quality, mechanical and microstructural properties. The parts, printed by the industrial system (ADAM), showed lower values of roughness, respect those produced using the 3D consumer printer (MFFF). The different sintering process parameters and the two debinding methods (catalytic or solvent based) affect the parts properties such as porosity, microstructure, grain size and amount of δ-ferrite. These proprieties are responsible for dissimilar tensile strength and hardness values. With the aim to compare the performances among traditional metal additive technology, MFFF and ADAM, a basic analysis of times and costs has been done.

The application of two metal extrusion techniques could be an alternative to other metal additive manufacturing technologies based on laser or electron beam. The low cost and printing simplicity are the main drivers of the replacements of these technologies in not extreme application fields.

The purpose of this paper is to understand the effect of four different factors: building orientation, heat treatment (solution annealing and aging), thermal history and process parameters on the mechanical properties and microstructural features of 17-4 precipitation hardening (PH) stainless steel (SS) parts produced using selective laser melting (SLM).

Various sets of test samples were built on a ProX 100™ SLM system under argon environment. Characterization studies were conducted using mechanical tensile and compression test, microhardness test, optical microscopy, X-ray diffraction and scanning electron microscopy.

Results indicate that building orientation has a direct effect on the mechanical properties of SLM parts, as vertically built samples exhibit lower yield and tensile strengths and elongation to failure. Post-SLM heat treatment proved to have positive effects on part strength and hardness, but it resulted in reduced ductility. Longer inter-layer time intervals between the melting of successive layers allow for higher austenite content because of lower cooling rates, thus decreasing material hardness. On the other hand, tensile properties such as elongation to failure, yield strength and tensile strength were not significantly affected by the change in inter-layer time intervals. Similar to other AM processes, SLM process parameters were shown to be instrumental in achieving desirable part properties. It is shown that without careful setting of process parameters, parts with defects (porosity and unmelted powder particles) can be produced.

Although the manufacturing of 17-4 PH SS using SLM has been investigated in the literature, the paper provides the first comprehensive study on the effect of different factors on mechanical properties and microstructure of SLM 17-4 PH. Optimizing process parameters and using heat treatment are shown to improve the properties of the part.

Regardless of the materials used, additive manufacturing (AM) is one of the most popular emerging fabrication processes used for creating complex and intricate structural components. This study aims to investigate the effects of process parameters – namely, nozzle diameter, layer thickness and infill density on microstructure as well as the mechanical properties of 17–4 PH stainless steel specimens fabricated via material extrusion AM.

The experimental approach investigates the effects of printing parameters, including nozzle diameter, layer thickness and infill density, on surface roughness, physical and mechanical properties of the printed specimens. The tests were triplicated to ensure reproducibility of the experimental results.

The highest ultimate tensile strength, 795.26 MPa, was obtained on specimen that was fabricated with a 0.4 mm nozzle diameter, 0.14 mm layer thickness and 30% infill density. Furthermore, a 0.4 mm nozzle diameter also provided slightly better ductility. This came at the expense of surface finishing, as a 0.25 mm nozzle diameter exhibited better surface finishing over a 0.4 mm nozzle diameter. Infill density was shown to slightly influence the tensile properties, whereas layer thickness showed a significant effect on surface roughness. By contrast, hardness and ductility were independent of nozzle diameter, layer thickness and infill density.

This paper presents a comprehensive analysis relating to various input printing parameters on microstructural, physical and mechanical properties of additively manufactured 17–4 PH stainless steel to improve the printability and processability via AM.

Characteristics of the metal powder are a key factor in the success of powder bed fusion (PBF) additive manufacturing. Powders for PBF from different manufacturers may have a different particle size and/or bulk packing and flow behavior. Powder properties change as the powder is reused for multiple builds. This study seeks to measure the variability of commercial 17-4 PH stainless steel powders to determine the effect of powder variability on part density and demonstrate characterization methods that ensure part quality.

Commercial atomized metal powders from four different vendors were produced with two different atomizing gases (N2 and argon). Powder was characterized in both new and extensively reused conditions. All powders were characterized for flow and packing behavior, particle size and internal porosity. Coupons were manufactured using the laser PBF process with optimized scan strategy and exposure parameters. The quality of fabricated parts was measured using bulk density measurement.

Despite differences in powder flowability and particle size, fully dense parts (>99 per cent) were produced using all powders, except one. Residual porosity in these parts appeared to result from gas trapped in the powder particles. The powder with extensive reuse (400+ h in machine fabrication environment) exhibited reduced flowability and increased fraction of fine particles, but still produced full density parts.

This study demonstrates that full density parts can be fabricated using powders with a range of flowability and packing behavior. This suggests that a single flowability measurement may be sufficient for quality assurance in a production environment.

The mechanical characterization of selective laser melting (SLM) parts is an industrial challenge. This paper aims to propose a methodology to control the fatigue life of 17-4Ph stainless steel by selecting the most relevant manufacturing parameters: i.e. laser power, laser travel speed, hatch spacing and laser defocusing.

A rough and refined design of experiment (DOE) is carried out to target the best combination of process parameters. A response surface model is then constructed to predict the parameter combination that optimizes the fatigue performance.

This study results show that the fatigue limit of the specimens manufactured by SLM (471.7 MPa at 107 cycles) has reached near 90% of the value found in samples machined from a bar. This demonstrates the applicability of the method proposed to optimize the SLM process and control the fatigue life of 17-4Ph stainless steel. The study results are compared with other research works and provide an increase of 18% to the fatigue limit.

This study showcases a DOE methodology to optimize the SLM parameters to achieve fatigue performance as great as that of solid 17-4Ph stainless steel.

The extrusion-based additive manufacturing method followed by debinding and sintering steps can produce metal parts efficiently at a relatively low cost and material wastage. In this study, 316L stainless-steel metal filled filaments were used to print metal parts using the extrusion-based fused filament fabrication (FFF) approach. The purpose of this study is to assess the effects of common FFF printing parameters on the geometric and mechanical performance of FFF manufactured 316L stainless-steel components.

The microstructural characteristics of the metal filled filament, three-dimensional (3D) printed green parts and final sintered parts were analysed. In addition, the dimensional accuracy of the green parts was evaluated, as well as the hardness, tensile properties, relative density, part shrinkage and the porosity of the sintered samples. Moreover, surface quality in terms of surface roughness after sintering was assessed. Predictive models based on artificial neural networks (ANNs) were used for characterizing dimensional accuracy, shrinkage, surface roughness and density. Additionally, the response surface method based on ANNs was applied to represent the behaviour of these parameters and to identify the optimum 3D printing conditions.

The effects of the FFF process parameters such as build orientation and nozzle diameter were significant. The pore distribution was strongly linked to the build orientation and printing strategy. Furthermore, porosity decreased with increased nozzle diameter, which increased mechanical performance. In contrast, lower nozzle diameters achieved lower roughness values and average deviations. Thus, it should be noted that the modification of process parameters to achieve greater geometrical accuracy weakened mechanical performance.

Near-dense 316L austenitic stainless-steel components using FFF technology were successfully manufactured. This study provides print guidelines and further information regarding the impact of FFF process parameters on the mechanical, microstructural and geometric performance of 3D printed 316L components.

This paper aims to establish the microstructures and the process-structure relationships in duplex stainless steel powders consolidated by selective laser melting (SLM).

A priori data on energy density levels most appropriate to consolidation of duplex stainless steel powders through SLM served as the basis to converge on the laser settings. Experimental designs with varying laser power and scan speeds and test pieces generated allowed metallographic evaluations based on optical and scanning electron microscopy and electro backscatter diffraction analyses.

Duplex stainless steel powders are established for processing by SLM. However, the dynamic point heat source and associated transient thermal fields affect the microstructures to be predominantly ferritic, with grains elongated in the build direction. Austenite precipitated either at the grain boundaries or as Widmanstätten laths, whereas the crystallographic orientations and the grain growth are affected around the cavities. Considerable CrN precipitation is also evidenced.

Duplex stainless steels are relatively new candidates to be brought into the additive manufacturing realm. Considering the poor machinability and other difficulties, the overarching result indicating suitability of duplex powders by SLM is of considerable value to the industry. More significantly, the metallographic evaluation and results of the current research allowed further understanding of the material consolidation aspects and pave ways for fine tuning and establishment of the process-structure-property relationships for this important process-material combination.

Additive manufacturing (AM) has the potential to revolutionise the fabrication of complex surgical instruments. However, AM parts typically have a higher surface roughness compared to machined or fine cast parts. High surface roughness has important implications for surgical instruments, particularly in terms of cleanliness and aesthetic considerations. In this study, bulk surface finishing methods are described to produce end-use selective laser melting parts.

The aim was to achieve a surface finish as close as possible to machined parts (Ra = 0.9 µm, Wa = 0.2 µm, Pv = 7.3 µm). A sample coupon was designed to systematically evaluate different finishing techniques. Processes included bulk finishing, blasting and centrifugal finishing methods on individual parts, as well as heat treatment before and after surface finishing.

Abrasive blasting or centrifugal finishing alone was not adequate to achieve an end-use surface finish. White oxide vapour blasting at high water pressure was the most effective of the abrasive blasting processes. For centrifugal finishing, a 4 h runtime resulted in an acceptable reduction in surface roughness (Ra = 2.9 µm, Wa = 2.0 µm, Pv = 34.6 µm: inclined surface [30°]) while not significantly increasing part radii. The combination of finishing methods resulting in the smoothest surfaces was white oxide blasting followed by 4 h of centrifugal finishing and a final glass bead blast (Ra = 0.6 µm, Wa = 0.9 µm, Pv = 6.9 µm: inclined surface [30°]). The order of these methods was important because white oxide blasting was significantly less effective when applied after the centrifugal finishing.

Collectively, these results describe the development of a practical bulk finishing method for stainless steel surgical instruments produced by AM.

This study aims to design and fabricate a customized multi-rooted dental implant (MRDI) for a canine strategic tooth to reduce surgical time/effort, and better assembly features, leading to enhanced primary and secondary stability and load-bearing capabilities by direct-metal laser sintering (DMLS).

A fractured tooth of a male German Shepherd three-year-old dog (extracted from a cadaver) was selected as the subject for the proposed work. The computer-aided design model of the implant was developed on SOLIDWORKS after a detailed review of literature and consultation with a veterinary doctor about the surgical procedures. Static stress analysis on the implant assembly and residual stress analysis with boundary distortion were performed on each part of the implant subassembly to ensure the fool-proof design.

The functional prototype of the innovative MRDI assembly through DMLS was successfully prepared with acceptable dimensional stability, surface roughness (Ra) and refined microstructure. The 3D printed functional prototype was observed to be residual stress-proof during printing and can bear up to 800 N bite force (required for an adult dog).

Innovative MRDI assembly has been 3D printed by using 17–4 precipitate hardened stainless steel without compromising the strength and can be implanted without bone grafting for better primary stability. Also, the prepared implant will be better for secondary stability due to enhanced osseointegration.

The corrosion behaviour of low alloy steel type AISI 4130 (before and after nitriding) and austenitic stainless steel type AISI 304L were studied in tap water +3.5 per cent NaCl. A liquid nitriding process had been applied on the low alloy steel.

The tests that were carried out in this study were anodic polarization, rotating bending fatigue and axial fatigue using compact tension (CT). For determining the corrosion potential and pitting potential (breakdown potential) for the alloys, anodic polarization curves were established using the potentiodynamic technique. Rotating bending fatigue tests were used to calculate the fatigue strength and damage ratio. Using linear elastic fracture mechanics, the CT specimens were prepared for determining the threshold stress intensity factor, fatigue crack growth rate and fracture toughness in air and in the solution.

The results showed that nitrided specimens showed higher fatigue strength in air compared to stainless steel. However, the corrosion fatigue limit for both these samples were approximately equal, while this limit for non‐nitrided sample was less. Moreover, the non‐nitrided steel had lower corrosion and pitting potentials than did the stainless steel. In addition, the CT tests showed that the nitrided specimens had a lower resistance to crack initiation in air and the solution compared to the non‐nitrided sample and the stainless steel.

These results can be attributed to the chemical and mechanical behaviour of the nitrided layer constituents, mainly FeN and CrN, which were recognized by X‐ray diffraction. Since, these components consist of very hard particles, they act to increase the hardness and fatigue limit. Moreover, due to the low conductivity of these nitrides, the corrosion and pitting potential of the nitrided steel becomes very high. However, the high breakdown potential does not help to increase the corrosion fatigue or damage ratio values due to the porous nature of the nitrided layer.

Although the nitrided steel had very high fatigue strength and pitting potential, this did not reflect in its corrosion fatigue and/or damage ratio improvement because of its surface roughness and the porous nature of the nitrided layer.