The microstructure and mechanical properties of deposited-IN625 by laser additive manufacturing

Abstract

Purpose

Laser additive manufacturing (LAM) technology based on powder bed has been used to manufacture complex geometrical components. In this study, IN625 superalloys were fabricated by high-power fiber laser without cracks, bounding errors or porosity. Meanwhile, the objectives of this paper are to systemically investigate the microstructures, micro-hardness and the precipitated Laves phase of deposited-IN625 under different annealing temperatures.

Design/methodology/approach

The effects of annealing temperatures on the microstructure, micro-hardness and the precipitated Laves phase were studied by optical microscope (OM), scanning electron microscopy (SEM), X-ray diffraction (XRD), energy dispersive spectrometer (EDS), selected area electron diffraction (SAED), backscattered electron (BSE) imaging in the SEM and transmission electron microscopy (TEM), respectively. The thermal stability of the dendritic morphology about IN625 superalloys was investigated through annealing at temperatures range from 1,000°C to 1,200°C.

Findings

It is found that the microstructure of deposited-IN625 was typical dendrite structure. Besides, some Laves phase precipitated in the interdendritic region results in the segregation of niobium and molybdenum. The thermal stability indicate that the morphology of dendrite can be stable up to 1,000°C. With the annealing temperatures increasing from 1,000 to 1,200°C, the Laves phase partially dissolves into the γ-Ni matrix, and the morphology of the remaining Laves phase is changing from irregular shape to rod-like or block-like shape.

Research limitations/implications

The heat treatment used on the IN625 superalloys is helpful for knowing the evolution of microstructures and precipitated phases thermal stability and mechanical properties.

Practical implications

Due to the different kinds of application conditions, the original microstructure of the IN625 superalloys fabricated by LAM may not be ideal. So exploring the influence of annealing treatment on IN625 superalloys can bring theory basis and guidance for actual production.

Originality/value

This study continues valuing the fabrication of IN625 by LAM. It shows the effect of annealing temperatures on the shape, size and distribution of Laves phase and the microstructures of deposited-IN625 superalloys.

Citation

Qin, L., Chen, C., Zhang, M., Yan, K., Cheng, G., Jing, H. and Wang, X. (2017), "The microstructure and mechanical properties of deposited-IN625 by laser additive manufacturing", Rapid Prototyping Journal, Vol. 23 No. 6, pp. 1119-1129. https://doi.org/10.1108/RPJ-05-2016-0081