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The “chiralisation” of Euclidean polygonal tessellations is a novel, recent method which has been used to design new auxetic metamaterials with complex topologies and improved geometric versatility over traditional chiral honeycombs. This paper aims to design and manufacture chiral honeycombs representative of four distinct classes of 2D Euclidean tessellations with hexagonal rotational symmetry using fused-deposition additive manufacturing and experimentally analysed the mechanical properties and failure modes of these metamaterials.

Finite Element simulations were also used to study the high-strain compressive performance of these systems under both periodic boundary conditions and realistic, finite conditions. Experimental uniaxial compressive loading tests were applied to additively manufactured prototypes and digital image correlation was used to measure the Poisson’s ratio and analyse the deformation behaviour of these systems.

The results obtained demonstrate that these systems have the ability to exhibit a wide range of Poisson’s ratios (positive, quasi-zero and negative values) and stiffnesses as well as unusual failure modes characterised by a sequential layer-by-layer collapse of specific, non-adjacent ligaments. These findings provide useful insights on the mechanical properties and deformation behaviours of this new class of metamaterials and indicate that these chiral honeycombs could potentially possess anomalous characteristics which are not commonly found in traditional chiral metamaterials based on regular monohedral tilings.

To the best of the authors’ knowledge, the authors have analysed for the first time the high strain behaviour and failure modes of chiral metamaterials based on Euclidean multi-polygonal tessellations.

The current study mainly focuses on the effect of varying diameter recycled steel fibers (RSF) on mechanical properties of concrete prepared with 25 and 50% of recycled coarse aggregate (RCA) as well as 100% natural aggregate (NA). Two types of RSF with 0.84 mm and 1.24 mm diameter having 30 mm length were incorporated into normal and recycled aggregate concrete (RAC).

The fresh behavior, compressive, splitting tensile, flexural strengths and modulus of elasticity of all the mixes were investigated to evaluate the mechanical properties of RACs. In addition, specimen crack and testing co-relation were analyzed to evaluate fiber response in the RAC.

According to the experimental results, it was observed that mechanical properties decreased with the increment replacement of NA by RCA. However, the RSF greatly improves the mechanical properties of both normal concrete and RACs. Moreover, mixes containing 1.24 mm diameter RSF had a more significant positive impact on mechanical properties than mixes containing 0.84 mm diameter RSF. The 0.84 mm and 1.24 mm RSF addition improved the mixes' compressive, splitting tensile and flexural strength by 10%–19%, 19%–30% and 3%–11%, respectively when compared to the null fiber mix. Therefore, based on the mechanical properties, the 1.24 mm diameter of RSF with 25% replacement of RCA was obtained as an optimum solution in terms of performance improvement, environmental benefit and economic cost.

The practice of RCA in construction is a long-term strategy for reducing natural resource extraction and the negative ecological impact of waste concrete.

This is the first study on the effects of varying size (0.84 mm and 1.24 mm diameter) RSF on the mechanical properties of RAC. Additionally, varying sizes of RSF and silica fume added a new dimension to the RAC.

The aim of this study is to determine the fracture behavior of wool felt and fabric based epoxy composites and their responses to electromagnetic waves.

Notched and unnotched tensile tests of composites made of wool only and hybridized with a glass fiber layer were carried out, and fracture behavior and toughness at macro scale were determined. They were exposed to electromagnetic waves between 8 and 18 GHz frequencies using two horn antennas.

The keratin and lignin layer on the surface of the wool felt caused lower values to be obtained compared to the mechanical values given by pure epoxy. However, the use of wool felt in the symmetry layer of the laminated composite material provided higher mechanical values than the composite with glass fiber in the symmetry layer due to the mechanical interlocking it created. The use of wool in fabric form resulted in an increase in the modulus of elasticity, but no change in fracture toughness was observed. As a result of the electromagnetic analysis, it was also seen in the electromagnetic analysis that the transmittance of the materials was high, and the reflectance was low throughout the applied frequency range. Hence, it was concluded that all of the manufactured materials could be used as radome material over a wide band.

Sheep wool is an easy-to-supply and low-cost material. In this paper, it is presented that sheep wool can be evaluated as a biocomposite material and used for radome applications.

The combined evaluation of felt and fabric forms of a natural and inexpensive reinforcing element such as sheep wool and the combined evaluation of fracture mechanics and electromagnetic absorption properties will contribute to the evaluation of biocomposites in aviation.

This study aims to investigate the possible defects and their root causes in a soft-termination multilayered ceramic capacitor (MLCC) when subjected to a thermal reflow process.

Specimens of the capacitor assembly were subjected to JEDEC level 1 preconditioning (85 °C/85%RH/168 h) with 5× reflow at 270°C peak temperature. Then, they were inspected using a 2 µm scanning electron microscope to investigate the evidence of defects. The reliability test was also numerically simulated and analyzed using the extended finite element method implemented in ABAQUS.

Excellent agreements were observed between the SEM inspections and the simulation results. The findings showed evidence of discontinuities along the Cu and the Cu-epoxy layers and interfacial delamination crack at the Cu/Cu-epoxy interface. The possible root causes are thermal mismatch between the Cu and Cu-epoxy layers, moisture contamination and weak Cu/Cu-epoxy interface. The maximum crack length observed in the experimentally reflowed capacitor was measured as 75 µm, a 2.59% difference compared to the numerical prediction of 77.2 µm.

This work's contribution is expected to reduce the additional manufacturing cost and lead time in investigating reliability issues in MLCCs.

Despite the significant number of works on the reliability assessment of surface mount capacitors, work on crack growth in soft-termination MLCC is limited. Also, the combined experimental and numerical investigation of reflow-induced reliability issues in soft-termination MLCC is limited. These cited gaps are the novelties of this study.

The purpose of this paper is to assess the hydrogen embrittlement sensitivity of carbon gradient heterostructure materials and to verify the reliability of the scratch method.

The surface-modified layer of 18CrNiMo7-6 alloy steel was delaminated to study its hydrogen embrittlement characteristics via hydrogen permeation, electrochemical hydrogen charging and scratch experiments.

The results showed that the diffusion coefficients of hydrogen in the surface and matrix layers are 3.28 × 10⁻⁷ and 16.67 × 10⁻⁷ cm²/s, respectively. The diffusible-hydrogen concentration of the material increases with increasing hydrogen-charging current density. For a given hydrogen-charging current density, the diffusible-hydrogen concentration gradually decreases with increasing depth in the surface-modified layer. Fracture toughness decreases with increasing diffusible-hydrogen concentration, so the susceptibility to hydrogen embrittlement decreases with increasing depth in the surface-modified layer.

The reliability of the scratch method in evaluating the fracture toughness of the surface-modified layer material is verified. An empirical formula is given for fracture toughness as a function of diffused-hydrogen concentration.

This paper aims to investigate the application of 3D printing technology, particularly using sand-type materials, in the creation of artificial rock models for rock mechanics experimentation.

Using a comprehensive analysis, this research explores the utilization of 3D printing technology in rock mechanics. Sand-type materials are specifically investigated for their ability to replicate natural rock characteristics. The methodology involves a review of recent achievements and experimentation in this field.

The study reveals that sand-type 3D printing materials demonstrate comparable properties to natural rocks, including brittle characteristics, surface roughness, microstructural features and crack propagation patterns.

While the research establishes the viability of sand-type 3D printing materials, it acknowledges limitations such as the need for further exploration and validation. Generalizability may be constrained, warranting additional research to address these limitations.

This research contributes insights into the potential application of sand-type 3D printing materials in indoor rock physics experiments. The findings may guide future endeavors in fabricating rock specimens with consistent structures for practical rock mechanics applications.

This paper aims to focus on the reliability of Sn15Bi–xAg and Sn15Bi–xCu solder joints during isothermal aging.

The effects of Ag or Cu additions on the microstructure, interfacial metallic compound layer and shear strength of Sn–15Bi (Sn15Bi) based solder joints during were investigated. The effects of Ag or Cu additions on the microstructure and tensile properties of Sn15Bi-based bulk solders were also investigated to provide a comprehensive analysis. The interfacial morphology and microstructure were observed by scanning electron microscopy and the composition in the structure was examined by energy dispersive spectrometer. The shear tests were carried out on the as-soldered and as-aged joints using a ball shear tester.

The results revealed that by adding Ag or Cu, the microstructure of Sn15Bi solder can be refined. Ag addition increased the tensile strength of Sn15Bi solder but had little effect on elongation. However, Cu addition decreased the tensile strength and elongation of Sn15Bi solder. For solder joints, Ag addition increased the shear strength and toughness of Sn15Bi/Cu joints but Cu addition decreased the shear strength and toughness of Sn15Bi/Cu joints.

The authors can potentially provide a replacement for Sn40Pb traditional solder with Sn15Bi solder by alloying Ag or Cu due to its lower cost and similar melting point as Sn–Pb solder.

This study aims to investigate the performance of filament-based material extrusion additive manufacturing (MEX), combined with debinding and sintering, as a novel approach to manufacturing ceramic components.

A commercial ZrO₂ filament was selected and analysed by infra-red (IR) spectroscopy, rheology and thermo-gravimetry. The influence of the print parameters (layer thickness, flow rate multiplier, printing speed) and sintering cycle were investigated to define a suitable printing and sintering strategy. Biaxial flexure tests were applied on sintered discs realised with optimised printing strategies, and the results were analysed via Weibull statistics to evaluate the mechanical properties of printed components. The hardness and thermal conductivity of sintered components were also tested.

Layer thickness and flow rate multiplier of the printing process were proved to have significant effect on the density of as-printed parts. Optimised samples display a sintered density >99% of the theoretical density, 20% linear sintering shrinkage, a characteristic flexural strength of 871 MPa with a Weibull modulus of 4.9, a Vickers hardness of 12.90 ± 0.3 GPa and a thermal conductivity of 3.62 W/mK. Gyroids were printed for demonstration purposes.

To the best of the authors’ knowledge, this work is the first to apply biaxial flexure tests and Weibull statistics to additively manufactured MEX zirconia components, hence providing comparable results to other additive technologies. Moreover, fractography analysis builds the connection between printing defects and the fracture mechanism of bending. This study also provides guidelines for fabricating high-density zirconia components with MEX.

This study aims to study the formation mechanism of micro-arc oxidation (MAO) coating on AZ31 magnesium alloy and how the annealing process affects its corrosion resistance.

This study involved immersion experiments, electrochemical experiments and slow strain rate tensile experiments, along with scanning electron microscopy, optical microscopy observation and X-ray diffraction analysis.

The findings suggest that annealing treatment can refine the grain size of AZ31 magnesium alloy to an average of 6.9 µm at 300°C. The change in grain size leads to a change in conductivity, which affects the performance of MAO coatings. The MAO coating obtained by annealing the substrate at 300°C has smaller pores and porosity, resulting in better adhesion and wear resistance.

The coating acts as a barrier to prevent corrosive substances from entering the substrate. However, the smaller pores and porosity reduce the channels for the corrosive solution to pass through the coating. When the coating cracks or falls off, the corrosive medium and substrate come into direct contact. Smaller and uniform grains have better corrosion resistance.

The combination of an Engineered Cementitious Composite (ECC) layer and steel plate to reinforce RC beams (ESRB) is a new strengthening method. The ESRB was proposed based on the steel plate at the bottom of RC beams, aiming to solve the problem of over-reinforced RC beams and improve the bearing capacity of RC beams without affecting their ductility.

In this paper, the finite element model of ESRB was established by ABAQUS. The results were compared with the experimental results of ESRB in previous studies and the reliability of the finite element model was verified. On this basis, parameters such as the width of the steel plate, thickness of the ECC layer, damage degree of the original beam and cross-sectional area of longitudinal tensile rebar were analyzed by the verified finite element model. Based on the load–deflection curve of ESRB, ESRB was discussed in terms of ultimate bearing capacity and ductility.

The results demonstrate that when the width of the steel plate increases, the ultimate load of ESRB increases to 133.22 kN by 11.58% as well as the ductility index increases to 2.39. With the increase of the damage degree of the original beam, the ultimate load of ESRB decreases by 23.7%–91.09 kN and the ductility index decreases to 1.90. With the enhancement of the cross-sectional area of longitudinal tensile rebar, the ultimate bearing capacity of ESRB increases to 126.75 kN by 6.2% and the ductility index elevates to 2.30. Finally, a calculation model for predicting the flexural capacity of ESRB is proposed. The calculated results of the model are in line with the experimental results.

Based on the comparative analysis of the test results and numerical simulation results of 11 test beams, this investigation verified the accuracy and reliability of the finite element simulation from the aspects of load–deflection curve, characteristic load and failure mode. Furthermore, based on load–deflection curve, the effects of steel plate width, ECC layer thickness, damage degree of the original beam and cross-sectional area of longitudinal tensile rebar on the ultimate bearing capacity and ductility of ESRB were discussed. Finally, a simplified method was put forward to further verify the effectiveness of ESRB through analytical calculation.